Method for producing dewatered microfibrillated cellulose

Patent metadata

Field	Value
Publication number	US-10113005-B2
Application number	US-201314653417-A
Country	US
Kind code	B2
Filing date	Dec 19, 2013
Priority date	Dec 20, 2012
Publication date	Oct 30, 2018
Grant date	Oct 30, 2018

Abstract

The present invention relates to a method for producing dewatered microfibrillated cellulose (MFC) comprising i) providing an aqueous MFC slurry, ii) optionally dewatering said MFC slurry by mechanical means to provide a partly dewatered MFC slurry, and iii) subjecting the MFC slurry or the partly dewatered MFC slurry to one or more drying operations by means of one or more absorbing materials to produce dewatered MFC. The produced MFC can be redispersed in water without deteriorating the material properties of the MFC.

First claim

The invention claimed is:

1. A method for producing dewatered microfibrillated cellulose (MFC) comprising:
i) providing an aqueous MFC slurry,
ii) optionally dewatering said MFC slurry by mechanical means to provide a partly dewatered MFC slurry, and
iii) subjecting the MFC slurry or the partly dewatered MFC slurry to one or more drying operations by contacting the MFC slurry or the partly dewatered MFC slurry with one or more absorbing materials comprising superabsorbent polymer to produce dewatered MFC,

wherein the one or more drying operations is done at ambient temperature and pressure and wherein the one or more drying operations prevents agglomeration of the MFC to obtain the dewatered MFC which is redispersible.

2. The method of claim 1 wherein the MFC slurry or the partly dewatered MFC slurry is contacted with a first absorbing material and subsequently with a second absorbing material to produce dewatered MFC.

3. The method of claim 2 wherein the first absorbent material comprises a cellulosic material.

4. The method of claim 2 wherein the second absorbing material comprises a superabsorbent polymer.

5. The method of claim 1 wherein the drying operation is repeated at least once.

6. The method of claim 1 wherein the dry content of the MFC slurry is at most 6% by weight.

7. The method of claim 1 wherein dry content of the partly dewatered MFC slurry is at most 20% by weight.

8. The method of claim 1 wherein dry content of the dewatered MFC is at least 20% by weight.

9. The method of claim 1 wherein the method is carried out on a moving substrate such that the MFC slurry or partly dewatered MFC slurry is placed on the substrate and moving along with the substrate to a drying section wherein the absorbing material is brought into contact with the MFC whereafter the absorbing material is removed and optionally this operation is repeated to produce dewatered MFC.

10. The method of claim 1 wherein the method is carried out on a moving substrate such that the MFC slurry or partly dewatered MFC slurry is placed on the substrate and moving along with the substrate to a first drying section wherein a first absorbing material is brought into contact with the MFC whereafter the first absorbing material is removed and the substrate along with the obtained MFC slurry is moved to a second drying section wherein a second absorbing material is brought into contact with the MFC whereafter the second absorbing material is removed to produce dewatered MFC.

11. The method of claim 1 wherein the one or more absorbing materials are regenerated and reused as absorbing material.

Assignees

• Kemira Oyj

Inventors

• Häggblom Martin
• Vuorenpalo Veli-Matti

Classifications

• C08B15/02 Primary

  Oxycellulose; Hydrocellulose; {Cellulosehydrate, e.g. microcrystalline cellulose} · CPC title

• C08L1/02 Primary

  Cellulose; Modified cellulose · CPC title

• C08J9/28

  by elimination of a liquid phase from a macromolecular composition or article, e.g. drying of coagulum · CPC title