Vacuum insulating glass (VIG) unit with pump-out port sealed using metal solder seal, and/or method of making the same

Patent metadata

Field	Value
Publication number	US-10280680-B2
Application number	US-201615170265-A
Country	US
Kind code	B2
Filing date	Jun 1, 2016
Priority date	Dec 31, 2013
Publication date	May 7, 2019
Grant date	May 7, 2019

Abstract

Certain example embodiments relate to vacuum insulating glass units having pump-out hole seals formed in connection with solder alloys that, when reactively reflowed, wet pre-coated metallic coatings, and/or associated methods. The alloys may be based on materials that form seals at temperatures that will not de-temper glass and/or decompose a laminate, and/or remain hermetic and lack porous structures in their bulks. SAC, InAg, and/or other preform materials may be used in different example embodiments.

First claim

What is claimed is:

1. A vacuum insulating glass (VIG) unit, comprising:
first and second substantially parallel spaced apart glass substrates, at least one of the first and second glass substrates being a heat treated glass substrate;
a plurality of spacers provided between the first and second substrates;
an edge seal;
a cavity between the first and second glass substrates, the cavity being evacuated to a pressure less than atmospheric; and
a hole seal member at least partially located in a pump-out hole formed in the first substrate that was used during VIG unit manufacturing to evacuate the cavity, the hole seal member and the first substrate being hermetically sealed to one another in the pump-out hole via a hole seal formed by reactively reflowing a solid solder alloy pre-form comprising metal, which causes (a) material from a first multi-layer thin film coating pre-provided on the first substrate to diffuse into the solder alloy material and vice versa, and (b) formation of an inter-metallic compound (IMC) between an uppermost layer of the first multi-layer thin film coating and the reactively reflowed solder.

2. The VIG unit of claim 1 , wherein the first multi-layer thin film coating comprises an activated energetic spray deposition deposited silver-inclusive layer, and an activated energetic spray deposition deposited nickel-inclusive layer, at least a portion of the first multi-layer thin film coating remaining in the VIG unit.

3. The VIG unit of claim 1 , wherein the alloy material comprises either (i) Sn, Ag, and Cu, or (ii) In and Ag.

4. The VIG unit of claim 1 , wherein at least one of the first and second substrates is thermally tempered, each thermally tempered substrate retaining at least 90% of its temper strength in the VIG unit.

5. The VIG unit of claim 1 , wherein the hole seal member has a second multi-layer thin film coating pre-provided thereto, the first and second multi-layer thin film coatings having the same layers as one another.

6. The VIG unit of claim 1 , wherein the first multi-layer thin film coating was formed in the pump-out hole.

7. A vacuum insulating glass (VIG) unit, comprising:
first and second substantially parallel spaced apart glass substrates, at least one of the first and second glass substrates being a heat treated glass substrate;
a plurality of spacers provided between the first and second substrates;
an edge seal;
a cavity between the first and second glass substrates, the cavity being evacuated to a pressure less than atmospheric; and
a hole seal member provided at least partially in a pump-out hole formed in the first substrate that was used to evacuate the cavity, the hole seal member and the first substrate being hermetically sealed to one another in the pump-out hole via a hole seal comprising an inter-metallic compound (IMC) between an uppermost layer of a first multi-layer thin film coating and reactively reflowed solder.

Assignees

• Guardian Glass Llc

Inventors

• Veerasamy Vijayen S
• Tucker Patricia

Classifications

• C03C17/3652

  the coating stack containing at least one sacrificial layer to protect the metal from oxidation · CPC title

• C03C17/36

  at least one coating being a metal · CPC title

• C03C17/3644

  the metal being silver · CPC title

• E06B3/6612

  Evacuated glazing units · CPC title

• E06B3/67334 Primary

  by soldering; Preparing the panes therefor · CPC title