Multiple well elevated temperature column flow testing

Patent metadata

Field	Value
Publication number	US-10301928-B2
Application number	US-201415036627-A
Country	US
Kind code	B2
Filing date	Aug 20, 2014
Priority date	Mar 28, 2014
Publication date	May 28, 2019
Grant date	May 28, 2019

Abstract

A method of flow testing can include dispensing at least one solid material and at least one liquid into each of multiple wells in a filter plate, and then heating the filter plate with the solid material and liquid therein to an elevated temperature. A flow testing system can include a multiple well filter plate, each of the wells having disposed therein a selected combination of formation particles, a fracturing fluid and a liquid hydrocarbon, and a heating device that heats the filter plate to an elevated temperature.

First claim

What is claimed is:

1. A method of flow testing, comprising:
dispensing a solid material and a liquid into each well of a multiple well filter plate, wherein each liquid comprises hydrocarbons and a fracturing fluid composition and at least two wells of the multiple wells contain different fracturing fluid compositions;
heating the filter plate with the solid material and liquid therein to a first elevated temperature;
flowing each of the liquids through the filter plate via gravity, vacuum assistance, or centrifugation;
measuring at least one of a volume of each of the liquids flowed through the filter plate or a mass of each of the liquid flowed through the filter plate;
determining if hydrocarbons are present in any of the liquids flowed through the filter plate; and
selecting one of the fracturing fluid compositions for use in a subterranean well fracturing operation based on at least one of the presence of hydrocarbons in the liquids flowed through the filter plate, volume measurements of the liquids flowed through the filter plate, or mass measurements of the liquids flowed through the filter plate.

2. The method of claim 1 , further comprising heating the filter plate prior to the dispensing.

3. The method of claim 1 , further comprising heating the solid material prior to the dispensing.

4. The method of claim 3 , wherein the heating the solid material comprises heating the solid material to substantially the first elevated temperature.

5. The method of claim 1 , further comprising heating the liquids prior to the dispensing.

6. The method of claim 5 , wherein the heating the liquids comprises heating the liquids to substantially the first elevated temperature.

7. The method of claim 1 , further comprising heating the filter plate after flowing each of the liquids through the filter plate via gravity, vacuum assistance, or centrifugation.

8. The method of claim 7 , further comprising flowing at least one of the group consisting of formation water and potassium chloride solution through the solid material, after the solid material is dispensed into the wells and before the liquids are dispensed into the wells.

9. The method of claim 8 , further comprising heating the filter plate after the dispensing of each of the liquids.

10. The method of claim 9 , further comprising dispensing liquid hydrocarbon into the wells after the heating the filter plate after the dispensing of each of the liquids.

11. The method of claim 10 , further comprising heating the filter plate after the dispensing of the liquid hydrocarbon.

12. The method of claim 11 , wherein flowing each of the liquids through the filter plate via gravity, vacuum assistance, or centrifugation further comprises allowing the liquid hydrocarbon to flow from the filter plate, after the heating of the filter plate after the dispensing of the liquid hydrocarbon.

13. The method of claim 12 , wherein during the allowing the liquid hydrocarbon to flow from the filter plate, each of the liquids and the liquid hydrocarbon are at a second elevated temperature.

14. The method of claim 13 , wherein the first and second elevated temperatures are substantially equal.

15. A flow testing system, comprising:
a multiple well filter plate, each of the wells having disposed therein a selected combination of formation particles, fracturing fluids, and a liquid hydrocarbon, wherein at least two wells of the multiple well filter plate contain different fracturing fluids;
a collection plate, wherein the fracturing fluid composition and the liquid hydrocarbon flow from the filter plate to the collection plate, wherein the fracturing fluid composition and the liquid hydrocarbon flow from the filter plate to the collection plate via gravity, vacuum assistance, or centrifugation;
a detection device configured to determine if any hydrocarbons are present in the collection plate; and
a first heating device that heats the filter plate to an elevated temperature.

16. The system of claim 15 , further comprising a second heating device that heats at least one sample container.

17. The system of claim 16 , wherein the second heating device heats the sample container to substantially the same elevated temperature as the first heating device heats the filter plate.

18. The system of claim 16 , wherein the second heating device heats the fracturing fluid.

19. The system of claim 16 , wherein the second heating device heats the liquid hydrocarbon.

20. The system of claim 16 , wherein the second heating device heats the formation particles.

Assignees

• Halliburton Energy Serv Inc
• Halliburton Energy Services Inc

Inventors

• Burks Jody M
• Radhakrishnan Potty Ajish Sreeni
• Lu Zheng

Classifications

• G01N33/2823 Primary

  Raw oil, drilling fluid or polyphasic mixtures · CPC title

• G01N11/06

  by timing the outflow of a known quantity · CPC title

• E21B47/10 Primary

  Locating fluid leaks, intrusions or movements · CPC title