Polycrystalline diamond constructions having improved thermal stability

Patent metadata

Field	Value
Publication number	US-10132121-B2
Application number	US-201113085089-A
Country	US
Kind code	B2
Filing date	Apr 12, 2011
Priority date	Mar 21, 2007
Publication date	Nov 20, 2018
Grant date	Nov 20, 2018

Abstract

A method for making a polycrystalline diamond construction is disclosed, which includes the steps of treating a polycrystalline diamond body having a plurality of bonded together diamond crystals and a solvent catalyst material to remove the solvent catalyst material therefrom, wherein the solvent catalyst material is disposed within interstitial regions between the bonded together diamond crystals, replacing the removed solvent catalyst material with a replacement material, and treating the body having the replacement material to remove substantially all of the replacement material from a first region of the body extending a depth from a body surface, and allowing the remaining amount of the replacement material to reside in a second region of the body that is remote from the surface.

First claim

What is claimed is:

1. A method for making a polycrystalline diamond construction comprising the steps of:
treating a polycrystalline diamond body comprising a plurality of bonded together diamond crystals and a solvent catalyst material to remove substantially all of the solvent catalyst material therefrom, wherein the solvent catalyst material is disposed within interstitial regions between the bonded together diamond crystals;
replacing substantially all of the removed solvent catalyst material with a replacement material not initially used to form the diamond body, wherein the replacement material fills the interstitial regions; and
treating the body comprising the replacement material to remove substantially all of the replacement material from a first region of the body extending a depth from a body surface, wherein the depth is greater than about 0.05 mm from the surface, and allowing the remaining amount of the replacement material to reside in a second region of the body that is remote from the surface.

2. The method as recited in claim 1 wherein during the step of replacing, the replacement material that is used has a melting temperature of less than about 1,200° C.

3. The method as recited in claim 1 wherein during the step of replacing, the replacement material that is used is selected from Group IB of the Periodic table.

4. The method as recited in claim 1 further comprising the step of attaching a substrate to the body.

5. The method as recited in claim 4 wherein the step of attaching takes place during the step of replacing, and wherein the substrate includes a binder material that is formed from the replacement material, and wherein the substrate is a cermet material.

6. The method as recited in claim 4 wherein the step of attaching takes place after the step of replacing.

7. The method as recited in claim 6 wherein the step of attaching takes place before the step of treating.

8. A method for making a polycrystalline diamond construction comprising the steps of:
treating a polycrystalline diamond body comprising a plurality of bonded together diamond crystals and a solvent catalyst disposed within interstitial regions to remove substantially all of the solvent catalyst material therefrom;
attaching the polycrystalline diamond body to a substrate, wherein during the step of attaching, a constituent of the substrate infiltrates into the polycrystalline diamond body to fill the interstitial regions, wherein the constituent of the substrate is a non-catalyst material not initially used to form the diamond body; and
leaching the polycrystalline diamond body to remove a portion of the infiltrated constituent from a region depth extending from a working surface of the body, wherein the infiltrated constituent remains in another region of the body.

9. The method as recited in claim 8 wherein during the step of treating, the polycrystalline diamond body is rendered substantially free of the solvent catalyst material.

10. The method as recited in claim 8 wherein during the step of leaching, the partial depth of the polycrystalline diamond body is rendered substantially free of the constituent.

11. The method as recited in claim 8 wherein the step of attaching is conducted at high pressure/high temperature conditions.

12. The method as recited in claim 8 wherein during the leaching step rendering interstitial regions within the partial depth of the diamond body substantially empty.

13. A method for making a polycrystalline diamond construction comprising the steps of:
treating a polycrystalline diamond body comprising a plurality of bonded together diamond crystals and a solvent catalyst material to remove substantially all of the solvent catalyst material therefrom to form a thermally stable diamond body, wherein the solvent catalyst material is disposed within interstitial regions between the bonded together diamond crystals;
infiltrating a replacement material through the entire polycrystalline diamond body to fill the interstitial regions, wherein the replacement material is inert up to about 2000° C. and is a material not initially used to form the diamond body; and
attaching the thermally stable diamond body to a substrate,
wherein after attachment to the substrate, the thermally stable diamond body comprises a first region adjacent the substrate having the interstitial regions filled with the replacement material, and a second region remote from the substrate being substantially free of the replacement material.

14. The method of claim 13 , wherein the replacement material infiltrates the entire polycrystalline diamond body, and wherein the method further comprises:
removing the replacement material from a portion of the interstitial regions to form the second region remote from the substrate.

Assignees

• Keshavan Madapusi K
• Eyre Ronald K
• Griffo Anthony
• Cariveau Peter Thomas
• Smith International

Inventors

• Keshavan Madapusi K
• Eyre Ronald K
• Griffo Anthony
• Cariveau Peter Thomas

Classifications

• E21B10/5673

  having a non planar or non circular cutting face · CPC title

• E21B10/55 Primary

  with preformed cutting elements · CPC title

• C01B32/28 Primary

  After-treatment, e.g. purification, irradiation, separation or recovery · CPC title

• C22C26/00

  Alloys containing diamond {or cubic or wurtzitic boron nitride, fullerenes or carbon nanotubes} · CPC title

• C22C2204/00

  End product comprising different layers, coatings or parts of cermet · CPC title