Peel adhesion test specimens and method for their preparation

Patent metadata

Field	Value
Publication number	US-10274416-B2
Application number	US-201715599209-A
Country	US
Kind code	B2
Filing date	May 18, 2017
Priority date	May 18, 2017
Publication date	Apr 30, 2019
Grant date	Apr 30, 2019

Abstract

A method of preparing specimens for peel-adhesion testing. The method includes applying a first predetermined amount of light-curable material to a substrate coupon, placing a first surface of a substantially transparent peel media in contact with the light-curable material disposed on the substrate coupon, where the substantially transparent peel media includes a second surface spaced from the first surface, and exposing the first predetermined amount of light-curable material disposed between the substrate coupon and the first surface to a light source to cure the first predetermined amount of light-curable material, with light from the light source passing through the substantially transparent peel media to the substrate coupon.

First claim

What is claimed is:

1. A method of preparing specimens for peel-adhesion testing, the method comprising:
applying a first predetermined amount of light-curable material to a substrate coupon;
placing a first surface of a substantially transparent peel media in contact with the light-curable material disposed on the substrate coupon, where the substantially transparent peel media includes a second surface spaced from the first surface; and
exposing the first predetermined amount of light-curable material disposed between the substrate coupon and the first surface to a light source to cure the first predetermined amount of light-curable material to both the substrate coupon and the substantially transparent peel media, with light from the light source passing through the substantially transparent peel media to the substrate coupon.

2. The method of claim 1 , wherein the first surface of the substantially transparent peel media is activated for promoting adhesion of the light-curable material to the substantially transparent peel media.

3. The method of claim 2 , wherein the first surface of the substantially transparent peel media is activated by chemically treating the first surface.

4. The method of claim 1 , further comprising:
applying a second predetermined amount of the light-curable material to the second surface of the substantially transparent peel media; and
exposing the second predetermined amount of light-curable material to a light source to cure the second predetermined amount of light-curable material to the second surface of the substantially transparent peel media.

5. The method of claim 4 , wherein the second surface of the substantially transparent peel media is activated for promoting adhesion of the light-curable material to the substantially transparent peel media.

6. The method of claim 4 , wherein the light-curable material disposed between the substrate coupon and the first surface and the light curable material applied to the second surface of the substantially transparent peel media are cured substantially simultaneously.

7. The method of claim 4 , wherein a first thickness of the light-curable material disposed between the substrate coupon and the first surface and a second thickness of the light curable material applied to the second surface of the substantially transparent peel media are substantially equal.

8. The method of claim 4 , further comprising forming a peel panel by separating the substantially transparent peel media, the first predetermined amount of light-curable material cured to the first surface and the substrate coupon, and the second predetermined amount of light-curable material cured to the second surface into at least two test strips cured to the substrate coupon.

9. The method of claim 1 , further comprising forming a peel panel by separating the substantially transparent peel media and the first predetermined amount of light-curable material cured to the first surface and the substrate coupon into at least two test strips cured to the substrate coupon.

10. The method of claim 1 , wherein the substantially transparent peel media comprises a polymeric material.

11. A method of preparing specimens for peel-adhesion testing, the method comprising:
applying a first predetermined amount of light-curable material to a substrate coupon;
activating a first and second surface of a substantially transparent peel media, where the first surface and the second surface are spaced from one another;
placing the first surface of the substantially transparent peel media in contact with the light-curable material disposed on the substrate coupon;
applying a second predetermined amount of the light-curable material to the second surface of the substantially transparent peel media; and
exposing the first predetermined amount of light-curable material and the second predetermined amount of light-curable material to a light source so that the first predetermined amount of light-curable material disposed between the substrate coupon and the first surface and the second predetermined amount of light curable material applied to the second surface of the substantially transparent peel media are cured substantially simultaneously with light from the light source passing through the substantially transparent peel media.

12. The method of claim 11 , wherein the first surface and the second surface of the substantially transparent peel media are activated for promoting adhesion of the first predetermined amount of light-curable material and the second predetermined amount of light-curable material to the substantially transparent peel media.

13. The method of claim 12 , wherein the first surface and the second surface of the substantially transparent peel media are activated by exposing the first surface and the second surface to oxygen plasma.

14. The method of claim 12 , wherein the first surface and the second surface of the substantially transparent peel media are activated by corona discharge treating the first surface and the second surface.

15. The method of claim 12 , wherein the first surface and the second surface of the substantially transparent peel media are activated by exposing the first surface and the second surface to ultraviolet light.

16. The method of claim 12 , wherein the first surface and the second surface of the substantially transparent peel media are activated by exposing the first surface and the second surface to ozone.

17. The method of claim 12 , wherein the first surface and the second surface of the substantially transparent peel media are activated by chemically treating the first surface and the second surface.

18. The method of claim 11 , wherein a thickness of the first predetermined amount of light-curable material disposed between the substrate coupon and the first surface and a thickness of the second predetermined amount of light curable material applied to the second surface of the substantially transparent peel media are substantially equal.

19. The method of claim 11 , further comprising forming a peel panel by separating the substantially transparent peel media, the first predetermined amount of light-curable material cured to the first surface and the substrate coupon, and the second predetermined amount of light- curable material cured to the second surface into at least two test strips cured to the substrate coupon.

20. The method of claim 11 , wherein the substantially transparent peel media comprises a polymeric material.

Assignees

• Boeing Co

Inventors

• Stevens Barton E
• Frank Katherine L

Classifications

• G01N3/08

  by applying steady tensile or compressive forces (G01N3/28 takes precedence) · CPC title

• G01N2203/0091

  Peeling or tearing · CPC title

• G01N1/44

  Sample treatment involving radiation, e.g. heat · CPC title

• G01N19/04 Primary

  Measuring adhesive force between materials, e.g. of sealing tape, of coating · CPC title

• G01N2203/0298

  Manufacturing or preparing specimens · CPC title