Powder metallurgy method for making components

Patent metadata

Field	Value
Publication number	US-10245639-B2
Application number	US-201213563216-A
Country	US
Kind code	B2
Filing date	Jul 31, 2012
Priority date	Jul 31, 2012
Publication date	Apr 2, 2019
Grant date	Apr 2, 2019

Abstract

A powder metallurgy method includes (a) forming a metallic powder into a shape, (b) thermo-mechanically forming the shape into an article having a polycrystalline microstructure, (c) heat treating the article to cause coarsening of the polycrystalline microstructure, and (d) controlling the grain size homogeneity and distribution in the article formed during coarsening in step (c) by selecting the metallic powder in step (a) to include a metallic powder particle size distribution that is truncated on fine and coarse particle size sides, the selected metallic powder particle size distribution reducing abnormal grain growth such that the polycrystalline microstructure coarsens to a predefined target grain size range.

First claim

What is claimed is:

1. A powder metallurgy method comprising:
(a) consolidating a metallic powder into a shape;
(b) thermo-mechanically forging the shape into an article having a polycrystalline microstructure;
(c) heat treating the article to cause coarsening of the polycrystalline microstructure; and
(d) controlling the grain size homogeneity and distribution in the article formed during coarsening in step (c) by selecting the metallic powder in step (a) to include a metallic powder particle size distribution that is truncated on fine and coarse particle size sides, the selected metallic powder particle size distribution reducing abnormal grain growth such that grains of the polycrystalline microstructure coarsen and are all within an ASTM grain size number of 4-8.

2. The method as recited in claim 1 , wherein step (d) includes controlling a size distribution of pores and inclusions in the article by selecting the metallic powder in step (a) to include the metallic powder particle size distribution that is truncated on the coarse particle size sides.

3. The method as recited in claim 1 , further including improving fatigue performance of the article by controlling the grain size homogeneity and distribution in the article formed during the coarsening in step (c) and controlling a size distribution of pores and inclusions in the article, by selecting the metallic powder in step (a) to include the metallic powder particle size distribution that is truncated on the fine and coarse particle size sides.

4. The method as recited in claim 1 , wherein the metallic powder is a superalloy.

5. The method as recited in claim 1 , wherein the metallic powder particle size distribution is truncated below 0.5 micrometers and above 200 micrometers.

6. The method as recited in claim 1 , wherein the metallic powder particle size distribution is truncated below 5 micrometers and above 160 micrometers.

7. The method as recited in claim 1 , wherein the metallic powder particle size distribution is truncated below 15 micrometers and above 140 micrometers.

8. The method as recited in claim 1 , wherein the metallic powder is a nickel- or cobalt-based composition and the metallic powder particle size distribution is truncated below 0.5 micrometers and above 200 micrometers.

9. The method as recited in claim 1 , wherein the consolidating of said step (a) includes at least one of extrusion or hot isostatic pressing.

10. A powder metallurgy method comprising:
improving fatigue performance of an article that is formed using a metallic powder by selecting the metallic powder to include a metallic powder particle size distribution that is truncated on a fine particle size side below 15 micrometers and a coarse particle size side above 140 micrometers,
the improved fatigue performance being caused by homogenous and narrower grain size distribution achieved by a reduction in abnormal grain growth in the article during heat treating such that grains of a polycrystalline micro structure of the article coarsen and are all within an ASTM grain size number of 4-8, and there is a reduction in a largest size of inclusions and pores in the article due to the selected metallic powder particle size distribution.

Assignees

• Wusatowska Sarnek Agnieszka M
• Mace Ronald S
• Wasan Harpreet
• Moore Ruston M
• Wezalis John M
• Housefield Larry G
• United Technologies Corp

Inventors

• Wusatowska-Sarnek Agnieszka M
• Mace Ronald S
• Wasan Harpreet
• Moore Ruston M
• Wezalis John M
• Housefield Larry G

Classifications

• B22F3/17

  by forging · CPC title

• B22F2003/248

  Thermal after-treatment · CPC title

• B22F1/0014 Primary

  Operations & Transport · mapped topic

• B22F2998/10

  Processes characterised by the sequence of their steps · CPC title

• B22F3/24 Primary

  After-treatment of workpieces or articles {(B22F3/1146 takes precedence)} · CPC title