Enhanced interventional CT imaging of cracks in rocks during hydraulic testing

Patent metadata

Field	Value
Publication number	US-10234407-B2
Application number	US-201816025088-A
Country	US
Kind code	B2
Filing date	Jul 2, 2018
Priority date	Aug 12, 2016
Publication date	Mar 19, 2019
Grant date	Mar 19, 2019

Abstract

The present invention improves the precision in observing cracks in rocks during a hydraulic fracturing test, improving a scientific understanding of the regular pattern of development cracks in of hydraulically fractured rocks. The technical solution includes: hydraulically fracturing the rock with aqueous solutions containing an interventional contrast-enhanced agent, forming hydraulically fractured cracks, wherein the difference in a mass attenuation coefficient μ/ρ of x-rays between the cracks and the rock is improved by the interventional contrast-enhanced agent in the cracks, moreover, the difference in mass energy absorption coefficient μ en /ρ of x-rays between the cracks and the rock is improved, then the linear attenuation coefficient of the reception of the detector is changed, improving the imaging resolution for hydraulically fractured cracks in the rock.

First claim

What is claimed is:

1. A system for high precision imaging of cracks in a hydraulic fracturing test of rock, comprising: an industrial x-ray CT in a laboratory setting, a high precision rotary platform and a hydraulic fracturing testing machine for rocks provided on the high precision rotary platform,
wherein the hydraulic fracturing testing machine for rocks includes a support device, a peripheral pressurizing device, an axial pressurizing device and a high pressure water pump, wherein the support device is used for clamping a rock sample to be fractured, the peripheral pressurizing device is disposed to surround the rock sample and used for applying pressure on periphery of the rock sample, the axial pressurizing device is provided below the support device and used for applying axial pressure to the rock sample, and the high pressure water pump is used for delivering interventional contrast-enhanced agent into the rock sample to form cracks within the rock sample,
wherein the industrial x-ray CT is used for forming a CT image of the cracks within the rock sample,
wherein the interventional contrast-enhanced agent is a dispersed nano bismuth solution which is made by the following steps: stirring a dispersant with a mass fraction of 5%, a nano bismuth powder with a mass fraction of 20% and a polyethylene glycol with a mass fraction of 75% for a first time period, and vibrating them for a second time period.

2. The system as defined by claim 1 , wherein diameters of particles of the nano bismuth material are in the range of 40-50 nm.

3. The system as defined by claim 2 , wherein the first time period is 10 minutes, and the second time period is 30 minutes.

4. The system as defined by claim 3 , wherein the support device includes an upper spacer and a lower spacer, and the upper spacer and the lower spacer support the rock sample from upper and lower sides of the rock sample respectively.

5. The system as defined by claim 4 , wherein the peripheral pressurizing device includes a triaxial cylinder surrounding the rock sample and a peripheral pressurizing pump in communication with the triaxial cylinder, and the peripheral pressurizing pump supplies power for the triaxial cylinder to apply peripheral pressure to the rock sample.

6. The system as defined by claim 5 , wherein the axial pressurizing device includes an axial actuator disposed on the high precision rotary platform and a self-balancing piston disposed on the axial actuator, such that the axial actuator applies axial pressure to the rock sample through the self-balancing piston.

7. The system as defined by claim 6 , wherein the laboratorial x-ray industrial CT includes an x-ray source and a CT detector, wherein the x-ray source is used for emitting x-rays, wherein the CT detector receives the x-rays that have penetrated the rock sample, and wherein the CT detector uses the received x-rays to form a CT image based on a distribution of linear attenuation coefficients obtained from materials within the rock sample being penetrated by the x-rays.

Assignees

• Inst Geology & Geophysics Cas

Inventors

• Li Shouding
• Zhou Zhongming
• Li Xiao
• He Jianming
• Liu Yanhui

Classifications

• G01N23/18

  Investigating the presence of flaws defects or foreign matter · CPC title

• G01N2203/0019

  Compressive · CPC title

• G01N2203/0647

  Image analysis · CPC title

• G01N2203/0242

  With circulation of a fluid · CPC title

• G01N2291/048

  Transmission, i.e. analysed material between transmitter and receiver · CPC title