Method for the continuous thermal hydrolysis of sludge with a high dryness value

Patent metadata

Field	Value
Publication number	US-10246360-B2
Application number	US-201415107606-A
Country	US
Kind code	B2
Filing date	Dec 23, 2014
Priority date	Dec 26, 2013
Publication date	Apr 2, 2019
Grant date	Apr 2, 2019

Abstract

Method and plant to implement the continuous thermal hydrolysis of sludge to be treated containing organic matter, the method comprising at least:
a. a step for de-structuring said sludge to be treated producing de-structured sludge; b. a step for the thermal hydrolysis of said de-structured sludge within a thermal hydrolysis reactor producing hydrolyzed sludge; c. a step for cooling said hydrolyzed sludge; said step for de-structuring consisting in:
introducing said sludge to be treated into a dynamic mixer; heating said sludge coming from said dynamic mixer, this heating being obtained by the introduction, into a heat exchanger, on the one hand of said sludge coming from said dynamic mixer and, on the other hand, of said hydrolyzed sludge, this introduction inducing said cooling.

First claim

The invention claimed is:

1. A method for the continuous thermal hydrolysis of sludge to be treated containing organic matter, the method comprising at least:
a. a step for de-structuring said sludge to be treated producing de-structured sludge, said sludge having a dry solids content greater than 20% (wt.);
b. a step for the thermal hydrolysis of said de-structured sludge within a thermal hydrolysis reactor producing hydrolyzed sludge;
c. a step for cooling said hydrolyzed sludge;
said step for de-structuring including:
introducing said sludge to be treated into a dynamic mixer comprising a chamber and a rotor
injecting steam into the dynamic mixer;
rotating the rotor at a speed gradient between 1500 rpm and 4000 rpm to mix and de-structure the sludge;
heating said sludge coming from said dynamic mixer, this heating being obtained by the introduction, into a heat exchanger, on the one hand of said sludge coming from said dynamic mixer and, on the other hand, of said hydrolyzed sludge, this introduction inducing said cooling.

2. The method of claim 1 , characterized in that said steam injected into said dynamic mixer has a temperature of 120° C. to 190° C. and/or a pressure of 2 bar to 13 bar.

3. The method of claim 1 , characterized in that the method comprises a step for carrying out, simultaneously, the injection of steam under pressure into said sludge coming from said heat exchanger and the mixing of said sludge with said steam by means of a dynamic injector-mixer so as to obtain a uniform mixture of sludges de-structured and heated to the desired temperature of thermal hydrolysis, said mixture being conveyed into said thermal hydrolysis reactor.

4. The method of claim 3 , characterized in that said steam injected into said dynamic injector-mixer has a pressure of 1 bar to 23 bars, and/or a temperature of 100° C. to 220° C.

5. The method of claim 1 , characterized in that said step for cooling is followed by a step for digesting said hydrolyzed and cooled sludges.

6. A plant for continuously thermally hydrolyzing sludge comprising:
a. means for conveying sludge to be treated;
b. a dynamic mixer having a rotor configured to rotate 1500-4000 rpm;
c. said dynamic mixer configured to receive the sludge and to de-structure the sludge and produce a homogeneous de-structured sludge;
d. a heat exchanger located downstream from the dynamic mixer and comprising an inlet configured to receive said homogeneous de-structured sludge from the dynamic mixer and an outlet for discharging heated homogeneous de-structured sludge;
e. a thermal hydrolysis reactor located downstream of said heat exchanger and including an inlet for receiving the heated homogeneous de-structured sludge produced by the heat exchanger;
f. means for recirculating said hydrolyzed sludge to a hydrolyzed sludge inlet associated with the heat exchanger such that the heat exchanger is a sludge-to-sludge heat exchanger that effectively cools the thermally hydrolyzed sludge; and
g. a dynamic injector-mixer located downstream of said heat exchanger, and wherein said dynamic injector-mixer is configured to receive the homogeneous de-structured sludge produced by said heat exchanger; and wherein said dynamic injector-mixer further comprises a steam inlet for receiving steam and an outlet for discharging a homogenous mixture of heated de-structured sludge.

7. The plant according to claim 6 , characterized in that said plant comprises means for injecting steam into said dynamic mixer.

8. The plant of claim 6 further comprising a digester located downstream of the thermal hydrolysis reactor for receiving and digesting thermally hydrolyzed sludge.

9. The plant of claim 6 wherein said heat exchanger extends essentially vertically or horizontally.

10. A method for continuous thermal hydrolysis of dehydrated sludge containing organic matter, the method comprising:
a. subjecting the dehydrated sludge having a dry solids content exceeding 20% (wt.) to a sludge de-structuring process and mechanically de-structuring the sludge and reducing the viscosity of the sludge and in the process forming a fluidized homogeneous de-structured sludge;
b. wherein mechanically de-structuring the sludge comprises:
i. directing the sludge into a dynamic mixer comprising a chamber having a rotor;
ii. injecting steam into the dynamic mixer and driving the rotor at a speed of 1500-4000 rpm;

c. directing the homogenized de-structured sludge from the dynamic mixer into and through a sludge-to-sludge heat exchanger and heating the homogenized de-structured sludge;
d. directing the heated homogenized de-structured sludge from the heat exchanger to a thermal hydrolysis reactor and thermally hydrolyzing the sludge; and
e. directing the thermally hydrolyzed sludge back to and through the sludge-to-sludge heat exchanger where the thermally hydrolyzed sludge heats the homogenized de-structured sludge produced by the dynamic mixer.

Assignees

• Veolia Water Solutions & Tech

Inventors

• Crampon Cedric
• Chauzy Julien
• Djafer Malik

Classifications

• C02F2303/06

  Sludge reduction, e.g. by lysis · CPC title

• C02F1/34

  with mechanical oscillations · CPC title

• C02F1/025

  Thermal hydrolysis · CPC title

• C02F2301/06

  Pressure conditions · CPC title

• C02F11/18 Primary

  by thermal conditioning (by pyrolysis C02F11/10) · CPC title