Molecular sieve SSZ-85 composition of matter and synthesis thereof
US-9359217-B2 · Jun 7, 2016 · US
US10112839B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10112839-B2 |
| Application number | US-201715716786-A |
| Country | US |
| Kind code | B2 |
| Filing date | Sep 27, 2017 |
| Priority date | Nov 9, 2016 |
| Publication date | Oct 30, 2018 |
| Grant date | Oct 30, 2018 |
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A method is disclosed for preparing molecular sieve SSZ-85 in the absence of a source of fluoride ions.
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The invention claimed is: 1. A method of preparing molecular sieve SSZ-85 comprising contacting under crystallization conditions a reaction mixture comprising a source of cobalt, a source of aluminum, a source of phosphorus, and an ionic liquid comprising a 1,3-diisopropylimidazolium cation; wherein the reaction mixture is substantially free of fluoride ions. 2. The method of claim 1 , wherein the reaction mixture has a composition, in terms of molar ratios, as follows: CoO/Al 2 O 3 0.05 to 0.5 P 2 O 5 /(CoO + Al 2 O 3 ) 0.5 to 1.5 [Q + A − ]/(CoO + Al 2 O 3 ) 1 to 100 wherein [Q + A − ] represents an ionic liquid comprising a 1,3-diisopropylimidazolium cation (Q + ) and an anion (A − ) which is not detrimental to the formation of the molecular sieve. 3. The method of claim 1 , wherein the reaction mixture has a composition, in terms of molar ratios, as follows: CoO/Al 2 O 3 0.05 to 0.5 P 2 O 5 /(CoO + Al 2 O 3 ) 0.8 to 1.2 [Q + A − ]/Al 2 O 3 2 to 50. wherein [Q + A − ] represents an ionic liquid comprising a 1,3-diisopropylimidazolium cation (Q + ) and an anion (A − ) which is not detrimental to the formation of the molecular sieve. 4. The method of claim 1 , wherein the crystallizations conditions include a temperature of from 100° C. to 135° C.
Phosphates, e.g. APO or SAPO compounds · CPC title
the other elements being metals only · CPC title
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