Systems and methods for non-flammable indication of incendivity

Patent metadata

Field	Value
Publication number	US-10145834-B2
Application number	US-201615214214-A
Country	US
Kind code	B2
Filing date	Jul 19, 2016
Priority date	Jul 19, 2016
Publication date	Dec 4, 2018
Grant date	Dec 4, 2018

Abstract

Incendivity test systems and methods are disclosed. Incendivity test systems include a non-flammable gas mixture and a test article in a test chamber. The non-flammable gas mixture includes a thermally reactive reagent that is formulated to thermally react to produce a reaction product. Incendivity test systems also include an energy source configured to apply an energy discharge such as a simulated lightning strike to the test article. Incendivity test systems also include a detection device configured to measure an indicator species in the non-flammable gas mixture (e.g., the thermally reactive reagent and/or the reaction product). Incendivity test methods include contacting the test article with the non-flammable gas mixture, applying the energy discharge to the test article, and then measuring the amount of the indicator species and determining the incendivity of the test article in response to the energy discharge based upon the amount of the indicator species.

First claim

The invention claimed is:

1. An incendivity test method comprising:
contacting a test article with a non-flammable gas mixture in a test chamber, wherein the non-flammable gas mixture includes a thermally reactive reagent;
applying an energy discharge to the test article while the test article is in contact with the non-flammable gas mixture;
after applying the energy discharge, measuring an amount of one or more components of the non-flammable gas mixture that represents an amount of the thermally reactive reagent that reacted in response to applying the energy discharge; and
determining an incendivity of the test article in response to the energy discharge based upon the amount of the thermally reactive reagent that reacted in response to applying the energy discharge.

2. The method of claim 1 , wherein the non-flammable gas mixture is a mixture that is too lean to support self-propagating combustion of the thermally reactive reagent.

3. The method of claim 1 , wherein the applying the energy discharge includes applying a simulated lightning strike to the test article.

4. The method of claim 1 , wherein the energy discharge has a peak power of greater than 1 kW (kilowatt).

5. The method of claim 1 , wherein the measuring includes measuring an amount of a reaction product produced by thermal reaction of the thermally reactive reagent after applying the energy discharge.

6. The method of claim 1 , wherein the measuring includes measuring by a gas analysis technique selected from the group consisting of mass spectrometry, gas chromatography, and gas chromatography mass spectrometry.

7. The method of claim 1 , wherein the measuring includes measuring by an optical technique selected from the group consisting of optical spectrometry, optical absorbance, optical transmittance, optical reflectance, nephelometry, luminescence, fluorescence, phosphorescence, laser induced fluorescence, planar laser induced fluorescence, laser excited atomic fluorescence, and Fourier transform infrared spectrometry.

8. The method of claim 1 , wherein the non-flammable gas mixture includes a plurality of thermally reactive reagents, wherein each of the thermally reactive reagents is configured to react in response to a different ignition source to produce a corresponding reaction product.

9. The method of claim 1 , wherein the thermally reactive reagent is a combustion fuel.

10. The method of claim 1 , wherein the thermally reactive reagent is configured to thermally decompose.

11. The method of claim 1 , wherein the thermally reactive reagent is a halocarbon.

12. An incendivity test method comprising:
contacting a test article with a non-flammable gas mixture that includes a thermally reactive reagent;
applying a simulated lightning strike to the test article while the test article is in contact with the non-flammable gas mixture;
after applying the simulated lightning strike, measuring an amount of one or more components of the non-flammable gas mixture that represents an amount of the thermally reactive reagent that reacted in response to applying the simulated lightning strike; and
determining an incendivity of the test article in response to the simulated lightning strike based upon the amount of the thermally reactive reagent that reacted in response to applying the lightning strike.

13. The method of claim 12 , wherein the contacting includes immersing the test article in the non-flammable gas mixture by flowing a stream of the non-flammable gas mixture over the test article.

14. The method of claim 12 , wherein the non-flammable gas mixture is a mixture that is too lean to support self-propagating combustion of the thermally reactive reagent.

15. The method of claim 12 , wherein the thermally reactive reagent is a halocarbon.

16. The method of claim 12 , further comprising preparing the non-flammable gas mixture by mixing the thermally reactive reagent with one or more of an oxidant, a diluent, and another thermally reactive reagent.

17. An incendivity test system comprising:
a test chamber;
a non-flammable gas mixture in the test chamber, wherein the non-flammable gas mixture includes a thermally reactive reagent that is formulated to thermally react to produce a reaction product;
a test article in the test chamber in contact with the non-flammable gas mixture;
an energy source configured to apply an energy discharge to the test article; and
a detection device configured to measure an amount of one or more indicator species selected from the group consisting of a component of the non-flammable gas mixture and the reaction product.

18. The system of claim 17 , wherein the detection device selected from the group consisting of a mass spectrometer, a gas chromatograph, a gas chromatography mass spectrometer, an optical spectrometer, a fluorescence spectrometer, a laser-induced fluorescence apparatus, a planar laser-induced fluorescence apparatus, a laser excited atomic fluorescence apparatus, and a Fourier transform infrared spectrometer.

19. The system of claim 17 , wherein the energy source is a lightning strike simulator.

20. The system of claim 17 , wherein the thermally reactive reagent is a halocarbon.

Assignees

• Boeing Co

Inventors

• Damazo Jason Scott
• Kwon Eddie
• Robb Andrew Michael

Classifications

• G01N25/52 Primary

  by determining flash-point of liquids · CPC title

• G01N31/12

  using combustion (G01N25/20 takes precedence) · CPC title

• G01N25/46

  for investigating the composition of gas mixtures · CPC title

• Y10T436/24

  Nuclear magnetic resonance, electron spin resonance or other spin effects or mass spectrometry · CPC title

• Y10T436/196666

  Carbon containing compound [e.g., vinylchloride, etc.] · CPC title