Thermomechanical processing of alpha-beta titanium alloys

Patent metadata

Field	Value
Publication number	US-10370751-B2
Application number	US-201715659661-A
Country	US
Kind code	B2
Filing date	Jul 26, 2017
Priority date	Mar 15, 2013
Publication date	Aug 6, 2019
Grant date	Aug 6, 2019

Abstract

One embodiment of a method of refining alpha-phase grain size in an alpha-beta titanium alloy comprises working an alpha-beta titanium alloy at a first working temperature within a first temperature range in the alpha-beta phase field of the alpha-beta titanium alloy. The alloy is slow cooled from the first working temperature. On completion of working at and slow cooling from the first working temperature, the alloy comprises a primary globularized alpha-phase particle microstructure. The alloy is worked at a second working temperature within a second temperature range in the alpha-beta phase field. The second working temperature is lower than the first working temperature. The is worked at a third working temperature in a third temperature range in the alpha-beta phase field. The third working temperature is lower than the second working temperature. After working at the third working temperature, the titanium alloy comprises a desired refined alpha-phase grain size.

First claim

We claim:

1. A method of refining alpha-phase grain size in an alpha-beta titanium alloy workpiece, the method comprising:
forging an alpha-beta titanium alloy at a first forging temperature within a first forging temperature range,
wherein forging the alpha-beta titanium alloy at the first forging temperature comprises at least one pass of both upset forging and draw forging, and
wherein the first forging temperature range spans 300° F. below the beta transus up to a temperature 30° F. below a beta transus temperature of the alpha-beta titanium alloy;

slow cooling the alpha-beta titanium alloy from the first forging temperature, wherein the step of slow cooling comprises cooling the alpha-beta titanium alloy at a cooling rate no greater than 5° F. per minute;
forging the alpha-beta titanium alloy at a second forging temperature within a second forging temperature range,
wherein forging the alpha-beta titanium alloy at the second forging temperature comprises at least one pass of both upset forging and draw forging,
wherein the second forging temperature range comprises a temperature range spanning 600° F. to 350° F. below the beta transus, and
wherein the second forging temperature is lower than the first forging temperature; and

forging the alpha-beta titanium alloy at a third forging temperature within a third forging temperature range,
wherein forging the alpha-beta titanium alloy at the third forging temperature comprises radial forging,
wherein the third forging temperature range is 1000° F. to 1400° F., and
wherein the third forging temperature is lower than the second forging temperature.

2. The method according to claim 1 , wherein the alpha-beta titanium alloy is one of a Ti-6Al-4V alloy (UNS R56400), a Ti-6Al-4V ELI alloy (UNS R56401), a Ti-6Al-2Sn-4Zr-2Mo alloy (UNS R54620), a Ti-6Al-2Sn-4Zr-6Mo alloy (UNS R56260), and a Ti-4Al-2.5V-1.5Fe alloy (UNS 54250).

3. The method according to claim 1 , wherein the alpha-beta titanium alloy is one of a Ti-6Al-4V alloy (UNS R56400) and a Ti-6Al-4V ELI alloy (UNS R56401).

4. The method according to claim 1 , wherein the alpha-beta titanium alloy is a Ti-4Al-2.5V-1.5Fe alloy (UNS 54250).

5. The method according to claim 1 , wherein the slow cooling comprises furnace cooling.

6. The method according to claim 1 , wherein slow cooling comprises transferring the alpha-beta titanium alloy from a furnace set at the first forging temperature to a furnace set at the second forging temperature.

7. The method according to claim 1 , further comprising, after the step of slow cooling the alpha-beta titanium alloy from the first forging temperature, heat treating the alpha-beta titanium alloy at a heat treating temperature in the first forging temperature range, and holding the alpha-beta titanium alloy at the heat treating temperature.

8. The method according to claim 7 , wherein holding the alpha-beta titanium alloy at the heat treating temperature comprises holding the alpha-beta titanium alloy at the heat treating temperature for a heat treating time in a time range from 1 hour to 48 hours.

9. The method according to claim 1 , further comprising annealing the alpha-beta titanium alloy after forging at the second forging temperature.

10. The method according to claim 9 , wherein annealing comprises heating the alpha-beta titanium alloy to an annealing temperature in an annealing temperature range spanning 500° F. to 250° F. below the beta transus and for 30 minutes to 12 hours.

11. The method according to claim 1 , further comprising reheating the alpha-beta titanium alloy intermediate any of the at least one or more press forging steps.

12. The method according to claim 11 , wherein reheating comprises heating the alpha-beta titanium alloy back to a previous working temperature, and holding the alpha-beta titanium alloy at the previous working temperature for a reheating time in a range spanning 30 minutes to 6 hours.

13. The method according to claim 1 , wherein radial forging comprises one series of at least two and no more than six reductions, wherein the radial forging temperature range is 1100° F. to 1400° F.

14. The method according to claim 1 , wherein radial forging comprises a multiple series of at least two and no more than six reductions at radial forging temperatures starting at no more than 1400° F. and decreasing to no less than 1000° F., with a reheat step prior to each reduction.

15. The method according to claim 1 , further comprising:
prior to forging the titanium alloy at the first forging temperature, beta heat treating the alpha-beta titanium alloy at a beta heat treating temperature,
wherein the beta heat treating temperature is from a beta transus temperature of the alpha-beta titanium alloy to a temperature 300° F. greater than the beta transus temperature of the alpha-beta titanium alloy; and
quenching the alpha-beta titanium alloy.

16. The method according to claim 15 , wherein beta heat treating the alpha-beta titanium alloy further comprises working the alpha-beta titanium alloy at the beta heat treating temperature.

17. The method according to claim 16 , wherein working the alpha-beta titanium alloy at the beta heat treating temperature comprises one or more of roll forging, swaging, cogging, open-die forging, impression-die forging, press forging, automatic hot forging, radial forging, upset forging, draw forging, and multiaxis forging.

Assignees

• Ati Properties Llc

Inventors

• Thomas Jean-Phillippe A
• Minisandram Ramesh S
• Forbes Jones Robin M
• Mantione John V
• Bryan David J

Classifications

• C22F1/183 Primary

  of titanium or alloys based thereon · CPC title

• C22C14/00

  Alloys based on titanium · CPC title

• C22F1/18

  High-melting or refractory metals or alloys based thereon · CPC title

• B21J5/00 Primary

  Methods for forging, hammering, or pressing (for working sheet-metal or metal tubes, rods, or profiles B21D; for working wire B21F); Special equipment or accessories therefor · CPC title