Method for analyzing molecular weight of the poly-p-phenylene terephthalamide

US10161862B2 · US · B2

Patent metadata
FieldValue
Publication numberUS-10161862-B2
Application numberUS-201615318667-A
CountryUS
Kind codeB2
Filing dateApr 7, 2016
Priority dateMar 15, 2016
Publication dateDec 25, 2018
Grant dateDec 25, 2018

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  1. Title

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Abstract

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A method for analyzing molecular weight of the poly-p-phenylene terephthalamide (PPTA) utilizing near infrared spectrum is provided for reducing the time required to analyze the molecular weight of PPTA. The method uses PPTA samples to build a spectrum-viscosity fitting curve. The molecular weight of an unknown PPTA is analyzed via a near infrared analysis software and the spectrum-viscosity fitting curve. The method is beneficial in that it has a short process time and high reliability.

First claim

Opening claim text (preview).

What is claimed is: 1. A method for analyzing molecular weight of the poly-p-phenylene terephthalamide (PPTA) utilizing near infrared spectrum, comprising the following steps: (a) preparing 60˜90PPTA samples with different molecular weight, wherein the viscosity of said PPTA samples ranges from 1 to 9 dL/g; (b) dissolving respectively said PPTA samples in a concentrated sulfuric acid and detecting the viscosity thereof by an Ubbelohde viscometer; (c) scanning respectively each of said PPTA samples 1˜10 times using a near infrared spectrometer to obtain corresponding spectral data thereof, and calculating an average spectral data of said spectral values; (d) extrapolating a spectrum data-viscosity fitting curve from said viscosity data of step (b) and said spectrum data of the step (c) via a near infrared analysis software; and (e) scanning an unknown PPTA resin using said near infrared spectrometer to obtain a near infrared spectrum data and calculating the viscosity of said unknown PPTA by said spectrum-viscosity fitting curve.

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Classifications

  • from aromatic diamines and aromatic dicarboxylic acids with both amino and carboxylic groups aromatically bound · CPC title

  • G01N21/359Primary

    using near infrared light · CPC title

  • Resins; Plastics · CPC title

  • by measuring flow of the material · CPC title

  • for analysing solids; Preparation of samples therefor · CPC title

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What does patent US10161862B2 cover?
A method for analyzing molecular weight of the poly-p-phenylene terephthalamide (PPTA) utilizing near infrared spectrum is provided for reducing the time required to analyze the molecular weight of PPTA. The method uses PPTA samples to build a spectrum-viscosity fitting curve. The molecular weight of an unknown PPTA is analyzed via a near infrared analysis software and the spectrum-viscosity fi…
Who is the assignee on this patent?
Shandong Wanshengbo Sci Tech Co Ltd, Univ Tsinghua, Shngdong Wanshengbo Sci Tech Co Ltd
What technology area does this patent fall under?
Primary CPC classification G01N21/359. Mapped technology areas include Physics.
When was this patent published?
Publication date Tue Dec 25 2018 00:00:00 GMT+0000 (Coordinated Universal Time) (B2). Legal status and post-grant events are not shown on this page.
What related patents are in patentsdb?
We list 8 related publications on this page (citations in our corpus or others sharing the same primary CPC).