Calibration of analytical instrument
US-2024393301-A1 · Nov 28, 2024 · US
US10283339B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10283339-B2 |
| Application number | US-201515518408-A |
| Country | US |
| Kind code | B2 |
| Filing date | Oct 7, 2015 |
| Priority date | Oct 29, 2014 |
| Publication date | May 7, 2019 |
| Grant date | May 7, 2019 |
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The present invention relates to a particle beam mass spectrometer and particle measurement method by means of same. More particularly, the present invention relates to a particle beam mass spectrometer including: a particle focusing unit focusing a particle beam induced by gas flow; an electron gun forming a charged particle beam by accelerating thermal electrons to ionize the particle beam focused by the particle focusing unit; a deflector deflecting the charged particle beam according to kinetic energy to charge ratio; and a sensing unit measuring a current induced by the deflected charged particle beam, wherein the deflector includes at least one particle beam separation electrode provided at each of opposite sides with respect to a progress axis of the charged particle beam before being deflected.
Opening claim text (preview).
The invention claimed is: 1. A particle beam mass spectrometer comprising: a particle focusing unit focusing a particle beam induced by gas flow; an electron gun forming a charged particle beam including a positive ion or a negative ion by accelerating thermal electrons to ionize the particle beam focused by the particle focusing unit; a deflector deflecting the charged particle beam according to kinetic energy to charge ratio; and a sensing unit measuring a current induced by the deflected charged particle beam, wherein the deflector includes at least one particle beam separation electrode provided at each of opposite sides with respect to a progress axis of the charged particle beam before being deflected, and the sensing unit is configured to simultaneously collect the positive ion and the negative ion in different regions of the sensing unit, wherein the positive ion and the negative ion are separated from each other by a voltage applied to the at least one particle beam separation electrode. 2. The particle beam mass spectrometer of claim 1 , wherein each particle beam separation electrode has a shape selected from a plate shape, a cylindrical shape, a spherical shape, an elliptical shape, and a bar shape with a cross section having a half-circular shape or a quarter-circular shape. 3. The particle beam mass spectrometer of claim 1 , wherein each particle beam separation electrode includes at least two separation electrodes provided at each of opposite sides with respect to the progress axis of the charged particle beam before being deflected. 4. The particle beam mass spectrometer of claim 3 , wherein each particle beam separation electrode includes an upper separation electrode and a lower separation electrode, whereby a four-pole (quadrupole) shape is provided, and polarities of the separation electrodes respectively provided at positions diagonally facing each other are same. 5. The particle beam mass spectrometer of claim 4 , wherein each particle beam separation electrode has a quarter-circular shape when viewed from a cross section, and has a bar shape in a longitudinal direction. 6. The particle beam mass spectrometer of claim 1 , wherein a DC or a combined signal of the DC with RF is applied to a separation electrode of the particle beam separation electrode. 7. The particle beam mass spectrometer of claim 6 , wherein a voltage applied to the particle beam separation electrode is a DC voltage having a constant value over time, or a signal of one of patterns where a voltage increases or decreases, or the voltage decreases after increases, or the voltage increases after decreases within a particular range over time is applied to the particle beam separation electrode. 8. The particle beam mass spectrometer of claim 1 , wherein the sensing unit includes Faraday cups ranging in number from 1 to 10, and when there is a plurality of the Faraday cups, the sizes of the Faraday cups are equal to each other or are different from each other. 9. The particle beam mass spectrometer of claim 1 , wherein the particle focusing unit is provided with an opening positioned at a body of the unit so as to discharge gas to outside. 10. A method of obtaining information about a size or a density or both of a particle by using the particle beam mass spectrometer of claim 1 .
Mass spectrometers or separator tubes · CPC title
Multipole linear ion traps, e.g. quadrupoles, hexapoles · CPC title
combined with mass spectrometry · CPC title
by investigating the ionisation of gases, e.g. aerosols; by investigating electric discharges, e.g. emission of cathode · CPC title
with electrons, e.g. electron impact ionisation, electron attachment (H01J49/145 takes precedence) · CPC title
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