Sampler and sampling method for molten material

Patent metadata

Field	Value
Publication number	US-10151669-B2
Application number	US-201615258478-A
Country	US
Kind code	B2
Filing date	Sep 7, 2016
Priority date	Apr 30, 2013
Publication date	Dec 11, 2018
Grant date	Dec 11, 2018

Abstract

A sampler has a sample chamber for a sample forming from a molten material, at least one lower cooling body, at least one upper cooling body, at least one inner cooling body, and at least one filling part. The sample chamber is surrounded jointly at least by the lower cooling body and the inner cooling body, such that at least the sample chamber can be cooled by at least the lower and inner cooling bodies. The filling part merges into the sample chamber by a filling opening. Between a region of the outer surface of the inner cooling body and a region of the outer surface of the upper cooling body opposite the outer surface of the inner cooling body, the sampler has at least one gap for conducting at least one gas. The volume of the respective cooling bodies is larger than the volume of the gap.

First claim

We claim:

1. A sampler ( 1 , 1 a ) comprising:
a sample chamber ( 2 ) for a sample ( 3 ) forming from a molten material;
at least one lower cooling body ( 6 );
at least one upper cooling body ( 8 );
at least one inner cooling body ( 7 ); and
at least one filling part,
wherein the sample chamber ( 2 ) is surrounded jointly at least by the at least one lower cooling body ( 6 ) and the at least one inner cooling body ( 7 ), such that at least the sample chamber ( 2 ) can be cooled by at least the at least one lower cooling body and the at least one inner cooling body,
wherein the at least one filling part is connected to the sample chamber ( 2 ) and merges into the sample chamber ( 2 ) by a filling opening ( 5 a ),
wherein each of the at least one lower cooling body, the at least one upper cooling body and the at least one inner cooling body comprises an outer surface ( 7 a , 8 a ), and
wherein the sampler ( 1 , 1 a ) comprises, between a region of the outer surface ( 7 a ) of the at least one inner cooling body ( 7 ) and a region of the outer surface ( 8 a ) of the at least one upper cooling body ( 8 ) opposite to the outer surface ( 7 a ) of the at least one inner cooling body ( 7 ), at least one gap ( 11 ) for conducting at least one gas, a volume of the respective cooling bodies ( 6 , 7 , 8 ) being larger than a volume of the at least one gap ( 11 ).

2. The sampler ( 1 , 1 a ) according to claim 1 , wherein at least the at least one lower cooling body ( 6 ) and the at least one inner cooling body ( 7 ) form a wall of the sample chamber ( 2 ), wherein the wall is formed by a region of the respective outer surface of the at least one lower cooling body ( 6 ) and of the at least one inner cooling body ( 7 ), such that the sample chamber ( 2 ) comprises a hollow space formed between the at least one lower cooling body ( 6 ) and the at least one inner cooling body ( 7 ).

3. The sampler ( 1 , 1 a ) according to claim 1 , wherein at least one of the at least one lower cooling body, the at least one upper cooling body and the at least one inner cooling body comprises at least one ventilation opening ( 16 ).

4. The sampler ( 1 , 1 a ) according to claim 3 , wherein the at least one ventilation opening ( 16 ) is closed by at least one closure, optionally a membrane ( 17 ), which can be opened while or after the sample chamber ( 2 ) is being filled with the molten material.

5. The sampler ( 1 , 1 a ) according to claim 4 , wherein the at least one closure comprises at least one plastic connection.

6. The sampler ( 1 , 1 a ) according to claim 4 , wherein the at least one closure has a pressure resistance of approximately 0.5 bar to approximately 4 bar.

7. The sampler ( 1 , 1 a ) according to claim 4 , wherein the at least one closure has a temperature resistance of approximately 50° C. to approximately 90° C.

8. The sampler ( 1 , 1 a ) according to claim 3 , wherein a diameter of the at least one ventilation opening ( 16 ) is approximately 0.7 mm to approximately 1.3 mm.

9. A method for sampling from molten material having a melting temperature of more than 600° C., the method comprising positioning the sampler according to claim 1 at one end of at least one of a lance and a carrier part and immersing the sampler into the molten material, subsequently filling the sample chamber of the sampler with molten material, and then pulling at least the sample out of the molten material by the sampler, wherein the at least one gas is supplied into the sampler before immersing the sampler, wherein the at least one gas flows out again from the sampler through the at least one filling part, the sampler is subsequently immersed into the molten material, the supply of gas is then changed, followed by the sample chamber filling up with molten material, and gas is then supplied again into the sampler during or after the sample chamber fills with molten material, such that at least the sample chamber is cooled by the supplied gas.

10. The method according to claim 9 , wherein the at least one gas flows through the at least one gap between at least the at least one inner cooling body and the at least one upper cooling body.

11. The method according to claim 9 , wherein the sample is held by the at least one lower cooling body.

12. The method according to claim 9 , wherein the sample is supplied to an analytical facility while it is in the sampler.

13. The method according to claim 9 , wherein the at least one inner cooling body is held by the at least one upper cooling body.

14. The method according to claim 9 , wherein the at least one gas flows out only through the at least one filling part before the molten material fills into the sample chamber, and the at least one gas flows out through at least one ventilation opening while or after the molten material fills into the sample chamber.

15. The method according to claim 14 , wherein the at least one gas flowing out through the at least one ventilation opening is discharged through at least one gas exit opening for discharging the supplied gas from the sampler.

16. The method according to claim 14 , wherein the at least one ventilation opening is closed by at least one closure, and wherein the at least one closure becomes permeable to gas while or after the molten material is filled into the sample chamber, by at least one of the temperature of the molten material and the pressure of the supplied gas.

17. The method according to claim 14 , wherein, after filling the sample chamber with molten material, the newly supplied gas flows through the at least one gap and then flows through the at least one ventilation opening out of the sampler, wherein this cools down the temperature of the sample.

Assignees

• Heraeus Electro Nite Int

Inventors

• Cappa Guido
• Broekmans Gerrit

Classifications

• G01N1/1409

  adapted for sampling molten metals · CPC title

• B01L2300/0681

  Filter · CPC title

• B01L3/502

  with fluid transport, e.g. in multi-compartment structures · CPC title

• B01L2400/0463

  Hydrodynamic forces, venturi nozzles · CPC title

• Y10S73/09

  Molten metal samplers · CPC title