Doped-carbon composites, synthesizing methods and applications of the same

Patent metadata

Field	Value
Publication number	US-10293329-B2
Application number	US-201715474281-A
Country	US
Kind code	B2
Filing date	Mar 30, 2017
Priority date	Jun 18, 2008
Publication date	May 21, 2019
Grant date	May 21, 2019

Abstract

A method of synthesizing a doped carbon composite includes preparing a solution having a carbon source material and a heteroatom containing additive, evaporating the solution to yield a plurality of powders, and subjecting the plurality of powders to a heat treatment for a duration of time effective to produce the doped carbon composite.

First claim

What is claimed is:

1. A method of synthesizing a doped carbon composite, comprising the steps of:
(a) preparing a solution having a material containing tannin and a non-metallic additive containing a doping chemical element;
(b) evaporating the solution to yield a plurality of powders; and
(c) subjecting the plurality of powders to a heat treatment for a duration of time effective to produce the doped carbon composite,
wherein no metal source material is used in the method, such that the doped carbon composite does not contain metal component.

2. The method of claim 1 , wherein the material containing the tannin is tannin sulfonate, lignin, lignosulfonate, or a mixture thereof.

3. The method of claim 1 , wherein the non-metallic additive containing the doping chemical element is one containing oxygen (O), nitrogen (N), phosphorus (P), boron (B), sulfur (S), iodine (I), fluorine (F), or a mixture thereof.

4. The method of claim 1 , wherein the heat treatment is performed at a temperature in a range of about 700° C. to about 1800° C.

5. The method of claim 4 , wherein the duration of time effective is in a range of about 10 minutes to about 2 hours.

6. The method of claim 1 , wherein the heat treatment is performed by subjecting the plurality of powders to a microwave radiation with a frequency of 2.45 GHz.

7. The method of claim 1 , wherein the heat treatment is performed by a heat source other than a microwave radiation source.

8. The method of claim 1 , further comprising the step of adding polyphosphoric acid to the plurality of powders prior to the subjecting step.

Assignees

• Univ Arkansas

Inventors

• Viswanathan Tito

Classifications

• C25B1/003

  Chemistry & Metallurgy · mapped topic

• C02F2101/30

  Organic compounds · CPC title

• B01J37/0236

  Drying, e.g. preparing a suspension, adding a soluble salt and drying · CPC title

• B01J27/24 Primary

  Nitrogen compounds · CPC title

• B01J21/18 Primary

  Carbon · CPC title