Apparatus and method for ionic liquid electroplating
US-2015101935-A1 · Apr 16, 2015 · US
US10240245B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10240245-B2 |
| Application number | US-201715635833-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jun 28, 2017 |
| Priority date | Jun 28, 2017 |
| Publication date | Mar 26, 2019 |
| Grant date | Mar 26, 2019 |
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Ionic liquid bath plating systems, methods, and plating anodes are provided for depositing metallic layers over turbomachine components and other workpieces. In an embodiment, the method includes placing workpieces in a plurality of cell vessels such that the workpieces are at least partially submerged in plating solution baths, which are retained within the cell vessels when the plating system is filled with a selected non-aqueous plating solution. After plating anodes are positioned adjacent the workpieces in the plating solution baths, the plurality of cell vessels are enclosed with lids such that the plurality of cell vessels contain vessel headspaces above the plating solution baths. A first purge gas is then injected into the plurality of cell vessels to purge the vessel headspaces. The workpieces and the plating anodes are then energized to deposit metallic layers on selected surfaces of the workpieces utilizing an ionic liquid bath plating process.
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What is claimed is: 1. A method carried-out utilizing an ionic liquid bath plating system including a plurality of cell vessels fluidly coupled to a gas-purged reservoir tank having a headspace, the method comprising: placing workpieces in the plurality of cell vessels such that the workpieces are at least partially submerged in plating solution baths, which are retained within the cell vessels when the ionic liquid bath plating system is filled with a selected non-aqueous plating solution; positioning plating anodes adjacent the workpieces in the plating solution baths; after positioning the plating anodes adjacent the workpieces, enclosing the plurality of cell vessels with lids such that the plurality of cell vessels contain vessel headspaces above the plating solution baths; after enclosing the plurality of cell vessels with lids, injecting a first purge gas into the plurality of cell vessels to purge the vessel headspaces; energizing the workpieces and the plating anodes to deposit metallic layers on selected surfaces of the workpieces utilizing an ionic liquid bath plating process; and purging the headspace of the gas-purged reservoir tank with a second purge gas different than the first purge gas. 2. The method of claim 1 further comprising circulating non-aqueous plating solution between the plating solution baths and the plating solution reservoir during the ionic liquid bath plating process. 3. The ionic liquid bath plating system of claim 2 further comprising conditioning the plating solution reservoir utilizing an electrolytic dummy cell having terminals in contact with the plating solution reservoir during the ionic liquid bath plating process. 4. The method of claim 1 further comprising selecting the first and second purge gasses to comprise an argon-based gas and a nitrogen-based gas, respectively. 5. The method of claim 1 wherein injecting comprises injecting, as the first purge gas, an argon-based gas into the plurality of cell vessels to create blankets of the argon-based gas overlying the plating solution baths retained within the plurality of cell vessels. 6. The method of claim 1 wherein injecting comprises delivering the first purge gas into the vessel headspaces in an ultradry state containing less than 0.1% moisture, by volume. 7. The method of claim 1 wherein placing comprises placing a plurality of rotor blade pieces in the plurality of cell vessels, the plurality of rotor blade pieces each having opposing suction and pressure sides; and wherein energizing comprises energizing the plurality of rotor blade pieces and the plating anodes to concurrently deposit metallic layers over at least the suction and pressure sides of the plurality of rotor blade pieces during the ionic liquid bath plating process. 8. The method of claim 1 wherein at least one the workpieces comprises a turbomachine component including multiple airfoils; wherein the plating anodes comprise a multi-airfoil plating anode from which multiple anode fingers extend; and wherein positioning comprises positioning the multi-airfoil plating anode adjacent the turbomachine component such that the multiple anode fingers extend between the multiple airfoils. 9. The method of claim 8 wherein the multiple airfoils included within the turbomachine component are arranged in an annular array; and wherein the method further comprises selecting the multi-airfoil plating anode to include an annular array of the multiple anode fingers, which extends between the annular array of the multiple airfoils when the multi-airfoil plating anode is positioned adjacent the turbomachine component. 10. A method carried-out utilizing an ionic liquid bath plating system including a cell vessel fluidly coupled to a gas-purged reservoir tank having a headspace, the method comprising: placing a workpiece in the cell vessel such that the workpiece is at least partially submerged in a plating solution bath, which is retained within the cell vessel when the ionic liquid bath plating system is filled with a selected non-aqueous plating solution; positioning a plating anode adjacent the workpiece in the plating solution bath; after positioning the plating anode adjacent the workpiece, enclosing the cell vessel with a lid such that the cell vessel contains a vessel headspace above the plating solution bath; after enclosing the cell vessel with the lid, injecting a first purge gas into the cell vessel to purge the vessel headspace; energizing the workpiece and the plating anode to deposit a metallic layer on selected surfaces of the workpieces utilizing an ionic liquid bath plating process; and purging the headspace of the gas-purged reservoir tank with a second purge gas different than the first purge gas. 11. The method of claim 10 further comprising circulating non-aqueous plating solution between the plating solution bath and the plating solution reservoir during the ionic liquid bath plating process. 12. The method of claim 11 further comprising conditioning the plating solution reservoir utilizing an electrolytic dummy cell having terminals in contact with the plating solution reservoir during the ionic liquid bath plating process. 13. The method of claim 10 further comprising selecting the first and second purge gasses to comprise an argon-based gas and a nitrogen-based gas, respectively. 14. The method of claim 10 wherein injecting comprises injecting, as the first purge gas, an argon-based gas into the cell vessel to create a blanket of the argon-based gas overlying the plating solution bath retained within the cell vessel. 15. The method of claim 10 wherein injecting comprises delivering the first purge gas into the vessel headspace in an ultradry state containing less than 0.1% moisture, by volume. 16. The method of claim 10 wherein placing comprises placing a rotor blade piece in the cell vessel, the rotor blade piece having opposing suction and pressure sides; and wherein energizing comprises energizing the rotor blade piece and the plating anode to concurrently deposit the metallic layer over at least the suction and pressure sides of the rotor blade piece during the ionic liquid bath plating process. 17. The method of claim 10 wherein the workpiece comprises a turbomachine component including multiple airfoils; wherein the plating anode comprises a multi-airfoil plating anode from which multiple anode fingers extend; and wherein positioning comprises positioning the multi-airfoil plating anode adjacent the turbomachine component such that the multiple anode fingers extend between the multiple airfoils. 18. The method of claim 17 wherein the multiple airfoils included within the turbomachine component are arranged in an annular array; and wherein the method further comprises selecting the multi-airfoil plating anode to include an annular array of the multiple anode fingers, which extend between the annular array of the multiple airfoils when the multi-airfoil plating anode is positioned adjacent the turbomachine component.
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