Portable NMR device for detecting an oil concentration in water

Patent metadata

Field	Value
Publication number	US-10345251-B2
Application number	US-201715440606-A
Country	US
Kind code	B2
Filing date	Feb 23, 2017
Priority date	Feb 23, 2017
Publication date	Jul 9, 2019
Grant date	Jul 9, 2019

Abstract

A portable nuclear magnetic resonance (NMR) device and a method of determining an oil concentration in water are disclosed. The portable NMR device can include a magnetic field assembly to carry out NMR measurements of water. The portable NMR device can include a housing to at least partly surround the magnetic field assembly and to substantially eliminate a magnetic fringe field generated by the magnetic field assembly outside the housing. The portable NMR device can also include an analysis module to receive the NMR measurement of the water and to determine, based on the received NMR measurements of the water, the oil concentration in the water.

First claim

The invention claimed is:

1. A portable nuclear magnetic resonance (NMR) device configured for detecting an oil concentration in water, the portable NMR device comprising:
a magnetic field assembly comprising at least one magnet and
at least one radiofrequency (RF) coil;
wherein the magnetic field assembly generates a magnetic field that is utilized in carrying out NMR measurements on water that passes through the portable NMR device; and
wherein the NMR measurements enable a detection of an oil in the water, when the oil concentration in the water is at least 50 parts per million (ppm);
a housing partly surrounding the magnetic field assembly that substantially eliminates a magnetic fringe field generated by the magnetic field assembly from extending beyond the outside of the housing; and
an analysis module that is configured in order to receive the carried out NMR measurements that are performed on the water and the analysis module being configured to determine, based on the received NMR measurements that are carried out on the water that passes through the portable NMR device, the oil concentration that is present in the water.

2. The portable NMR device of claim 1 , wherein the magnetic field assembly connects and attaches to an oil cleaning system via coupling.

3. The portable NMR device of claim 2 , wherein the magnetic field assembly is utilized in order to carry out NMR measurements on the water that is exiting the oil cleaning system which had been connected and attached via said coupling to the magnetic field assembly.

4. The portable NMR device of claim 3 , wherein the analysis module determines based on the received NMR measurements, the oil concentration in the water exiting the oil cleaning system.

5. The portable NMR device of claim 2 , wherein the magnetic field assembly is further configured to carry out NMR measurements on, and detect at least one contaminant within the water that is exiting the oil cleaning system which is connected and attached via said coupling to the magnetic field assembly.

6. The portable NMR device of claim 5 , wherein the analysis modulus is further configured to determine, based on the carried out NMR measurements that are received by the analysis module, a concentration of the at least one oil contaminant, that was detected in the water exiting the oil cleaning system and wherein the analysis module is also utilized to indicate, based on the determined concentration of the at least one oil contaminant, an amount of oil cleanliness.

7. The portable NMR device of claim 2 , wherein the magnetic field assembly is further configured to carry out NMR measurements on, and detect, by performing a first and second detection, at least one contaminant within, the water that is exiting the oil cleaning system which is connected and attached via said coupling to the magnetic field assembly.

8. The portable NMR device of claim 7 , wherein the analysis modulus is further configured to compare, based on the carried out NMR measurements that are received by the analysis module, the first and second detections of the at least one contaminant and to subsequently determine, based on the comparison, an indication of oil cleanliness by using a lack of difference between the first and second detections as the indication of oil cleanliness.

9. A method of detecting an oil concentration in water, the method comprising:
generating with a portable nuclear magnetic resonance (NMR) device, containing at least one magnetic field source a magnetic field within a measurement volume in order to enable an on-line and in-line detection of an oil concentration in water that passes through the portable NMR device, when the oil concentration in the water is at least 50 parts per million (ppm);
carrying out nuclear magnetic resonance (NMR) measurements on the water in order to detect the oil concentration in the water with the portable NMR device;
determining via an analysis based on the carried out and obtained NMR measurements, that is performed by and with a computer processor of the portable NMR device, a measurement of the oil concentration in the water; and
shielding an environment external to the measurement volume of the portable NMR device in order to substantially eliminate a magnetic fringe field from extending beyond an outer housing of the portable NMR device.

10. The method of claim 9 , further comprising generating with the portable nuclear magnetic resonance (NMR) device, contained the at least one magnetic field source a magnetic field in order to enable a detection of at least one oil contaminant in the water that passes through the portable NMR device.

11. The method of claim 10 , further comprising carrying out NMR measurements with the portable nuclear magnetic resonance device (NMR) device, containing the at least one magnetic field source in order to carry our the actual detection of the at least one oil contaminant in the water.

12. The method of claim 11 , further comprising determining via the analysis performed by with a computer processor, based on the carried out and obtained NMR measurements, the determined concentration of the at least one oil contaminant that was detected in the water.

13. The method of claim 12 , further comprising based on the determined concentration indicating, with the computer processor of the portable nuclear magnetic resonance (NMR) device that performs the analysis of the at least one oil contaminant in the water that passes through the portable NMR device, and subsequently providing as a result an indication of an amount of oil cleanliness within the water that passes through the portable NMR device.

Assignees

• Aspect Imaging Ltd

Inventors

• Rapoport Uri

Classifications

• G01N33/18

  Water · CPC title

• G01N24/082 Primary

  Measurement of solid, liquid or gas content · CPC title

• G01R33/307

  specially adapted for moving the sample relative to the MR system, e.g. spinning mechanisms, flow cells or means for positioning the sample inside a spectrometer · CPC title

• G01R33/421

  of main or gradient magnetic field · CPC title

• G01N33/1833

  Oil in water · CPC title