Method for joining silicon carbide components to one another

Patent metadata

Field	Value
Publication number	US-10217534-B2
Application number	US-201816019893-A
Country	US
Kind code	B2
Filing date	Jun 27, 2018
Priority date	Sep 23, 2011
Publication date	Feb 26, 2019
Grant date	Feb 26, 2019

Abstract

A method for fabricating assemblies that includes providing a first component that further includes silicon carbide and that has an upper portion and a tapered lower portion; providing a second component that further includes silicon carbide and that has an upper portion that is adapted to receive the tapered lower portion of the first component; providing a predetermined amount of multiphase Al—Si braze foil; grinding the Al—Si braze foil into a powder; mixing a predetermined amount of braze paste binder with the Al—Si powder to form a slurry; uniformly applying the slurry to the tapered lower portion of the first component; uniformly applying the slurry to the upper portion of the second component and inserting the tapered lower portion of the first component into the upper portion of the second component; and heating the applied slurry to a temperature of 725° C. to 1450° C. for a predetermined period of time.

First claim

What is claimed:

1. A method for joining components to one another, comprising:
(a) providing a first component, wherein the first component includes ceramic, metal, or composite, and wherein the first component has an upper portion and a contoured lower portion;
(b) providing a second component, wherein the second component includes ceramic, metal, or composite, and wherein the second component has an upper portion and a lower portion, and wherein the upper portion is adapted to receive the contoured lower portion of the first component;
(c) providing a predetermined amount of Al—Si braze foil, wherein the Al—Si braze foil includes a first phase that melts at a first temperature, and a second phase interspersed throughout the first phase, and wherein the second phase melts at a second temperature that is lower than the melting temperature of the first phase;
(d) grinding the Al—Si braze foil into a powder;
(e) mixing a predetermined amount of braze paste binder with the Al—Si powder to form a slurry;
(f) uniformly applying the slurry to the lower portion of the first component;
(g) uniformly applying the slurry to the upper portion of the second component and bringing the upper portion of the second component into contact with the lower portion of the first component; and
(h) heating the applied slurry to a temperature in the range of 725° C. to 1450° C. for a predetermined period of time, wherein heating the applied slurry to a temperature in the range of 725° C. to 1450° C. for a predetermined period of time softens the first phase and melts the second phase, wherein the first phase remains in a solid or a semi-solid state, and wherein the second phase segregates to the boundaries of the first phase and transforms the applied slurry into a substantially porosity-free adherent material that joins the first component to the second component.

2. The method of claim 1 , wherein the first component is a silicon carbide ceramic-matrix composite.

3. The method of claim 1 , wherein the second component is a silicon carbide ceramic-matrix composite.

4. The method of claim 1 , wherein the first component is a silicon carbide plug.

5. The method of claim 1 , where in the second component is silicon carbide tube.

6. The method of claim 1 , wherein the first phase of the Al—Si braze foil includes silicon and the second phase of the Al—Si braze foil includes aluminum.

7. The method of claim 1 , wherein a mixing ratio of powder to binder is 56% powder to 44% binder.

8. A method for joining components to one another, comprising:
(a) providing a first component, wherein the first component includes ceramic, metal, or composite, and wherein the first component has an upper portion and a tapered lower portion;
(b) providing a second component, wherein the second component includes ceramic, metal, or composite, and wherein the second component has an upper portion that is adapted to receive the tapered lower portion of the first component;
(c) providing a predetermined amount of Al—Si braze foil, wherein the Al—Si braze foil includes a first phase that melts at a first temperature, and a second phase interspersed throughout the first phase, and wherein the second phase melts at a second temperature that is lower than the melting temperature of the first phase;
(d) grinding the Al—Si braze foil into a powder;
(e) mixing a predetermined amount of braze paste binder with the Al—Si powder to form a slurry;
(f) uniformly applying the slurry to the tapered lower portion of the first component;
(g) uniformly applying the slurry to the upper portion of the second component and inserting the tapered lower portion of the first component into the upper portion of the second component; and
(h) heating the applied slurry to a temperature in the range of 725° C. to 1450° C. for a predetermined period of time, wherein heating the applied slurry to a temperature in the range of 725° C. to 1450° C. for a predetermined period of time softens the first phase and melts the second phase, wherein the first phase remains in a solid or a semi-solid state, and wherein the second phase segregates to the boundaries of the first phase and transforms the applied slurry into a substantially porosity-free adherent material that joins the first component to the second component.

9. The method of claim 8 , wherein the first component is a silicon carbide ceramic-matrix composite.

10. The method of claim 8 , wherein the second component is a silicon carbide ceramic-matrix composite.

11. The method of claim 8 , wherein the first component is a silicon carbide plug.

12. The method of claim 8 , where in the second component is silicon carbide tube.

13. The method of claim 8 , wherein the first phase of the Al—Si braze foil includes silicon and the second phase of the Al—Si braze foil includes aluminum.

14. The method of claim 8 , wherein a mixing ratio of powder to binder is 56% powder to 44% binder.

15. A method for joining silicon carbide components to one another, comprising:
(a) providing a first component, wherein the first component includes silicon carbide, and wherein the first component has an upper portion and a tapered lower portion;
(b) providing a second component, wherein the second component includes silicon carbide, and wherein the second component has an upper portion that is adapted to receive the tapered lower portion of the first component;
(c) providing a predetermined amount of Al—Si braze foil, wherein the Al—Si braze foil includes a first phase that melts at a first temperature, and a second phase interspersed throughout the first phase, and wherein the second phase melts at a second temperature that is lower than the melting temperature of the first phase;
(d) grinding the Al—Si braze foil into a powder;
(e) mixing a predetermined amount of braze paste binder with the Al—Si powder to form a slurry;
(f) uniformly applying the slurry to the tapered lower portion of the first component;
(g) uniformly applying the slurry to the upper portion of the second component and inserting the tapered lower portion of the first component into the upper portion of the second component; and
(h) heating the applied slurry to a temperature in the range of 725° C. to 1450° C. for a predetermined period of time, wherein heating the applied slurry to a temperature in the range of 725° C. to 1450° C. for a predetermined period of time softens the first phase and melts the second phase, wherein the first phase remains in a solid or a semi-solid state, and wherein the second phase segregates to the boundaries of the first phase and transforms the applied slurry into a substantially porosity-free adherent material that joins the first component to the second component.

16. The method of claim 15 , wherein the first component is a silicon carbide plug.

17. The method of claim 15 , where in the second component is silicon carbide tube.

18. The method of claim 15 , wherein the first phase of the Al—Si braze foil includes silicon and the second phase of the Al—Si braze foil includes aluminum.

19. The method of claim 15 , wherein a mixing ratio of powder to binder is 56% powder to 44% binder.

20. The method of claim 15 , wherein the first and second components are adapted for use in a nuclear reactor.

Assignees

• Edison Welding Inst Inc

Inventors

• Sadek Alber
• Herderick Edward D
• Cooper Kirk E
• Ames Nathan D

Classifications

• C04B2237/595

  whereby the interlayer is continuous, but heterogeneous on macro-scale, e.g. one part of the interlayer being a joining material, another part being an electrode material · CPC title

• C04B35/565

  based on silicon carbide · CPC title

• C04B2237/59

  Aspects relating to the structure of the interlayer · CPC title

• C04B37/026

  consisting of metals or metal salts · CPC title

• C22C21/02

  with silicon as the next major constituent · CPC title