Powder, process of making the powder, and articles made therefrom
US-2017137313-A1 · May 18, 2017 · US
US10351459B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10351459-B2 |
| Application number | US-201615234114-A |
| Country | US |
| Kind code | B2 |
| Filing date | Aug 11, 2016 |
| Priority date | Aug 14, 2015 |
| Publication date | Jul 16, 2019 |
| Grant date | Jul 16, 2019 |
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A method for treating a mold includes grinding an outer metal surface of a mold body of the mold with a first material; lapping the outer metal surface after the grinding with a second material that is finer than the first material; and polishing the outer metal surface after the lapping to achieve an average surface roughness (R a ) less than or equal to about 0.15 μm and a waviness height (W a ) less than or equal to about 100 nm. A mold for shaping glass-based material can include a mold body having an outer metal surface, wherein the outer metal surface has an average surface roughness (R a ) less than or equal to about 0.15 μm and a waviness height (W a ) less than or equal to about 100 nm.
Opening claim text (preview).
We claim: 1. A mold comprising: a mold body having a metal surface; and a metal oxide layer on the metal surface of the mold body, wherein: the metal oxide layer has first and second opposing surfaces, the first surface of the metal oxide layer contacts and faces the metal surface of the mold body, the second surface of the metal oxide layer includes a plurality of grains, and the plurality of grains has an average grain size of about 300 μm or less. 2. The mold of claim 1 , wherein the second surface includes at least one grain body area and at least one grain boundary area and wherein an average height differential between the at least one grain body area and the at least one grain boundary area is about 2 μm or less. 3. The mold of claim 2 , wherein the average height differential is about 1 μm or less. 4. The mold of claim 1 , wherein the average grain size is about 150 μm or less. 5. The mold of claim 1 , wherein the second surface of the metal oxide layer has a waviness (Wa) of less than or equal to about 500 nm. 6. The mold of claim 5 , wherein the second surface of the metal oxide layer has a waviness (Wa) of less than or equal to about 100 nm. 7. The mold of claim 1 , wherein the second surface of the metal oxide layer has an average surface roughness (Ra) of about 1 μm or less. 8. The mold of claim 7 , wherein the second surface of the metal oxide layer has an average surface roughness (Ra) of about 0.4 μm or less. 9. The mold of claim 8 , wherein the second surface of the metal oxide layer has an average surface roughness (Ra) in a range from about 0.2 μm to about 0.4 μm. 10. The mold of claim 1 , wherein the second surface of the metal oxide layer has a waviness (Wa) of less than or equal to about 500 nm and an average surface roughness (Ra) of about 1 μm or less. 11. The mold of claim 1 , wherein the second surface of the metal oxide layer has a waviness (Wa) of less than or equal to about 500 nm and an average surface roughness (Ra) in a range from about 0.2 μm to about 0.4 μm. 12. The mold of claim 1 , wherein a ratio of an R volume below the surface of the metal oxide layer divided by the R volume above the surface of the metal oxide layer is less than or equal to 2. 13. The mold of claim 1 , wherein the mold body comprises: at least 90% nickel by weight; and at least one of titanium, aluminum, zirconium, silicon, manganese, or cerium, wherein a sum of a weight percent of titanium, aluminum, zirconium, silicon, manganese and cerium is in a range from about 0.6% to about 1%. 14. The mold of claim 13 , wherein the mold body comprises at least 99% nickel by weight. 15. The mold of claim 13 , wherein the metal oxide layer is nickel oxide.
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