Ceramic matrix composite articles formation method

Patent metadata

Field	Value
Publication number	US-10329201-B2
Application number	US-201715710965-A
Country	US
Kind code	B2
Filing date	Sep 21, 2017
Priority date	Sep 21, 2017
Publication date	Jun 25, 2019
Grant date	Jun 25, 2019

Abstract

A method for forming a ceramic matrix composite article includes laying up a first group of plies; laying up a second group of plies, the first and second groups of plies being adjacent to each other; compacting the first group of plies and the second group of plies in the same processing step; and performing a first infiltration process on the first group of plies. The method also includes performing a second infiltration process on the second group of plies, the first infiltration process being one of a melt infiltration process or a chemical vapor infiltration process, and the second infiltration process being the other of the melt infiltration process or the chemical vapor infiltration process.

First claim

What is claimed is:

1. A method for forming a ceramic matrix composite article comprising:
laying up a first group of plies;
laying up a second group of plies, the first and second groups of plies being adjacent to each other;
compacting the first group of plies and the second group of plies in the same processing step;
performing a first infiltration process on the first group of plies subsequent to compacting the first group of plies and the second group of plies in the same processing step; and
performing a second infiltration process on the second group of plies subsequent to compacting the first group of plies and the second group of plies in the same processing step, the first infiltration process being one of a melt infiltration process or a chemical vapor infiltration process, and the second infiltration process being the other of the melt infiltration process or the chemical vapor infiltration process.

2. The method of claim 1 , wherein the first infiltration process is the melt infiltration process, wherein the second infiltration process is the chemical vapor infiltration process, and wherein performing the first infiltration process on the first group of plies comprises performing the first infiltration process on the first group of plies prior to performing the second infiltration process on the second group of plies.

3. The method of claim 2 , further comprising:
providing a barrier between a least a portion of the first group of plies and the second group of plies.

4. The method of claim 2 , wherein performing the first infiltration process on the first group of plies comprises performing the melt infiltration process substantially solely on the first group of plies.

5. The method of claim 1 , wherein the first infiltration process is the melt infiltration process, wherein the second infiltration process is the chemical vapor infiltration process, and wherein performing the second infiltration process on the second group of plies comprises performing the second infiltration process on the second group of plies prior to performing the first infiltration process on the first group of plies.

6. The method of claim 5 , wherein performing the second infiltration process on the second group of plies comprises covering, at least in part, the first group of plies prior to performing the chemical vapor infiltration process on the second group of plies.

7. The method of claim 1 , wherein compacting the first group of plies and the second group of plies in the same processing step comprises exposing the first and second groups of plies to temperatures between about 200 degrees Celsius and about 400 degrees Celsius and to pressures between about 100 pounds per square inch (psi) and about 300 psi.

8. The method of claim 1 , further comprising:
forming the first group of plies, wherein forming the first group of plies comprises passing a first group of tows through a first slurry; and
forming the second group of plies, wherein forming the second group of plies comprises passing a second group of tows through a second slurry, wherein the first slurry is different than the second slurry.

9. The method of claim 8 , wherein the first slurry and second slurry each contain a resin, and wherein the resin has a glass transition temperature between about 100 degrees Celsius and about 300 degrees Celsius.

10. The method of claim 9 , wherein the preform has char yield between about 10% and about 20%.

11. The method of claim 8 , wherein the first slurry includes between about ten (10) and about twenty (20) volume percent of carbon powder added thereto and between about ten (10) and about twenty (20) volume percent of SiC powder added thereto, and wherein the second slurry includes between about five (5) and about twenty (20) volume percent of SiC powder added thereto and less than about five (5) volume percent of carbon powder added thereto.

12. The method of claim 11 , wherein the second resin defines a glass transition temperature within about ten percent of a glass transition temperature defined by the first resin.

13. The method of claim 8 , wherein the first infiltration process is the melt infiltration process, and wherein the first slurry includes a carbon powder added thereto.

14. The method of claim 1 , further comprising:
pyrolyzing the first group of plies and the second group of plies in the same processing step subsequent to compacting the first group of plies and the second group of plies in the same processing step.

15. The method of claim 14 , wherein the first group of plies and the second group of plies together form a preform, and wherein the preform has char yield less than about 30% subsequent to pyrolyzing the first group of plies and the second group of plies.

16. A method for forming a ceramic matrix composite article comprising:
laying up a first group of plies;
laying up a second group of plies, the first and second groups of plies being adjacent to each other;
compacting the first group of plies and the second group of plies;
pyrolyzing the first group of plies and the second of plies in the same processing step;
performing a first infiltration process on the first group of plies subsequent to pyrolyzing the first group of plies and the second of plies in the same processing step; and
performing a second infiltration process on the second group of plies subsequent to pyrolyzing the first group of plies and the second of plies in the same processing step, the first infiltration process being one of a melt infiltration process or a chemical vapor infiltration process, and the second infiltration process being the other of the melt infiltration process or the chemical vapor infiltration process.

17. The method of claim 16 , wherein pyrolyzing the first group of plies and the second of plies in the same processing step comprises pyrolyzing the first group of plies and the second of plies in the same processing step subsequent to compacting the first group of plies and the second group of plies.

18. The method of claim 16 , wherein compacting the first group of plies and the second group of plies comprises compacting the first group of plies and the second group of plies in the same processing step.

19. The method of claim 16 , wherein the first infiltration process is the melt infiltration process, wherein the second infiltration process is the chemical vapor infiltration process, and wherein performing the first infiltration process on the first group of plies comprises performing the first infiltration process on the first group of plies prior to performing the second infiltration process on the second group of plies.

20. The method of claim 16 , wherein the first infiltration process is the melt infiltration process, wherein the second infiltration process is the chemical vapor infiltration process, and wherein performing the second infiltration process on the second group of plies comprises performing the second infiltration process on the second group of plies prior to performing the first infiltration process on the first group of plies.

Assignees

• Gen Electric

Inventors

• Steibel James Dale
• Subramanian Suresh
• Viswanathan Suresh
• Weaver Jared Hogg

Classifications

• B32B18/00 Primary

  Layered products essentially comprising ceramics, e.g. refractory products · CPC title

• B32B7/02

  Physical, chemical or physicochemical properties · CPC title

• C04B2235/3826

  Silicon carbides · CPC title

• C04B2235/422

  Carbon · CPC title

• C04B35/6267

  Pyrolysis, carbonisation or auto-combustion reactions · CPC title