Microwave heating system

Patent metadata

Field	Value
Publication number	US-10390388-B2
Application number	US-201414498721-A
Country	US
Kind code	B2
Filing date	Sep 26, 2014
Priority date	Sep 27, 2013
Publication date	Aug 20, 2019
Grant date	Aug 20, 2019

Abstract

A microwave heating system comprises a bowl, dome and rotor device. The dome is fit to the bowl. The bowl and dome form a volume. The bowl is connected to a microwave source such that a microwave field is supplied to the volume. The microwave field is attenuated in a region between the rotor device and the dome compared to a region between the bowl and the rotor device. The rotor device is rotatably supported by the bowl and supports a reaction vessel. The rotor device includes a base plate with a through-hole and a tubular member that receives the reaction vessel. The base plate and tubular member are metal. The rotor device is coupled to the base plate so that a longitudinal axis of the tubular member passes through the through-hole.

First claim

The invention claimed is:

1. A microwave heating system, comprising
a bowl,
a dome adapted to be fit to the bowl, such that a volume is formed by the bowl and dome, and
a rotor device adapted to support at least one reaction vessel and being rotatably supported by the bowl, the rotor device comprising
a base plate comprising at least one through-hole, and
at least one tubular member having a longitudinal axis and being adapted to receive the at least one reaction vessel and to be coupled to the base plate in such a way that the longitudinal axis of the at least one tubular member passes through the at least one through-hole such that a portion of the at least one reaction vessel when present extends beyond the base plate,
wherein the base plate and the at least one tubular member comprise metal, and
wherein the bowl is adapted to be connected to a microwave generating unit, the microwave generating unit supplying a microwave field to the volume, the base plate and the at least one tubular member configured to attenuate the microwave field in a region between the rotor device and the dome and above a sample when present in the at least one reaction vessel within the at least one tubular member compared to a region between the bowl and the base plate of the rotor device, the microwave field propagating from the region between the bowl and the rotor device into the at least one tubular member and the at least one reaction vessel to heat the sample by microwave absorption.

2. The system according to claim 1 , wherein the bowl and the dome have rotationally symmetric shapes.

3. The system according to claim 1 , wherein the dome is moveably fastened to the bowl.

4. The system according to claim 1 , further comprising
a drive unit for rotating the rotor device.

5. The system according to claim 1 , further comprising
a sensor unit arranged in the region between the rotor device and the dome.

6. The system according to claim 1 , wherein the rotor device further comprises a support element arranged at one side of the base plate, wherein the support element is microwave transparent.

7. The system according to claim 6 , wherein the at least one tubular member is arranged on the side of the base plate opposite to the side at which the support element is arranged.

8. The system according to claim 1 , wherein the base plate and the at least one tubular member are integrally formed.

9. The system according to claim 1 , wherein the metal comprises aluminum, stainless steel and/or a nickel-based alloy.

10. The system according to claim 1 , wherein the base plate and/or the at least one tubular member comprise an anticorrosive coating.

11. The system according to claim 1 , wherein the at least one tubular member is adapted to attenuate microwave propagation within the tubular member.

12. The system according to claim 1 , wherein a diameter of the at least one tubular member is between 10 mm and 50 mm.

13. The system according to claim 1 , wherein the at least one through-hole is a plurality of through-holes, the at least one tubular member is a plurality of tubular members, and the longitudinal axis of each tubular member passes through one of the plurality of through-holes.

14. The system according to claim 13 , wherein the plurality of through-holes comprises a first group of through-holes which are positioned in a vicinity of a periphery of the base plate.

15. The system according to claim 13 , wherein the plurality of through-holes comprises a second group of through-holes which are positioned at a distance between a center of the base plate and a periphery of the base plate.

16. The system according to claim 1 , wherein the at least one reaction vessel has a tubular body, wherein an outer portion of the tubular body has a tooth profile.

17. The system according to claim 16 , wherein the tooth profile has one of square, rectangular, triangular, or rounded cross-sectional shape.

18. The system according to claim 1 , wherein microwave radiation propagates within the at least one tubular member into the rest of the reaction vessel due to a dielectric property of the sample present in the at least one reaction vessel.

19. The system according to claim 1 , wherein the base plate and the at least one tubular member are integrally formed.

20. The system according to claim 1 , wherein the base plate and the at least one tubular member are physically and electrically coupled.

Assignees

• Anton Paar Gmbh

Inventors

• Kotzian Heimo
• Zentner Rainer
• Zach Johannes
• Gangl Elisabeth

Classifications

• B01J2219/1227

  Reactors comprising tubes with open ends · CPC title

• B01J2219/1266

  Microwave deflecting parts · CPC title

• B01J2219/1257

  Rotating supports · CPC title

• B01J2219/1233

  Closure means, such as lids, caps, seals (B01J3/03 takes precedence; pressure relief systems in the lid, e.g. rupture discs B01J2219/0027) · CPC title

• B01J2219/1218

  Multiple reactors · CPC title