Nano-level evaluation of kerogen-rich reservoir rock

Patent metadata

Field	Value
Publication number	US-10151715-B2
Application number	US-201815916027-A
Country	US
Kind code	B2
Filing date	Mar 8, 2018
Priority date	Sep 3, 2015
Publication date	Dec 11, 2018
Grant date	Dec 11, 2018

Abstract

Nano-level evaluation of kerogen-rich reservoir rock is described. A nano-scale beam is formed from kerogen-rich reservoir rock. The nano-scale beam includes reservoir rock and kerogen having polymeric properties. A maximum dimension of the nano-scale beam is at least 100 nanometer (nm) and at most 1000 nm. A tension test is performed on the nano-scale beam. The tension test is imaged using a transmission electron microscope (TEM). A material parameter of the kerogen in the nano-scale beam is determined based on results of the tension test and images obtained responsive to the imaging.

First claim

The invention claimed is:

1. A method comprising:
forming a nano-scale beam from kerogen-rich reservoir rock, the nano-scale beam comprising reservoir rock and kerogen having polymeric properties, wherein a maximum dimension of the nano-scale beam is at least 100 nanometer (nm) and at most 1000 nm;
performing a tension test on the nano-scale beam;
imaging the tension test using a transmission electron microscope (TEM), wherein the tension test is a cantilever test;
determining a material parameter of the kerogen in the nano-scale beam based on results of the tension test and images obtained responsive to the imaging; and
applying heat to the nano-scale beam while performing the cantilever test.

2. The method of claim 1 , wherein the material parameter of the kerogen in the nano-scale beam comprises a tensile strength of the nano-scale beam.

3. The method of claim 1 , wherein performing the cantilever test comprises applying a force of the order of micro-Newtons on a free-end of the nano-scale beam, wherein determining the material parameter comprises measuring a bending of the cantilever responsive to force.

4. The method of claim 3 , further comprising applying the force at a rate of displacement of substantially between 1 nm/s to 100 nm/s.

5. The method of claim 3 , further comprising applying the load until the nano-scale beam fails.

6. The method of claim 1 , wherein the force is a cantilever force applied using a nano-indenter, wherein performing the cantilever test comprises:
applying the heat to the nano-indenter; and
applying the cantilever force using the nano-indenter while applying heat to the nano-indenter.

7. The method of claim 6 , wherein applying heat to the nano-scale beam comprises applying the heat directly to the nano-scale beam and to the nano-indenter.

8. The method of claim 1 , further comprising determining an effect of the heat applied to the nano-scale beam on the material parameter of the kerogen in the nano-scale beam.

9. The method of claim 8 , further comprising determining a mechanical property profile of the kerogen-rich reservoir rock based on the effect of the heat applied to the nano-scale beam.

10. The method of claim 1 , wherein the nano-scale beam comprises a plurality of stacked shale bedding planes, wherein the tension test is performed either parallel to or perpendicular to the plurality of stacked shale bedding planes.

11. The method of claim 10 , wherein performing the tension test parallel to the plurality of stacked shale bedding planes comprises applying tension in a direction that is perpendicular to a direction in which the plurality of stacked shale bedding planes are stacked.

12. The method of claim 10 , wherein performing the tension test perpendicular to the plurality of stacked shale bedding planes comprises applying tension in a direction that is parallel to a direction in which the plurality of stacked shale bedding planes are stacked.

Assignees

• Saudi Arabian Oil Co

Inventors

• Hull Katherine Leigh
• Abousleiman Younane N

Classifications

• G01N3/08

  by applying steady tensile or compressive forces (G01N3/28 takes precedence) · CPC title

• G01N23/20025 Primary

  Sample holders or supports therefor · CPC title

• G01N33/24 Primary

  Earth materials (G01N33/42 takes precedence) · CPC title

• E21B49/00

  Testing the nature of borehole walls; Formation testing; Methods or apparatus for obtaining samples of soil or well fluids, specially adapted to earth drilling or wells · CPC title

• G01N2203/0647

  Image analysis · CPC title