Sulfuric acid adding facility and operation method therefor

Patent metadata

Field	Value
Publication number	US-10351929-B2
Application number	US-201615549831-A
Country	US
Kind code	B2
Filing date	Feb 8, 2016
Priority date	Feb 12, 2015
Publication date	Jul 16, 2019
Grant date	Jul 16, 2019

Abstract

Provided are a sulfuric acid adding facility and an operation method therefor which enable an increase in the maximum capacity and the operation rate of a sulfuric acid supply pump provided in the sulfuric acid adding facility. In a sulfuric acid adding facility, sulfuric acid is added to an autoclave used in a leaching step of a high pressure acid leaching method for a nickel oxide ore. The sulfuric acid adding facility is provided with the same number (n+1) (n is an integer, at least 1) of each of the following: a plurality of sulfuric acid adding pipes for adding sulfuric acid into the autoclave; and a plurality of sulfuric acid supply pumps for supplying sulfuric acid to the sulfuric acid adding pipes. Each of the first through n+1th sulfuric acid supply pumps includes at least three diaphragms and discharge ports of the same number as that of the diaphragms.

First claim

The invention claimed is:

1. A sulfuric acid adding facility for adding sulfuric acid to an autoclave used in a leaching step in a high pressure nickel oxide ore acid leaching method, the facility comprising:
a plurality of sulfuric acid addition pipes for adding sulfuric acid into the autoclave and
a plurality of sulfuric acid supply pumps that are connected to the sulfuric acid addition pipes and supply sulfuric acid to the sulfuric acid addition pipes, wherein
the number of sulfuric acid addition pipes and sulfuric acid supply pumps is the same and is two or more;
each sulfuric acid supply pump includes three or more diaphragms and the same number of discharge ports as the number of the diaphragms, wherein:
more than half of the discharge ports of a kth sulfuric acid supply pump are
connected to a corresponding (kth) sulfuric acid addition pipe, wherein “kth” represents one of the two or more sulfuric acid supply pumps, and
the remaining discharge ports of the kth sulfuric acid supply pump are connected to sulfuric acid addition pipes other than the kth sulfuric acid addition pipe, and
the sulfuric acid addition pipes to which the remaining discharge ports are connected to the discharge ports of diaphragms of sulfuric acid supply pumps other than the kth sulfuric acid supply pump so as not to overlap with the sulfuric acid addition pipes to which the remaining discharge ports are connected.

2. A method for operating a sulfuric acid adding facility for adding sulfuric acid to an autoclave used in a leaching step in a high pressure nickel oxide ore acid leaching method, wherein
the sulfuric acid adding facility includes:
a plurality of sulfuric acid addition pipes for adding sulfuric acid into the autoclave and
a plurality of sulfuric acid supply pumps that are connected to the sulfuric acid addition pipes and supply sulfuric acid to the sulfuric acid addition pipes, wherein
the number of sulfuric acid addition pipes and sulfuric acid supply pumps is the same and is two or more;
each sulfuric acid supply pump includes three or more diaphragms and the same number of discharge ports as the number of the diaphragms, wherein:
more than half of the discharge ports of a kth sulfuric acid supply pump are
connected to a corresponding (kth) sulfuric acid addition pipe, wherein “kth” represents one of the two or more sulfuric acid supply pumps, and
the remaining discharge ports of the kth sulfuric acid supply pump are connected to sulfuric acid addition pipes other than the kth sulfuric acid addition pipe, and
the sulfuric acid addition pipes to which the remaining discharge ports are connected to the discharge ports of diaphragms of sulfuric acid supply pumps other than the kth sulfuric acid supply pump so as not to overlap with the sulfuric acid addition pipes to which the remaining discharge ports are connected;

wherein the method of operation comprises, at the time of normal operation of the sulfuric acid adding facility,
an operating step wherein more than half of the three or more diaphragms are operated and the remaining-diaphragms are stopped at each of the sulfuric acid supply pumps, and
an adding step wherein sulfuric acid is added into the autoclave by discharging sulfuric acid from a discharge port of an operated diaphragm via the corresponding sulfuric acid addition pipe.

3. The method for operating a sulfuric acid adding facility according to claim 2 , wherein
the sulfuric acid adding facility includes two sulfuric acid addition pipes and two sulfuric acid supply pumps,
and, at the time when operation of any one of the sulfuric acid supply pumps is to be stopped,
the method comprises a stopping step wherein a kth sulfuric acid supply pump is put in a stopped state by stopping the operated diaphragms of the kth sulfuric acid supply pump, and
an opening step wherein, in the sulfuric acid supply pumps other than the kth sulfuric acid supply pump, the remaining stopped diaphragms are operated and sulfuric acid is added into the autoclave via a sulfuric acid addition pipe to which the remaining discharge ports of are connected.

Assignees

• Sumitomo Metal Mining Co

Inventors

• Sakamoto Takashi
• Nakai Osamu
• Oku Masayuki
• Sato Hideaki
• Shirai Sho

Classifications

• C22B3/08

  Sulfuric acid {, other sulfurated acids or salts thereof} · CPC title

• C22B3/02 Primary

  Apparatus therefor · CPC title

• C22B23/043

  Sulfurated acids or salts thereof · CPC title

• Y02P10/234

  Cross-Sectional Technologies · mapped topic

• Y02P10/20

  Recycling · CPC title