Apparatus for purifying material of biological origin

Patent metadata

Field	Value
Publication number	US-10144889-B2
Application number	US-201514877161-A
Country	US
Kind code	B2
Filing date	Oct 7, 2015
Priority date	Nov 26, 2010
Publication date	Dec 4, 2018
Grant date	Dec 4, 2018

Abstract

The present invention relates to a process and an apparatus for purifying tall oil material for the production of biofuels and components thereof. The present invention relates further to hydroprocessing of the purified material to obtain biofuels and components thereof.

First claim

The invention claimed is:

1. An apparatus for purifying tall oil material, characterized in that the apparatus comprises three sequentially arranged evaporators ( 10 , 16 , 20 ) wherein
the first evaporator ( 10 ) is arranged to evaporate said tall oil material to produce a first fraction comprising hydrocarbons having a boiling point of up to 250° C. at normal pressure and water and a second fraction comprising fatty acids, resin acids, neutral substances and residue components,
the second evaporator ( 16 ) is arranged to evaporate said second fraction and to produce a liquid fraction, and
the third evaporator ( 20 ) is arranged to evaporate the liquid fraction and to produce a third fraction comprising fatty acids, resin acids and neutral substances having a boiling point under 500° C. at normal pressure and a residue fraction,
a first connection ( 14 ) arranged to feed the second fraction to the second evaporator ( 16 ),
a further connections ( 19 ) between said second evaporators ( 16 ) and said third evaporator ( 20 ), and
a residue outlet ( 22 ) for recovering the residue fraction from the third evaporator ( 20 ).

2. The apparatus according to claim 1 , characterized in that the apparatus further comprises a first product outlet ( 12 ) for recovering the first fraction comprising hydrocarbons having a boiling point of up to 250° C. at normal pressure and water from the first evaporator ( 10 ), a second product outlet ( 18 ) for recovering the third fraction from said third evaporator ( 20 ).

3. The apparatus according to claim 1 , characterized in that the apparatus further comprises one or more first feed inlets ( 8 ) arranged to feed the tall oil material to said first evaporator ( 10 ).

4. The apparatus according to claim 1 , characterized in that the evaporators ( 10 , 16 , 20 ) are selected from the group consisting of evaporators using thin film evaporation technology.

5. The apparatus according to claim 4 , characterized in that the evaporators are selected from the group consisting of thin film evaporator, falling film evaporator, short path evaporator and plate molecular still.

6. The apparatus according to claim 1 , characterized in that the apparatus further comprises at least one catalytic hydroconversion unit (C 1 , C 2 ) for converting the hydrocarbons having a boiling point of up to 250° C. at normal pressure of the first fraction to one more biofuels or components thereof selected from the group consisting of gasoline, naphtha, jet fuel, diesel and fuel gases and/or for converting the third fraction comprising fatty acids, resin acids and neutral substances having a boiling point under 500° C. at normal pressure to one or more biofuels or components thereof selected from diesel, jet fuel, gasoline, naphtha and fuel gases.

Assignees

• Upm Kymmene Corp

Inventors

• Nousiainen Jaakko
• Laumola Heli
• Rissanen Arto
• Kotoneva Jari
• Ristolainen Matti

Classifications

• C10L2270/026

  for diesel engines, e.g. automobiles, stationary, marine · CPC title

• C10L2200/0469

  Renewables or materials of biological origin · CPC title

• C10L2270/023

  for gasoline engines · CPC title

• B01D3/14

  Fractional distillation {or use of a fractionation or rectification column} · CPC title

• C10G2400/04

  Diesel oil · CPC title