Rapid curing of thin composite material sections

Patent metadata

Field	Value
Publication number	US-10315335-B2
Application number	US-201414295402-A
Country	US
Kind code	B2
Filing date	Jun 4, 2014
Priority date	Jun 7, 2013
Publication date	Jun 11, 2019
Grant date	Jun 11, 2019

Abstract

A method of preparing and rapidly curing a composite material having a thin cross section. The composite material includes a mixture of solid particles, at least some of which are a material that reacts with CO2, such as a silicate, for example Wollastonite. The green material is prepared by mixing the solid components with a liquid such as water to form a slurry, and forming green bodies by placing the slurry in forms. The green bodies are reacted with CO2 to form cured composite materials having thin sections, in the range of 10 to 15 mm. Curing in periods of 6 hours has been demonstrated.

First claim

What is claimed is:

1. A method of rapidly curing a thin composite material section, comprising the steps of:
forming a particulate composition comprising ground calcium silicate having a median particle size of about 1 μm to about 100 μm, and at least one of ground calcium carbonate or SiO 2 containing material having a median particle size of about 3 μm to about 25 mm;
forming a liquid composition comprising water and a water-soluble dispersant;
mixing the particulate composition and the liquid composition to form a slurry;
forming the slurry into a green body having a desired shape with a cross section in the range of 5 mm to 25 mm;
reacting the green body with CO 2 in a curing chamber under a pressure of about ambient atmospheric pressure to about 50 psi above ambient atmospheric pressure to produce a cured composite material.

2. The method of rapidly curing a thin composite material section of claim 1 , wherein said cross section is in the range of 11 mm to 14 mm.

3. The method of rapidly curing a thin composite material section of claim 1 , wherein said ground calcium silicate material is synthetic wollastonite.

4. The method of rapidly curing a thin composite material section of claim 1 , wherein the at least one of ground calcium carbonate or SiO 2 containing material is at least one of sand and flyash.

5. The method of rapidly curing a thin composite material section of claim 1 , wherein the step of forming the particulate composition further comprises mixing the ground calcium silicate material and the at least one of ground calcium carbonate or SiO 2 containing material with continuous or discontinuous fibers.

6. The method of rapidly curing a thin composite material section of claim 1 , further comprising the step of heating the cured composite material to drive off water.

7. The method of rapidly curing a thin composite material section of claim 1 , wherein said step of reacting the green body with CO 2 in a curing chamber is performed for 6 hours or less.

8. The method of rapidly curing a thin composite material section of claim 1 , wherein said step of reacting the green body with CO 2 in a curing chamber is performed at a temperature of 60° C.

9. The method of rapidly curing a thin composite material section of claim 1 , wherein the step of forming the slurry into the green body having desired shape comprising placing the slurry in a mold prior to the reacting step.

10. The method of rapidly curing a thin composite material section of claim 9 , wherein the step of placing the slurry in a mold further comprises applying vibration.

11. The method of rapidly curing a thin composite material section of claim 9 , wherein the step of placing the slurry in a mold further comprises pressing.

12. The method of rapidly curing a thin composite material section of claim 1 , wherein the step of forming the slurry into the green body having desired shape comprises extrusion.

13. The method of rapidly curing a thin composite material section of claim 1 , wherein said thin composite material has a length in the range of 55 to 220 mm.

14. The method of rapidly curing a thin composite material section of claim 1 , wherein said thin composite material has a width in the range of 55 to 220 mm.

15. The method of rapidly curing a thin composite material section of claim 1 , wherein said thin composite material comprises bonding elements having a mean particle size in the range of 5 to 50 micrometers.

16. The method of rapidly curing a thin composite material section of claim 1 , wherein said thin composite material comprises bonding elements having a mean particle size in the range of 5 to 25 micrometers.

Assignees

• Solidia Technologies Inc

Inventors

• Hu Xudong
• Ravikumar Deepak
• Patten Devin

Classifications

• C04B20/12

  Multiple coating or impregnating · CPC title

• C04B20/107

  Acids or salts thereof · CPC title

• B28B11/24 Primary

  for curing, setting or hardening (processes for influencing or modifying the setting or hardening ability of mortars, concrete or artificial stone compositions, in general C04B40/00) · CPC title

• B01J3/04

  Pressure vessels, e.g. autoclaves · CPC title

• C04B14/042

  Magnesium silicates, e.g. talc, sepiolite · CPC title