Production apparatus and production method for fine particles

Patent metadata

Field	Value
Publication number	US-10124406-B2
Application number	US-201815915017-A
Country	US
Kind code	B2
Filing date	Mar 7, 2018
Priority date	Apr 5, 2017
Publication date	Nov 13, 2018
Grant date	Nov 13, 2018

Abstract

A production apparatus for fine particles includes a vacuum chamber, a material supply device, a plurality of electrodes arranged and a collection device connecting to the other end of the vacuum chamber and collecting fine particles, which generates plasma and produces fine particles from the material particles, in which a first electrode arrangement region on the material supply port's side and a second electrode arrangement region apart from the first electrode arrangement region to the collection device's side which respectively cross a direction in which the material flows between the vicinity of the material supply port and the collection device are provided in the intermediate part of the vacuum chamber, and both the first electrode arrangement region and the second electrode arrangement region are provided with a plurality of electrodes respectively to form the electrodes in multi-stages.

First claim

What is claimed is:

1. A production apparatus for fine particles comprising:
a vacuum chamber;
a material supply device connected to one end side of the vacuum chamber and supplying material particles to the vacuum chamber from a material supply port;
plural electrodes arranged in an intermediate part of the vacuum chamber and generating plasma inside the vacuum chamber when AC power phases of which differ from one another are applied to respective electrodes; and
a collection device connecting to an other end of the vacuum chamber and collecting fine particles, which generates plasma in the vacuum chamber and produces fine particles from the material particles,
wherein a first electrode arrangement region on the material supply port's side and a second electrode arrangement region apart from the first electrode arrangement region to the collection device's side which respectively cross a direction in which the material flows between a vicinity of the material supply port and the collection device are provided in the intermediate part of the vacuum chamber,
both the first electrode arrangement region and the second electrode arrangement region are provided with the plural electrodes respectively to form the electrodes in multi-stages, and
an angle of inclination of the electrodes arranged in the first electrode arrangement region is larger than an angle of inclination of the electrodes arranged in the second electrode arrangement region.

2. The production apparatus for fine particles according to claim 1 ,
wherein a diameter of a circle formed by respective tip ends of the plural electrodes arranged in the second electrode arrangement region is larger than a diameter of a circle formed by respective tip ends of the plural electrodes arranged in the first electrode region.

3. The production apparatus for fine particles according to claim 1 ,
wherein a heat insulating member installed inside the vacuum chamber has a shape in which a diameter of an inner side of an electrode installation place on the collection device's side is smaller than a diameter of an inner side of an electrode installation place in the vicinity of the material supply port.

4. The production apparatus for fine particles according to claim 1 , further comprising:
discharge gas supply pipes capable of supplying a discharge gas from an opposite side of the material supply port in an electrode installation direction.

5. The production apparatus for fine particles according to claim 1 ,
wherein AC power sources are respectively connected to the plural electrodes and AC power phases of which differ from one another is applied to the plural electrodes respectively from the AC power sources to thereby generate arc discharge as the plasma inside the vacuum chamber.

6. A production method for fine particles comprising the steps of:
generating thermal plasma by applying AC power phases of which differ from one another to plural electrodes respectively, which are formed in multi-stages by being arranged respectively in a first electrode arrangement region on a material supply port's side and a second electrode arrangement region apart from the first electrode arrangement region to a fine particle collection device's side which respectively cross a direction in which material particles flow in a discharge gas in a vacuum chamber between a vicinity of the material supply port and the fine particle collection device which are provided in an intermediate part of the vacuum chamber, in which an angle of inclination of the electrodes arranged in the first electrode arrangement region is larger than an angle of inclination of the electrodes arranged in the second electrode arrangement region;
supplying the material particles into a region of the thermal plasma from the material supply port of a material supply device; and
generating fine particles by evaporating and vaporizing the material particles to generate a material gas when passing through the region of the thermal plasma and by cooling the material gas rapidly at a moment when the material gas exits from the region of the thermal plasma.

7. The production method for fine particles according to claim 6 ,
wherein a diameter of a circle formed by respective tip ends of the plural electrodes arranged in the second electrode arrangement region is larger than a diameter of a circle formed by respective tip ends of the plural electrodes arranged in the first electrode region.

8. The production method for fine particles according to claim 5 ,
wherein the plasma is arc discharge performing pulsed discharge by supplying power phases of which differ from one another from AC power sources to the plural electrodes respectively.

9. The production method for fine particles according to claim 5 ,
wherein the plasma is arc discharge generated by electrodes arranged in parallel so as to be two stages or more in a direction in which the material flows, which is vertically long discharge toward the direction in which the material flows or a high-temperature region is vertically long.

10. The production method for fine particles according to claim 6 , further comprising:
forming a swirling flow in the vicinity of the electrodes by supplying the discharge gas from an opposite side of the material supply port in an electrode installation direction.

11. The production apparatus for fine particles according to claim 1 ,
further including a heat insulating member installed inside the vacuum chamber to insulate the vacuum chamber,
wherein the heat insulating member includes a carbon material.

12. The production apparatus for fine particles according to claim 1 ,
further including a heat insulating member installed inside the vacuum chamber to insulate the vacuum chamber,
wherein the heat insulating member includes a ceramic material.

13. The production apparatus for fine particles according to claim 2 ,
wherein a ratio of the diameter of a circle formed by respective tip ends of the plural electrodes arranged in the second electrode arrangement region to the diameter of a circle formed by respective tip ends of the plural electrodes arranged in the first electrode region is 0.5 or more to 1 or less.

14. The production apparatus for fine particles according to claim 1 ,
wherein a number of the plural electrodes is a multiple of 6.

Assignees

• Panasonic Ip Man Co Ltd

Inventors

• Nagai Hisao
• Koiwasaki Takeshi
• Tanabe Masaaki
• Okuma Takafumi

Classifications

• B22F1/056

  Submicron particles having a size above 100 nm up to 300 nm · CPC title

• B22F1/054

  Nanosized particles · CPC title

• C01F7/027

  Treatment involving fusion or vaporisation · CPC title

• C01B32/963

  Preparation from compounds containing silicon · CPC title

• B01J2219/0809

  employing two or more electrodes · CPC title