Estimating molecular weight of hydrocarbons
US-12140585-B2 · Nov 12, 2024 · US
US10161862B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10161862-B2 |
| Application number | US-201615318667-A |
| Country | US |
| Kind code | B2 |
| Filing date | Apr 7, 2016 |
| Priority date | Mar 15, 2016 |
| Publication date | Dec 25, 2018 |
| Grant date | Dec 25, 2018 |
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A method for analyzing molecular weight of the poly-p-phenylene terephthalamide (PPTA) utilizing near infrared spectrum is provided for reducing the time required to analyze the molecular weight of PPTA. The method uses PPTA samples to build a spectrum-viscosity fitting curve. The molecular weight of an unknown PPTA is analyzed via a near infrared analysis software and the spectrum-viscosity fitting curve. The method is beneficial in that it has a short process time and high reliability.
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What is claimed is: 1. A method for analyzing molecular weight of the poly-p-phenylene terephthalamide (PPTA) utilizing near infrared spectrum, comprising the following steps: (a) preparing 60˜90PPTA samples with different molecular weight, wherein the viscosity of said PPTA samples ranges from 1 to 9 dL/g; (b) dissolving respectively said PPTA samples in a concentrated sulfuric acid and detecting the viscosity thereof by an Ubbelohde viscometer; (c) scanning respectively each of said PPTA samples 1˜10 times using a near infrared spectrometer to obtain corresponding spectral data thereof, and calculating an average spectral data of said spectral values; (d) extrapolating a spectrum data-viscosity fitting curve from said viscosity data of step (b) and said spectrum data of the step (c) via a near infrared analysis software; and (e) scanning an unknown PPTA resin using said near infrared spectrometer to obtain a near infrared spectrum data and calculating the viscosity of said unknown PPTA by said spectrum-viscosity fitting curve.
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