Separating impurities from a fluid stream using multiple co-current contactors

Patent metadata

Field	Value
Publication number	US-10300429-B2
Application number	US-201514948422-A
Country	US
Kind code	B2
Filing date	Nov 23, 2015
Priority date	Jan 9, 2015
Publication date	May 28, 2019
Grant date	May 28, 2019

Abstract

A method for decontaminating a contaminated fluid stream, comprising receiving the contaminated fluid stream, distributing the contaminated fluid stream substantially equally across a plurality of separation units sharing a unitary pressure boundary, receiving a solvent stream, and co-currently contacting the contaminated fluid stream with the solvent stream in the plurality of separation units.

First claim

What is claimed is:

1. An apparatus for decontaminating a contaminated fluid stream, comprising:
a vessel comprising:
a contaminated fluid stream inlet;
a decontaminated fluid stream outlet;
a solvent inlet;
a contaminated solvent stream outlet; and

a co-current contacting bundle disposed within the vessel, wherein the co-current contacting bundle comprises at least two substantially parallel separation units, and wherein each separation unit comprises:
a contacting section including an inlet section and a mass transfer section, the mass transfer section comprising a tubular body having a first end into which a contaminated fluid stream is directed, the inlet section including a nozzle situated at the first end of the tubular body and oriented to direct an atomized solvent stream, generated by the nozzle, into the tubular body such that the atomized solvent stream flows in the same direction as a direction of flow of the contaminated fluid stream, thereby forming a mixed stream, the tubular body arranged to permit absorption of contaminants in the contaminated fluid stream by the atomized solvent stream to generate a contaminated solvent stream and an at least partially decontaminated fluid stream; and
a separation section arranged to receive the contaminated solvent stream and the at least partially decontaminated fluid stream from the mass transfer section, the separation section configured to separate the contaminated solvent stream from the at least partially decontaminated fluid stream.

2. The apparatus of claim 1 , wherein at least one separation section comprises a vortex tube finder in gaseous communication with the fluid stream outlet.

3. The apparatus of claim 1 , wherein a plurality of the separation sections each comprise a contaminated solvent outlet orifice, wherein the vessel comprises a common contaminated solvent collection plenum in fluid communication with the contaminated solvent outlet orifices, and wherein the common contaminated solvent collection plenum is in fluid communication with the contaminated solvent stream outlet.

4. The apparatus of claim 3 , wherein the vessel further comprises a demisting section disposed within the common contaminated solvent collection plenum.

5. The apparatus of claim 1 , further comprising:
a second co-current contacting bundle disposed within the vessel, wherein the second co-current contacting bundle comprises at least two secondary separation units, wherein the second co-current contacting bundle is in-line with the first co-current contacting bundle, and wherein each secondary separation unit comprises:
a second contacting section including a second inlet section and a second mass transfer section downstream of the second inlet section; and
a second separation section downstream of the second mass transfer section.

6. The apparatus of claim 1 , wherein at least one separation unit comprises a coalescing element disposed in the tubular body upstream of the separation section, the coalescing element configured to coalesce droplets of the contaminated solvent stream.

7. The apparatus of claim 1 , wherein each separation unit is between about 2 inches (about 5 centimeters) and about 24 inches (about 61 centimeters) in diameter.

8. The apparatus of claim 1 , further comprising an anti-swirl element disposed in the tubular body downstream of the separation section, the anti-swirl element configured to reduce swirl of the at least partially contaminated fluid stream.

9. The apparatus of claim 1 , further comprising a vortex breaker in the solvent stream outlet.

10. The apparatus of claim 1 , wherein at least one of the separation units includes an outlet section through which the contaminated solvent stream and the at least partially decontaminated fluid stream exit the separation unit separately, the outlet section having a liquid boot that collects the contaminated solvent stream, the separation unit further comprising:
a recycle gas inlet disposed in the separation section and connected to a portion of the liquid boot where gas remaining in the contaminated solvent stream is separated therefrom, the recycle gas inlet configured to direct gas in the liquid boot back to the separation section.

Assignees

• Grave Edward J
• Yeh Norman K
• Freeman Stephanie A
• Exxonmobil Upstream Res Co

Inventors

• Grave Edward J
• Yeh Norman K
• Freeman Stephanie A

Classifications

• B01D2252/204

  Amines · CPC title

• B01D53/1468

  Removing hydrogen sulfide · CPC title

• B01D53/1462 Primary

  Removing mixtures of hydrogen sulfide and carbon dioxide · CPC title

• B01D2257/308

  Carbonoxysulfide COS · CPC title

• B01D2257/306

  Organic sulfur compounds, e.g. mercaptans · CPC title