Ore slurry pre-treatment method and ore slurry manufacturing method

Patent metadata

Field	Value
Publication number	US-10273558-B2
Application number	US-201515552013-A
Country	US
Kind code	B2
Filing date	Dec 1, 2015
Priority date	Feb 25, 2015
Publication date	Apr 30, 2019
Grant date	Apr 30, 2019

Abstract

Provided is a hydrometallurgical process for nickel oxide ore effectively reducing the amount of sulfuric acid used in the leaching step and the amount of a neutralizer such as slaked lime used in the final neutralization step without reducing nickel yield. The present invention is a method for pre-treating ore slurry to be submitted for leaching treatment in a hydrometallurgical process for nickel oxide ore, the method comprising: a separating step for separating the ore slurry into a coarse particle fraction, in which particles having a particle diameter of less than 45 μm are 30 mass % of the solids or less, and a fine particle fraction, and feeding said fine particle fraction to the leaching process; and a vibration sieving step for separating the separated coarse particle fraction into oversize particles and undersize particles using vibration sieving and feeding the ore slurry of said undersize particles to the leaching process.

First claim

The invention claimed is:

1. A method for pre-treating ore slurry to be provided to a leaching treatment in a hydrometallurgical process for nickel oxide ore, the method comprising:
a separation step for separating ore slurry into a coarse particle fraction in which particles having a particle diameter of less than 45 μm are 30% by mass or less in a solid content and a fine particle fraction and supplying the fine particle fraction to the leaching treatment; and
a vibration sieving step for separating, by a vibration sieve having a mesh size of 300 μm or more and 500 μm or less, the separated coarse particle fraction into a fraction on the sieve and a fraction under the sieve and supplying the fraction under the sieve as ore slurry to the leaching treatment.

2. The method for pre-treating ore slurry according to claim 1 , wherein any one or more of a hydrocyclone and a density separator are used in the separation step.

3. The method for pre-treating ore slurry according to claim 2 , wherein the separation step includes
a classification and separation step for supplying the ore slurry to a hydrocyclone and subjecting the ore slurry to classification and separation, and
a specific gravity separation step for supplying an underflow classified by the hydrocyclone in the classification and separation step to a density separator and subjecting the underflow to specific gravity separation.

4. The method for pre-treating ore slurry according to claim 1 , wherein the hydrometallurgical process for nickel oxide ore includes
ore slurry formation step for forming slurry of the nickel oxide ore (ore slurry),
a leaching step for carrying out a leaching treatment on the ore slurry under high temperature and high pressure by adding sulfuric acid,
a solid-liquid separation step for separating a residue while the obtained leached slurry is washed in multiple stages, to obtain a leachate containing nickel and impurity elements,
a neutralization step for separating a neutralized precipitate containing the impurity elements by adjusting a pH of the leachate to obtain a post-neutralization solution containing nickel,
a sulfuration step for carrying out a sulfuration treatment on the post-neutralization solution to generate a sulfide containing nickel and a barren solution, and
a final neutralization step for recovering and detoxifying the barren solution discharged in the sulfuration step.

5. A method for manufacturing ore slurry to be provided to a leaching treatment in a hydrometallurgical process for nickel oxide ore, the method comprising:
ore slurry formation step for obtaining a coarse ore slurry from the nickel oxide ore;
a separation step for separating the coarse ore slurry into a coarse particle fraction in which particles having a particle diameter of less than 45 μm are 30% by mass or less in a solid content and a fine particle fraction;
a vibration sieving step for separating, by a vibration sieve having a mesh size of 300 μm or more and 500 μm or less, the separated coarse particle fraction into a fraction on the sieve and a fraction under the sieve; and
ore slurry condensation step for loading the ore slurry of the fine particle fraction separated in the separation step and the ore slurry of the fraction under the sieve separated in the vibration sieving step into a solid-liquid separation device and separating and removing moisture contained in the ore slurry to condense ore components.

Assignees

• Sumitomo Metal Mining Co

Inventors

• Higuchi Hirotaka
• Ohara Go
• Nakai Osamu
• Imamura Masaki

Classifications

• C22B23/005 Primary

  Preliminary treatment of ores, e.g. by roasting or by the Krupp-Renn process · CPC title

• C22B23/0453

  Treatment or purification of solutions, e.g. obtained by leaching (C22B23/0407 takes precedence) · CPC title

• C22B3/08

  Sulfuric acid {, other sulfurated acids or salts thereof} · CPC title

• C22B23/043

  Sulfurated acids or salts thereof · CPC title

• C22B23/0415

  with acids or salt solutions except ammonium salts solutions · CPC title