Self cleaning gas-liquid separator for serial or parallel collection of liquid fractions

Patent metadata

Field	Value
Publication number	US-10279294-B2
Application number	US-201214123191-A
Country	US
Kind code	B2
Filing date	Jun 1, 2012
Priority date	Jun 1, 2011
Publication date	May 7, 2019
Grant date	May 7, 2019

Abstract

An apparatus, process, and system are disclosed that effectively provide separation of a combined gas/liquid flow stream into its separated gas and liquid factions. The invention is primarily directed to the fields of preparative supercritical fluid chromatography (SFC) and supercritical fluid extraction (SFE), but will have other utilization and applicability where phases of dramatically different density, viscosity and volumetric flow require separation.

First claim

What is claimed is:

1. An apparatus for a gas-liquid flowstream, comprising:
a constraint housing having an upper end and a lower end, and being configured for receiving a pressurized gas-liquid or aerosolized flowstream for forming within the constraint housing coalesced droplets as the gas-liquid flowstream passes therethrough to thereby separate the gas-liquid flowstream into a gas phase and a liquid phase;
wherein the lower end of the constraint housing has an opening to allow at least a portion of the separated gas phase to exit the constraint housing and thereby improve a drainage time of the liquid phase; and
a drip line connected to an exit of the opening in the lower end of the constraint housing and providing a path for direct drainage of the liquid phase from the constraint housing, and the drip line is configured for release of liquid phase droplets from the apparatus.

2. The apparatus of claim 1 , wherein the constraint housing comprises a channel for collection of the liquid phase, and the drip line is connected to an open portion of the channel.

3. The apparatus of claim 2 , wherein the channel comprises a spiral channel.

4. The apparatus of claim 1 further comprising:
a coalescence filter disposed inside the constraint housing; and
an inlet flowpath having fluidic communication with an interior cavity of the filter.

5. The apparatus of claim 4 , wherein at least a portion of the filter has an external surface area relatively larger than a cross-sectional area of said inlet flowpath to the filter.

6. The apparatus of claim 4 , wherein the filter is shaped as one of a cylinder, a sphere, a cuboid, a prism, or a trapezoid.

7. The apparatus of claim 1 , further comprising:
a coalescence filter disposed inside the constraint housing; and
the drip line drains liquid separated from said filter.

8. The apparatus of claim 1 , wherein the lower end of the constraint housing comprises a tapered portion, and the drip line is coupled to the tapered portion.

9. The apparatus of claim 1 , wherein the drip line comprises a fabrication of polymer filaments or inert metal wires, and the liquid droplets are drained along an exterior surface of the drip line.

10. A gas-liquid separation system, comprising:
the apparatus of claim 1 , wherein the constraint housing comprises an inlet flowpath that receives the pressurized gas-liquid or aerosolized flowstream; and
a vent.

11. The system of claim 10 , wherein the drip line collects the liquid phase and the vent collects the gas component.

12. The system of claim 10 , further comprising:
a make-up pump which draws solvent liquid from a reservoir and pumps the liquid into the pressurized gas-liquid flowstream prior to entering said inlet flowpath.

13. The system of claim 10 , further comprising:
a pressurized gas source which provides a gas flow to a channel for collection of the liquid phase, wherein said gas flow provides a downdraft to force liquid out of the channel.

14. The system of claim 10 , further comprising:
a pressurized rinse assembly connected by a valve or pump to the inlet flowpath of the constraint housing,
wherein the rinse assembly provides a wash solvent into said inlet flowpath thereby providing a wash to the constraint housing.

15. The system of claim 10 , further comprising:
a coalescence filter inserted in the constraint housing;
a channel disposed between the coalescence filter and the constraint housing, the channel configured for receiving the gas-liquid flowstream after the flowstream passes through the coalescence filter,
wherein the drip line is connected to an open portion of the channel.

16. The system of claim 10 , wherein
the constraint housing comprises a channel for collection of the liquid fraction, and
the system further comprises a gas supply line for providing a gas to the channel.

17. The system of claim 10 , further comprising a pump coupled to the lower end of the constraint housing.

Assignees

• Fogelman Kimber D
• Berger Terry A
• Wikfors Edwin E
• Agilent Technologies Inc

Inventors

• Fogelman Kimber D
• Berger Terry A
• Wikfors Edwin E

Classifications

• B01D11/0203

  with a supercritical fluid · CPC title

• B01D46/0082

  Operations & Transport · mapped topic

• B01D46/0031 Primary

  with collecting, draining means · CPC title

• B01D15/247

  Fraction collectors · CPC title

• G01N30/80

  Fraction collectors · CPC title