Sequential biaxial strain of semi-crystalline tubes

Patent metadata

Field	Value
Publication number	US-10207449-B2
Application number	US-201514748862-A
Country	US
Kind code	B2
Filing date	Jun 24, 2015
Priority date	Jun 24, 2014
Publication date	Feb 19, 2019
Grant date	Feb 19, 2019

Abstract

The present disclosure provides a processing method for a polymer material to create a medical device with improved mechanical properties. This method allows better tailoring of the material's mechanical properties, hence a device to withstand greater structural loads in vivo. The method comprises providing an extruded polymer tube having an initial diameter and an initial length along a longitudinal direction, and longitudinally, bi-directionally straining the extruded polymer tube in a mold from the initial length to an expanded or extended length. The mold comprises a plurality of stationary heating elements. After longitudinally straining the tube, it is radially expanding in the mold from the initial diameter to an expanded diameter.

First claim

The invention claimed is:

1. A method of processing a polymer, the method comprising:
heating an extruded polymer tube to a first temperature in a mold comprising a plurality of stationary heating elements, the first temperature being between a glass transition temperature and a cold crystallinity temperature of the polymer, the extruded polymer tube having an initial diameter, an initial length, and a lumen therethrough along a longitudinal direction, and longitudinally straining the extruded polymer tube from the initial length to an extended length; and
after the step of longitudinally straining an extruded polymer tube, radially expanding the extruded polymer tube in the mold wherein the extruded polymer tube is expanded from the initial diameter to an expanded diameter.

2. The method of claim 1 wherein the step of longitudinally straining an extruded polymer tube comprises straining the extruded polymer tube to the extended length being about 20 percent to about 200 percent greater than the initial length.

3. The method of claim 1 further comprising extruding a polymer material through a tubular die to define the extruded polymer tube before the step of longitudinally straining an extruded polymer tube.

4. The method of claim 3 further comprising disposing the extruded polymer tube into the mold before the step of longitudinally straining an extruded polymer tube.

5. The method of claim 4 wherein the step of disposing the extruded polymer tube comprises positioning the plurality of stationary heating elements circumferentially about the extruded polymer tube.

6. The method of claim 1 , wherein the step of heating the extruded polymer tube comprises heating the extruded polymer tube to the first temperature being between about 74° C. and about 90° C.

7. The method of claim 1 , wherein the step of heating the extruded polymer tube comprises heating the extruded polymer tube to the first temperature being about 90° C.

8. The method of claim 1 , further comprising cooling the extruded polymer tube to a second temperature after the step of longitudinally straining an extruded polymer tube and before the step of radially expanding the extruded polymer tube.

9. The method of claim 8 wherein the step of cooling the extruded polymer tube comprising cooling the extruded polymer tube to the second temperature being below the first temperature and above the glass transition temperature.

10. The method of claim 9 wherein the step of cooling the extruded polymer tube comprises cooling the extruded polymer tube to the second temperature being about 74° C.

11. The method of claim 1 further comprising pressurizing the lumen after the step of longitudinally straining an extruded polymer tube and before the step of radially expanding the extruded polymer tube, the step of pressurizing comprises increasing from a first pressure to a second pressure with a gas.

12. The method of claim 11 wherein the step of pressurizing the lumen comprises pressurizing the lumen from the first pressure being about atmospheric pressure to the second pressure being between about 2 bar and about 25 bar.

13. The method of claim 8 further comprising cooling the extruded polymer tube to a third temperature, defining a processed polymer tube, the step of cooling the extruded polymer tube being after the step of radially expanding an extruded polymer tube.

14. The method of claim 13 further comprising cutting the processed polymer tube to define a medical device.

15. The method of claim 1 wherein the step of radially expanding the extruded polymer tube comprising expanding the initial diameter about 100% to about 500% to the expanded diameter.

Assignees

• Cook Medical Technologies Llc

Inventors

• Klausen Kasper
• Løvdal Alexandra

Classifications

• B29C49/04 Primary

  Extrusion blow-moulding · CPC title

• A61L31/14

  Materials characterised by their function or physical properties {, e.g. injectable or lubricating compositions, shape-memory materials, surface modified materials} · CPC title

• B29C49/6472

  in several stages · CPC title

• A61M25/0054

  with regions for increasing flexibility · CPC title

• B29L2023/00

  Tubular articles (B29L2024/00 takes precedence {; catheters B29L2031/7542}) · CPC title