Process for the production of solid cooling agents

Patent metadata

Field	Value
Publication number	US-10328405-B2
Application number	US-201515329457-A
Country	US
Kind code	B2
Filing date	Jul 26, 2015
Priority date	Jul 29, 2014
Publication date	Jun 25, 2019
Grant date	Jun 25, 2019

Abstract

Suggested is a process for the production of solid cooling agents, wherein a pre-scraped melt, i.e., a melt of menthol compounds with added seed crystals is applied to a pre-cooled area by even deposition of drops.

First claim

The invention claimed is:

1. A process for the production of a menthol pastille with a curved side and a flat side, comprising the step of:
placing a pre-scraped melt of menthol compounds with added seed crystals of L-menthol onto a pre-cooled single steel belt by even deposition of drops, and wherein the steel belt has cooling zones independently of one another each having a temperature below the respective melting point of said L-menthol seed crystals in the range of from about 15 to about 42° C.

2. The process of claim 1 , wherein seed crystals are used which were formed by treatment of the melt to be used in a scraped surface heat exchanger.

3. The process of claim 1 , wherein the menthol compounds are selected from the group consisting of Menthol, Racemic Menthol, Menthol Methyl Ether, Menthone Glyceryl Acetal (FEMA GRAS 3807), Menthone Glyceryl Ketal (FEMA GRAS 3808), Menthyl Lactate (FEMA GRAS 3748), Menthol Ethylene Glycol Carbonate (FEMA GRAS 3805), Menthol Propylene Glycol Carbonate (FEMA GRAS 3806), Menthyl-N-ethyloxamate, Monomethyl Succinate (FEMA GRAS 3810), Monomenthyl Glutamate (FEMA GRAS 4006), Menthoxy-1,2-propanediol (FEMA GRAS 3784), Menthoxy-2-methyl-1,2-propanediol (FEMA GRAS 3849) and the menthane carboxylic acid esters and amides WS-3, WS-4, WS-5, WS-12, WS-14 and WS-30 and mixtures thereof.

4. The process of claim 1 , wherein the pre-scraped melt of menthol compounds has a temperature in the range of from about 40 to about 60° C.

5. The process of claim 1 , wherein the pre-scraped melt contains from about 0.1 to 12 wt. % seed crystals.

6. The process of claim 5 , wherein the pre-scraped melt contains from about 0.1 to about 12 wt. % seed crystals of L-menthol.

7. The process of claim 1 , wherein the step of placing a pre-scraped melt of menthol compounds with added seed crystals of L-menthol onto a pre-cooled single steel belt occurs by even deposition of drops from a rotoformer.

Assignees

• Symrise Ag

Inventors

• Siewert Jürgen
• Michler Michael
• Niekerken Jörg
• Lenz Oliver
• Wolter Christian

Classifications

• B29B9/10

  by moulding the material, i.e. treating it in the molten state · CPC title

• B01J2/26 Primary

  on endless conveyor belts · CPC title

• A61K9/2013

  Organic compounds, e.g. phospholipids, fats · CPC title

• A61K47/12 Primary

  Carboxylic acids; Salts or anhydrides thereof · CPC title

• C07C29/78

  by condensation or crystallisation · CPC title