Elimination of contaminants in wet natural rubber

Patent metadata

Field	Value
Publication number	US-10227420-B2
Application number	US-201615564322-A
Country	US
Kind code	B2
Filing date	Apr 8, 2016
Priority date	Apr 10, 2015
Publication date	Mar 12, 2019
Grant date	Mar 12, 2019

Abstract

A method for preparation of decontaminated natural rubber is provided. The method is characterized in that it comprises a decontamination step in which wet natural rubber coagulum passes through a system comprising an extruder and a filter installed at the extruder outlet, the extruder comprising an axially symmetrical grooved sheath comprising in its thickness grooves opening on the inner surface of the sheath.

First claim

The invention claimed is:

1. A method for preparation of decontaminated natural rubber, characterized in that it comprises a decontamination step in which wet natural rubber coagulum with a humidity level greater than 12% by weight passes through a system comprising an extruder and a filter installed at the extruder outlet,
the extruder comprising a grooved sheath, a screw arranged in the sheath and comprising a hub and a thread which extends radially outwardly relative to the hub,
a grooved sheath having an axially symmetrical structure comprising in its thickness grooves opening on the inner surface of the sheath,
each groove comprising
a bottom face delimited by two bottom ridges,
two side faces extending towards the inside from the bottom face, each being delimited by a bottom ridge and a ridge intersecting the inner surface of the sheath,

and characterized in that the sheath is such that, in any plane perpendicular to the axis of the sheath, R expressed in mm being the distance between the sheath center and the inner surface of the sheath:
a. the ratio (total length of groove openings expressed in mm)/(2πR), designated A, is at least equal to 0.25 and at most equal to 0.9;
b. the ratio (number of grooves/2R), designated B, is greater than or equal to 0.1;
c. the ratio (depth of grooves expressed in mm)/(2R), designated C, is greater than 0.02, and
d. the plane passing through the two bottom ridges forming, with each plane passing through a bottom ridge and an intersection ridge delimiting a side face, an angle d at least equal to 60° and at most equal to 90°.

2. A method according to claim 1 , characterized in that the grooved sheath is a cylindrical structure.

3. A method according to claim 1 , characterized in that A is at least equal to 0.3 and at most equal to 0.7.

4. A method according to claim 1 , characterized in that A is at least equal to 0.45 and at most equal to 0.55.

5. A method according to claim 1 , characterized in that each groove is trapezoid in form, the large base of the trapezium forming the bottom of the groove, the sides of the trapezium adjacent to the large base forming the side walls of the groove, the height of the trapezium being the depth of the groove.

6. A method according to claim 1 , characterized in that the bottom of the grooves is an arc of circle C R and the ratio C is calculated by the formula (I)

D
extF

-

D
intF

D
intF

>
0.02

(
I
)

D intF being the diameter of the inner surface of the sheath, or 2R
D extR being the diameter of circle C R , the center of which is the hub axis.

7. A method according to claim 1 , characterized in that the grooves of the sheath are parallel to the axis of the sheath.

8. A method according to claim 1 , characterized in that the grooves of the sheath are helical.

9. A method according to claim 1 , characterized in that the filter allows filtration of contaminants of size greater than 1 mm.

10. A method according to claim 1 , characterized in that the filter is a filter carrier comprising one or more mesh filters.

11. A method according to claim 1 , characterized in that the system also comprises a gear pump at the extruder outlet before the filter.

12. A method according to claim 1 , characterized in that the hub diameter is constant.

13. A method according to claim 1 , characterized in that the extruder is a single screw extruder.

14. A method according to claim 1 , characterized in that the extruder is supplied with a wet natural rubber coagulum with a humidity rate varying from 12% to 40%.

15. A method for processing of natural rubber, characterised in that it comprises the following successive steps:
a. Cleaning, homogenisation and coagulation of natural rubber;
b. Decontamination by the method defined in claim 1 ;
c. Drying of the decontaminated natural rubber.

16. A system comprising a grooved sheath extruder, a filter and in some cases a gear pump, characterized in that the extruder, the filter and the gear pump are as defined in claim 1 .

17. A method according to claim 1 , characterized in that the filter allows filtration of contaminants of size greater than 500 μm.

18. A method according to claim 1 , characterized in that the filter allows filtration of contaminants of size greater than 100 μm.

19. A method according to claim 1 , characterized in that the extruder is a single screw extruder with a thread of regular pitch.

Assignees

• Michelin & Cie

Inventors

• Dussillols Jérôme
• Merceron Jean-Luc

Classifications

• B29C48/686

  having grooves or cavities · CPC title

• B29C48/2715

  of plasticising units · CPC title

• B29C48/2552

  provided in the feeding, melting, plasticising or pumping zone, e.g. screw, barrel, gear-pump or ram · CPC title

• B29C48/022

  characterised by the choice of material · CPC title

• B29C48/6801

  characterised by the material or their manufacturing process · CPC title