Smokeless tobacco composition

Patent metadata

Field	Value
Publication number	US-10219537-B2
Application number	US-201514971283-A
Country	US
Kind code	B2
Filing date	Dec 16, 2015
Priority date	Jul 23, 2007
Publication date	Mar 5, 2019
Grant date	Mar 5, 2019

Abstract

The invention provides a process for preparing a tobacco composition suitable for use as a smokeless tobacco composition, the process including: providing a slurry comprising water and a tobacco material, the slurry comprising at least about 75% by weight water, based on the total weight of the slurry; heating the slurry to a temperature of at least about 60° C. for a time sufficient to pasteurize the tobacco material; adding an amount of a base to the slurry sufficient to raise the pH of the slurry to at least about 8.5, thereby forming a pH-adjusted slurry; and continuing to heat the pH-adjusted slurry to a temperature of at least about 60° C. for a time sufficient for the pH of the slurry to drop at least about 0.5 pH unit following the adding step.

First claim

We claim:

1. A process for preparing a tobacco composition suitable for use as a smokeless tobacco composition, comprising:
providing a slurry comprising water and a tobacco material;
heating the slurry to a temperature of at least about 60° C. for a time sufficient to pasteurize the tobacco material;
adding an amount of a base to the slurry sufficient to raise the pH of the slurry to at least about 8.5, thereby forming a pH-adjusted slurry;
continuing to heat the pH-adjusted slurry to a temperature of at least about 60° C. for a time sufficient for the pH of the slurry to drop at least about 0.5 pH unit following said adding step, wherein the moisture content of the tobacco material is maintained during the heating step at a level of at least about 30% by weight;
cooling the pH-adjusted slurry to about ambient temperature, the pH-adjusted slurry having a pH of at least about 8 at the time the cooling step begins; and
packaging the tobacco material in a pouch.

2. The process of claim 1 , further comprising the step of adding a salt to the slurry prior to said heating step.

3. The process of claim 2 , wherein said salt addition step comprises adding about 1 to about 5% by weight of sodium chloride, based on the dry weight of the tobacco material.

4. The process of claim 1 , wherein said slurry heating step comprises heating the slurry to a temperature of at least about 70° C. for at least about 30 minutes.

5. The process of claim 1 , wherein said step of continuing to heat the pH-adjusted slurry comprises heating the pH-adjusted slurry for at least about 1.5 hours.

6. The process of claim 1 , wherein said adding step comprises adding sufficient base to raise the pH of the slurry to at least about 9.0.

7. The process of claim 1 , wherein the base is selected from the group consisting of sodium carbonate, potassium carbonate, sodium bicarbonate, potassium bicarbonate, sodium hydroxide, potassium hydroxide, and mixtures thereof.

8. The process of claim 1 , wherein the moisture content of the tobacco composition, as present within the pouch prior to insertion into the mouth of a user, is about 25 weight percent to about 50 weight percent.

9. The process of claim 1 , wherein said slurry heating step comprises heating the slurry to a temperature of about 70° C. to about 100° C. for at least about 30 minutes.

10. The process of claim 1 , wherein said step of continuing to heat the pH-adjusted slurry comprises heating the pH-adjusted slurry to a temperature of about 70° C. to about 95° C. for at least about 1.5 hours.

11. The process of claim 1 , wherein the heating step comprises direct steam injection into the tobacco material.

12. The process of claim 1 , further comprising treating the tobacco material with a buffering agent in the form of a mixture of a metal carbonate and a metal bicarbonate; and incorporating the tobacco material into a smokeless tobacco product.

13. The process of claim 1 , further comprising the step of drying the tobacco material by continued heating of the tobacco material to reduce the moisture content prior to said cooling and packaging steps.

14. A process for preparing a tobacco composition suitable for use as a smokeless tobacco composition, comprising:
providing a slurry comprising water and a tobacco material;
heating the slurry to a temperature of at least about 60° C. for a time sufficient to pasteurize the tobacco material;
adding an amount of a base to the slurry sufficient to raise the pH of the slurry to at least about 8.5, thereby forming a pH-adjusted slurry;
continuing to heat the pH-adjusted slurry to a temperature of at least about 60° C. for a time sufficient for the pH of the slurry to drop at least about 0.5 pH unit following said adding step, wherein the moisture content of the tobacco material is maintained during the heating step at a level of at least about 30% by weight and wherein the heating step comprises direct steam injection into the tobacco material;
drying the tobacco material by continued heating of the tobacco material to reduce the moisture content;
cooling the pH-adjusted slurry to about ambient temperature, the pH-adjusted slurry having a pH of at least about 8 at the time the cooling step begins; and
packaging the tobacco material in a pouch.

Assignees

• Reynolds Tobacco Co R

Inventors

• Mua John-Paul
• Monsalud Jr Luis Rosete
• Holton Jr Darrell Eugene
• Figlar James Neil

Classifications

• A24B15/183

  sterilization, preservation or biological decontamination · CPC title

• A24B15/283

  by encapsulation of the chemical substances · CPC title

• A24F23/02

  Tobacco pouches · CPC title

• A24B15/186

  by coating with a coating composition, encapsulation of tobacco particles (encapsulation of additives other than tobacco : A24B15/283) · CPC title

• A24B15/18

  Treatment of tobacco products or tobacco substitutes · CPC title