Method and apparatus for characterizing clathrate hydrate formation conditions employing microfluidic device
US-2016299047-A1 · Oct 13, 2016 · US
US10197487B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10197487-B2 |
| Application number | US-201715611497-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jun 1, 2017 |
| Priority date | Jun 3, 2016 |
| Publication date | Feb 5, 2019 |
| Grant date | Feb 5, 2019 |
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The systems and methods provided herein relate generally to the prevention of migration of condensate in a condensation particle counter between components designed to handle condensate (e.g. saturator, condenser, condensate reservoir) and components which may be damaged by the condensate (e.g. detection and flow control devices).
Opening claim text (preview).
We claim: 1. A condensation particle counter system comprising: an inlet for introducing a sample stream to be analyzed; a saturator for introducing a condensate into said sample stream; wherein said saturator is in fluid communication with a condensate reservoir; a condenser in fluid communication with said saturator for condensing said condensate onto particles contained in said sample stream; a particle counter in fluid communication with said condenser for detecting or characterizing said particles in said sample stream; and a valve positioned between said particle counter and said condenser for isolating said particle counter from said condenser, said saturator and said condensate reservoir. 2. The condensation particle counter system of claim 1 further comprising: a second valve positioned between said inlet and said saturator for isolating said inlet from said condenser, said saturator and said condensate reservoir. 3. The condensation particle counter system of claim 2 , wherein said valve and said second valve are configured to automatically close when no power is supplied to said particle counter or a vacuum pump, thereby isolating said particle counter and said inlet. 4. The condensation particle counter system of claim 2 , wherein said valve and said second valve are pinch valves. 5. The condensation particle counter system of claim 2 further comprising a flow control orifice positioned between said inlet and said saturator, wherein said second valve is positioned between said flow control orifice and said saturator and further isolates said flow control orifice from said condenser, said saturator and said condensate reservoir. 6. The condensation particle counter system of claim 1 , wherein said valve is configured to automatically close when no power is supplied to said particle counter or a vacuum pump, thereby isolating said particle counter. 7. The condensation particle counter system of claim 1 , wherein said valve is configured to automatically close when there is no sample fluid flow through said inlet. 8. The condensation particle counter system of claim 1 , wherein said valve is configured to automatically close when there is a change in an ambient temperature. 9. The condensation particle counter system of claim 1 , wherein said condensation particle counter is a scattered light particle counter, an emitted light particle counter or a transmission particle counter. 10. The condensation particle counter system of claim 1 , wherein said valve is a pinch valve. 11. The condensation particle counter system of claim 1 , wherein said condensate is water, methanol, ethanol, propanol, butanol, glycerol or a combination thereof. 12. The condensation particle counter system of claim 11 , wherein said condensate is glycerol. 13. A method for isolating condensate in a condensation particle counter comprising: providing a condensation particle counter comprising: an inlet with a flow control orifice; a saturator for introducing condensate in fluid communication with a condensate reservoir; a condenser for condensing said condensate onto particles; an particle counter for detecting and characterizing said particles; and isolating said saturator, said condenser and said condensate reservoir from said inlet and said particle counter, thereby preventing condensate from contaminating said particle counter or said flow control orifice; wherein said step of isolating said saturator, said condenser and said particle counter is performed by a first valve positioned between said saturator and said inlet and a second valve positioned between said condenser and said particle counter. 14. The method of claim 13 , wherein said first valve and said second valve are pinch valves. 15. The method of claim 13 , wherein said step of isolating is performed when the particle counter is not operational, when the particle counter is powered off, and/or there is no flow through said flow orifice. 16. The method of claim 13 , wherein said particle counter is an optical particle counter. 17. A condensation particle counter system comprising: an inlet with a flow control orifice for introducing a sample stream to be analyzed; a saturator for introducing a condensate into said sample stream; wherein said saturator is in fluid communication with a condensate reservoir; a condenser in fluid communication with said saturator for condensing said condensate onto particles contained in said sample stream; a particle counter in fluid communication with said condenser for detecting or characterizing said particles in said sample stream; a first valve positioned between said particle counter and said condenser for isolating said particle counter from said condenser, said saturator and said condensate reservoir; and a second valve positioned between said inlet and said saturator for isolating said flow control orifice from said condenser, said saturator and said condensate reservoir; wherein said first valve and said second valve are configured to automatically close when said particle counter is not operational, said particle counter is powered off and/or there is no flow through said flow orifice.
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