Method for granulating polymers and product produced by this method

Patent metadata

Field	Value
Publication number	US-10189970-B2
Application number	US-201314438137-A
Country	US
Kind code	B2
Filing date	Oct 23, 2013
Priority date	Oct 26, 2012
Publication date	Jan 29, 2019
Grant date	Jan 29, 2019

Abstract

A granulation method that can be used to obtain a polymer from “post-consumer” materials, and a motor vehicle part made from polymers produced by recycling used polymers.

First claim

What is claimed is:

1. A method for granulating polymers from ground post-consumer materials, wherein said method comprises a step of:
extracting dissolved salts and/or small unmelted clusters present within said polymers;
wherein said extracting step comprises the step of adding a fluid or mixture of fluids in an extruder which solubilizes said dissolved salts and/or small unmelted clusters or entrains them, at least one of said dissolved salts and/or small unmelted clusters so extracted being evacuated under atmospheric pressure or under vacuum during extrusion before passing into an extrusion head;
wherein said fluid is at least one of water or a mixture containing water, introduced into said extruder at a pressure greater than that present in said extruder;
wherein 60 g of water or more is added per kg of extruded material; and
wherein said method further comprises a step of granulating said polymers after passing through a die of said extrusion head;
wherein said method is used to extrude a polymer that is used for molding a part, that, after coating, has a maximum in the appearance areas of visible parts of 4 faults of type grains, craters, or particles, per m 2 , of size greater than 50 μm.

2. The method for granulating according to claim 1 , wherein said fluid is a mixture comprising at least one of liquid carbon dioxide, liquid nitrogen, acetone, alcohol.

3. The method for granulating according to claim 1 , wherein said fluid or said mixture of fluids is added last, including after any additives.

4. The method for granulating according to claim 3 , said fluid or said mixture of fluids being added in the second half of the length of the extruder, about two thirds of the way along said extruder.

5. The method for granulating according to claim 1 , wherein said polymers to be granulated are polyolefins, which are chosen from homopolymers or copolymers of olefins.

6. The method for granulating according to claim 2 , wherein said fluid or said mixture of fluids is added last, including after any additives.

7. The method for granulating according to claim 3 , wherein said polymers to be granulated are polyolefins which are chosen from homopolymers or copolymers of olefins.

8. The method for granulating according to claim 2 , wherein said polymers to be granulated are polyolefins which are chosen from homopolymers or copolymers of olefins.

9. The method for granulating according to claim 2 , wherein the alcohol is selected from methanol, ethanol and butanol.

10. The method for granulating according to claim 5 , wherein said polyolefin is polypropylene.

11. The method for granulating according to claim 7 , wherein said polyolefin is polypropylene.

12. The method for granulating according to claim 8 , wherein said polyolefin is polypropylene.

Assignees

• Viot Frederic
• Cassagnau Philippe
• Massardier Nageotte Valerie
• Melis Flavien
• Plastic Omnium Cie
• Inst Nat Sciences Appliquees Lyon
• Univ Claude Bernard Lyon
• Univ Jean Monnet Saint Etienne
• Centre Nat Rech Scient

Inventors

• Viot Frederic
• Cassagnau Philippe
• Massardier-Nageotte Valérie
• Melis Flavien

Classifications

• B29K2105/26

  Scrap {or recycled material} · CPC title

• C08J11/08

  using selective solvents for polymer components · CPC title

• B29B9/16

  Auxiliary treatment of granules · CPC title

• B29C48/395

  using screws surrounded by a cooperating barrel, e.g. single screw extruders · CPC title

• C08J2300/30

  Polymeric waste or recycled polymer · CPC title