Microfluidic oscillating tube densitometer for downhole applications

Patent metadata

Field	Value
Publication number	US-10301938-B2
Application number	US-201514821318-A
Country	US
Kind code	B2
Filing date	Aug 7, 2015
Priority date	Apr 15, 2009
Publication date	May 28, 2019
Grant date	May 28, 2019

Abstract

Devices, methods and systems for determining one or more properties of at least one fluid sample. A tube configured to receive the at least one fluid sample wherein the tube is placed in a pressure housing. Further, an excitation source configured to generate vibration of the tube whereby a circulation of an electrical current along a portion of the tube is subjected to at least one magnetic field produced by at least one magnet. Further still, at least one vibration sensor that converts vibrations of the tube into a measurement signal. Finally, a processor that receives the measurement signal determines a resonant frequency from the measurement signal using a frequency measuring device to determine a property of the one or more properties of the at least one sample fluid.

First claim

What is claimed is:

1. A logging tool for determining a property of a fluid sample, the logging tool comprising:
a pressure housing;
a fluid sampling device comprising a probe configured to establish fluid communication with a formation and to draw the fluid sample into the logging tool; and
a device disposed within the pressure housing for determining a property of a fluid sample, the device comprising:
a tube in fluid communication with the fluid sampling device;
a filter configured to separate the fluid sample from aqueous mud filtrate prior to entry into the tube;
a current source configured to pass an electrical current along a portion of the tube;
at least one magnet configured to apply a magnetic field to the portion of the tube, wherein the magnetic field generates vibration within the tube when the electrical current passes along the portion of the tube, the tube surrounding the at least one magnet along an exterior of the least one magnet;
a sensor configured to generate a measurement signal by measuring an electromagnetic force voltage that is induced within the tube; and

a processor that receives the measurement signal and determines the property of the fluid sample using the measurement signal.

2. The logging tool of claim 1 , wherein the filter includes a microporous membrane that separates the fluid sample from aqueous mud filtrate.

3. A logging tool for determining a property of a fluid sample, the logging tool comprising:
a pressure housing;
a fluid sampling device comprising a probe configured to establish fluid communication with a formation and to draw the fluid sample into the logging tool; and
a device disposed within the pressure housing for determining a property of a fluid sample, the device comprising:
a tube in fluid communication with the fluid sampling device;
a filter configured to separate the fluid sample from aqueous mud filtrate prior to entry into the tube;
a current source configured to pass an electrical current along a portion of the tube, wherein the portion of the tube that passes the electrical current is electrically isolated from the fluid sampling device;
at least one magnet configured to apply a magnetic field to the portion of the tube, wherein the magnetic field generates vibration within the tube when the electrical current passes along the portion of the tube;
a sensor configured to generate a measurement signal by measuring an electromagnetic force voltage that is induced within the tube; and

a processor that receives the measurement signal and determines the property of the fluid sample using the measurement signal.

4. The device logging tool of claim 3 , further comprising:
at least one union for electrically isolating the portion of the tube that passes the electrical current from the fluid sampling device while maintaining fluid communication with the fluid sampling device.

5. The logging tool of claim 1 , wherein the tube comprises at least one bend.

6. The device logging tool of claim 1 , wherein the tube vibrates at a frequency characteristic of the property of the fluid sample.

7. The device logging tool of claim 1 , wherein the property of the fluid sample is density.

8. The device logging tool of claim 1 , wherein the fluid sample is less than 100 micro liters.

9. The logging tool of claim 1 , wherein the tube has a cavity with an internal cavity volume equal to or less than 1000 micro liters.

10. The logging tool of claim 1 , wherein the device determines the property of the fluid sample while the fluid sample is stationary within the tube.

11. The logging tool of claim 1 , wherein the logging tool comprises at least one of a sampling-while-drilling tool, a logging-while-drilling tool, and a wireline tool.

12. The logging tool of claim 1 , wherein an amplitude of the induced electromagnetic force voltage is equal to or less than 100 millivolts.

13. The logging tool of claim 12 , wherein the induced electro-magnetic force voltage is amplified by a factor of 100 to 1,000 before being processed by the processor.

14. The logging tool of claim 1 , wherein the processor determines the property of the fluid sample using a temperature measurement and a pressure measurement.

15. The logging tool of claim 14 , wherein the temperature measurement is at least one of: a temperature of the tube and a temperature of the fluid sample.

16. The logging tool of claim 14 , wherein the pressure measurement is at least one of: a pressure within the tube and a pressure of the fluid sample.

17. The logging tool of claim 1 , wherein each end of the tube is secured by a holding device that comprises a plurality of blocks and each end of the tube is clamped between the blocks.

18. The logging tool of claim 17 , wherein the holding device comprises an insulating material that insulates each end of the tube from the plurality of blocks.

19. The logging tool of claim 1 , wherein the tool is configured to operate at temperatures above 150 ° C. and at pressures above 15,000 pounds per square inch (psi).

20. A logging tool for determining density of a formation fluid, the logging tool comprising:
a pressure housing;
a fluid sampling device comprising a probe configured to establish fluid communication with a formation and to draw the formation fluid into the logging tool; and
a device disposed within the pressure housing for determining density of the formation fluid, the device comprising:
a tube in fluid communication with the fluid sampling device;
a microporous membrane that separates the formation fluid from aqueous mud filtrate prior to entry into the tube;
a current source configured to pass an electrical current along a portion of the tube, wherein the portion of the tube that passes the electrical current is electrically isolated from the fluid sampling device;
at least one magnet configured to apply a magnetic field to the portion of the tube, wherein the magnetic field generates vibration within the tube when the electrical current passes along the portion of the tube;
a sensor configured to generate a measurement signal by measuring an electromagnetic force voltage that is induced within the tube; and

a processor that receives the measurement signal and determines the density of the formation fluid using the measurement signal.

Assignees

• Schlumberger Technology Corp

Inventors

• Harrison Christopher
• Coleou Chloe
• Grant Bill
• Jundt Jacques

Classifications

• E21B49/08 Primary

  Obtaining fluid samples or testing fluids, in boreholes or wells · CPC title

• E21B2049/085

  Fixed Constructions · mapped topic

• G01N29/02

  Analysing fluids (using acoustic emission techniques G01N29/14 {; constructional or flow details for analysing fluids G01N29/222; optoacoustic fluid cells G01N29/2425}) · CPC title

• G01N9/002 Primary

  using variation of the resonant frequency of an element vibrating in contact with the material submitted to analysis (G01N9/34 takes precedence) · CPC title

• G01N27/74

  of fluids (G01N24/00 takes precedence) · CPC title