Device for polymerising lactams in moulds

Patent metadata

Field	Value
Publication number	US-10179429-B2
Application number	US-201315101326-A
Country	US
Kind code	B2
Filing date	Dec 3, 2013
Priority date	Dec 3, 2013
Publication date	Jan 15, 2019
Grant date	Jan 15, 2019

Abstract

A device for polymerizing lactams in molds includes a hopper for storing solid lactam and a lactam feeding component that includes a plasticizing screw so as the lactam to be melted and simultaneously taken in a dosed manner to a mixing chamber. The device further includes a first dosing component to feed a liquid initiator, and a second dosing component to feed a liquid activator. The mixing chamber is configured to receive in a dosed manner the lactam, the initiator, and the activator from the feeding and dosing components. The mixing chamber has three separate inlets to receive, separately, the lactam, the initiator, and the activator, to allow them to flow into the mixing chamber coming into contact with one another for the first time, at the moment immediately prior to entering into a mold located adjacent the chamber and arranged for the polymerization reaction to take place inside the mold.

First claim

The invention claimed is:

1. A device for polymerizing lactams in molds, comprising:
a hopper for storing solid lactam;
a lactam feeding means configured to receive the solid lactam from the hopper, wherein said lactam feeding means comprises a plasticizing screw configured to melt the lactam and simultaneously drive the molten lactam in a dosed manner towards a mixing chamber, the plasticizing screw dosing the molten lactam into the mixing chamber in a continuous way;
the device further includes:
a first dosing means for feeding a liquid initiator;
a second dosing means for feeding a liquid activator;
wherein said mixing chamber is configured to receive in a dosed manner the lactam, the initiator and the activator, from respectively said lactam feeding means, said first dosing means and said second dosing means, said mixing chamber having three separate inlets for receiving, separately, the lactam, the initiator, and the activator, so as to allow the lactam, the initiator, and the activator respectively to flow into the mixing chamber, coming into contact with one another for the first time at the moment immediately prior to entering a mold located next to the chamber and arranged for the polymerization reaction to take place inside the mold.

2. The device according to claim 1 , wherein the first dosing means for feeding the initiator, comprises a syringe propeller attached to the first inlet of the mixing chamber and the second dosing means for feeding the activator, comprises a syringe propeller attached to the second inlet of the mixing chamber.

3. The device according to claim 1 , wherein said lactam feeding means comprises means for controlling the lactam dose accessing the mixing chamber by controlling the rotation of the plasticizing screw.

4. The device according to claim 1 , wherein said plasticizing screw is surrounded by heating means.

5. The device according to claim 1 , wherein the lactam feeding means is a extruder configured for melting the lactam in said plasticizing screw and taking the lactam towards said mixing chamber.

6. The device according to claim 1 , which further comprises a nozzle arranged between the mixing chamber and the mold, being said nozzle configured to receive the mixture formed by the lactam, the initiator and the activator in a dosed manner and to deliver said mixture to the mold.

7. The device of claim 5 , wherein said extruder is inclined relative to the horizontal at an angle ranging between 10 and 35 degrees.

8. The device of claim 5 , wherein the mixing chamber comprises a pumping system configured for pumping the dose of the lactam, initiator and activator mixture in a substantially continuous manner.

9. The device of claim 8 , wherein said pumping system is a piston pump.

10. The device according to claim 6 , wherein the mixing chamber has an outlet and is configured such that at the outlet, the initiator and the activator come out through the central portion of the section of said chamber, whereas the lactam flow comes out through the perimetrical portion such that the lactam is disposed in the nozzle where the three components come into contact for the first time.

11. The device according to claim 1 , wherein the lactam feeding means is an injector configured to melt the lactam in said plasticizing screw, to take the lactam towards said mixing chamber in a dosed manner and by means of the same plasticizing screw used as an plunger, to push the lactam, the initiator and the catalyst mixture through a nozzle towards the mold.

Assignees

• Fundacion Tecnalia Res & Innovation

Inventors

• De La Calle Lizarazu Amaia
• Elizetxea Ezeiza Cristina
• García Arrieta Sonia

Classifications

• B29K2105/0067

  Melt · CPC title

• B29K2077/00

  Use of {PA, i.e.} polyamides, e.g. polyesteramides {or derivatives thereof}, as moulding material · CPC title

• B29C67/246

  Moulding high reactive monomers or prepolymers, e.g. by reaction injection moulding [RIM], liquid injection moulding [LIM] (casting monomers B29C39/006, mixing construction B29B7/74) · CPC title

• B29C45/00

  Injection moulding, i.e. forcing the required volume of moulding material through a nozzle into a closed mould; Apparatus therefor (injection blow-moulding B29C49/06) · CPC title

• B29K2867/046

  PLA, i.e., polyactic acid or polyactide · CPC title