Crossflow tray for a mass transfer column, mass transfer column and use of the mass transfer column

Patent metadata

Field	Value
Publication number	US-10183234-B2
Application number	US-201615072463-A
Country	US
Kind code	B2
Filing date	Mar 17, 2016
Priority date	Mar 18, 2015
Publication date	Jan 22, 2019
Grant date	Jan 22, 2019

Abstract

The invention relates to a crossflow tray for a mass transfer column ( 27 ) in which a gas is conducted in countercurrent to a liquid, the crossflow tray ( 1 ) having passage orifices ( 3 ) for the gas and at least two downcomers ( 5 ), the downcomers ( 5 ) projecting beyond the top surface of the crossflow tray ( 1 ) and a collecting cup ( 13 ) being disposed beneath each downcomer ( 5 ). The downcomer ( 5 ) projects into the collecting cup ( 13 ), the minimum horizontal cross-sectional area of the collecting cup ( 13 ) is 1.2 to 4 times greater than the horizontal cross-sectional area of the downcomer ( 5 ) at the outlet, and the collecting cup ( 13 ) has a circumferential wall ( 15 ) having an overflow ( 19 ).
The invention further relates to a mass transfer column comprising the crossflow trays and to a use of the mass transfer column.

First claim

The invention claimed is:

1. A crossflow tray for a mass transfer column in which a gas is conducted in countercurrent to a liquid, the crossflow tray having passage orifices for the gas and at least two downcomers, the downcomers projecting beyond the top surface of the crossflow tray and a collecting cup being disposed beneath each downcomer wherein the downcomer projects into the collecting cup, the minimum horizontal cross-sectional area of the collecting cup being 1.2 to 4times greater than the horizontal cross-sectional area of the downcomer at the outlet, and where the collecting cup has a circumferential wall having an overflow, the overflow being disposed only on the side of the collecting cup facing away from the shell of the mass transfer column.

2. The crossflow tray according to claim 1 , wherein the circumferential wall of the collecting cup forms the overflow by having a lower height in the region of the overflow.

3. The crossflow tray according to claim 1 , wherein the circumferential wall runs at right angles to the base of the collecting cup.

4. The crossflow tray according to claim 1 , wherein the downcomer has a cross-sectional constriction, such that the horizontal cross-sectional area of the downcomer at the inlet is greater than the horizontal cross-sectional area at the outlet.

5. The crossflow tray according to claim 4 , wherein a ratio of the horizontal cross-sectional area at the inlet to the horizontal cross-sectional area at the outlet is in the range from 1:1 to 4:1.

6. The crossflow tray according to claim 1 , wherein the downcomer is formed symmetrically with respect to a plane of symmetry that runs vertically in the middle of the downcomer.

7. The crossflow tray according to claim 4 , wherein the walls of the downcomer that run parallel to the plane of symmetry have a region in which the wall runs at an angle of inclination between 10 and 80°with respect to the vertical, in order to form the cross-sectional constriction.

8. The crossflow tray according to claim 7 , wherein the wall of the downcomer runs vertically above and below the region inclined with respect to the vertical.

9. The crossflow tray according to claim 1 , wherein all the downcomers are positioned such that the distance between the wall of the downcomer that projects through the crossflow tray and the outer edge of the crossflow tray is at least sufficiently great at every point that at least one passage orifice can be formed in the crossflow tray.

10. A mass transfer column for conducting a mass transfer operation, comprising at least two crossflow trays according to claim 1 .

11. The mass transfer column according to claim 10 , wherein all the downcomers of a crossflow tray are disposed in the same half of the crossflow tray and every two superposed crossflow trays are arranged such that the downcomers of the upper crossflow tray end above the half of the lower crossflow tray in which there are no downcomers.

12. A method for thermal separation of a mixture comprising (meth)acrylic monomers conducted in the mass transfer column according to claim 10 , comprising:
passing a liquid and a gas stream in countercurrent through the mass transfer column wherein the (meth)acrylic monomers are present either in the gas stream or in the liquid.

13. The method according to claim 12 , wherein the thermal separation process is a condensation when the (meth)acrylic monomers are present in the gas stream and a rectification when the (meth)acrylic monomers are present in the liquid.

Assignees

• Basf Se

Inventors

• Blaschke Tim
• Cremer Ulrich
• Hammon Ulrich

Classifications

• B01D3/225

  Dual-flow sieve trays · CPC title

• B01F3/04496

  Operations & Transport · mapped topic

• B01F3/04468

  Operations & Transport · mapped topic

• C07C67/48

  Separation; Purification; Stabilisation; Use of additives · CPC title

• C07C51/42

  Separation; Purification; Stabilisation; Use of additives · CPC title