Reducing microtexture in titanium alloys

Patent metadata

Field	Value
Publication number	US-10323312-B2
Application number	US-201514964180-A
Country	US
Kind code	B2
Filing date	Dec 9, 2015
Priority date	Dec 10, 2014
Publication date	Jun 18, 2019
Grant date	Jun 18, 2019

Abstract

A method includes heating an initial titanium alloy comprising a duplex microstructure at a first solution temperature that is below a phase transition temperature of the alloy. Substantially all secondary alpha phase domains may dissolve during the heating. The method also includes cooling the initial titanium alloy at a first cooling rate to form a recrystallized annealed titanium alloy comprising primary alpha phase domains. The method further includes heating the recrystallized annealed titanium alloy to a second solution temperature that is below the phase transition temperature of the alloy. The method additionally includes cooling the recrystallized annealed titanium alloy at a second cooling rate to form a treated titanium alloy comprising the duplex microstructure. The second cooling rate is different than the first cooling rate. A distribution of crystallographic orientations of primary alpha phase domains in the treated titanium alloy may be different than in the initial titanium alloy.

First claim

The invention claimed is:

1. A method comprising:
heating, at a first solution temperature, an initial titanium alloy comprising a duplex microstructure comprising primary alpha phase domains and secondary alpha phase domains, wherein the duplex microstructure includes a first volume fraction of primary alpha phase domains and a second volume fraction of secondary alpha phase domains, wherein the first solution temperature is below a phase transition temperature of the initial titanium alloy, and wherein substantially all of the secondary alpha phase domains dissolve during the heating at the first solution temperature;
cooling the initial titanium alloy at a first cooling rate to form a recrystallized annealed titanium alloy comprising substantially only primary alpha phase domains;
heating the recrystallized annealed titanium alloy at a second solution temperature, wherein the second solution temperature is below the phase transition temperature of the recrystallized annealed titanium alloy; and
cooling the recrystallized annealed titanium alloy at a second cooling rate to form a treated titanium alloy comprising the duplex microstructure comprising primary alpha phase domains and secondary alpha phase domains, wherein the treated titanium alloy comprises a third volume fraction of primary alpha phase domains and a fourth volume fraction of secondary alpha phase domains, wherein the second cooling rate is different than the first cooling rate, and wherein a distribution of crystallographic orientations of the primary alpha phase domains in the treated titanium alloy is different than a distribution of crystallographic orientations of the primary alpha phase domains in the initial titanium alloy.

2. The method of claim 1 , wherein the first volume fraction and the third volume fraction are different.

3. The method of claim 1 wherein an average size of the primary alpha phase domains in the treated titanium alloy is different than an average size of the primary alpha phase domains in the initial titanium alloy.

4. The method of claim 1 , wherein an average width of the secondary alpha phase domains in the treated titanium alloy is different than an average width of the secondary alpha phase domains in the initial titanium alloy.

5. The method of claim 1 , wherein the phase transition temperature comprises a beta transus transition temperature.

6. The method of claim 5 , wherein the first solution temperature and the second solution temperature are between about 30° C. and about 50° C. below the beta transus transition temperature.

7. The method of claim 1 , wherein cooling the initial titanium alloy at a first cooling rate to form the recrystallized annealed titanium alloy comprising substantially only primary alpha phase domains comprises turning off a furnace in which the initial titanium alloy was heated and allowing the initial titanium alloy to cool in the furnace.

8. The method of claim 1 , wherein cooling the recrystallized annealed titanium alloy at the second cooling rate comprises quenching the recrystallized annealed titanium alloy in a cooling medium.

9. The method of claim 8 , wherein the cooling medium comprises water.

10. The method of claim 1 , wherein an average microtexture region volume in the initial alloy is larger than an average microtexture region volume in the treated alloy.

11. The method of claim 1 , wherein the first cooling rate is greater than the second cooling rate.

12. The method of claim 1 , wherein the second cooling rate is greater than the first cooling rate.

Assignees

• Rolls Royce Corp

Inventors

• Glavicic Michael George

Classifications

• C22F1/183 Primary

  of titanium or alloys based thereon · CPC title

• C22F1/002

  by rapid cooling or quenching; cooling agents used therefor · CPC title

• C22C14/00

  Alloys based on titanium · CPC title