Microfluidic system and method for performing a flash separation of a reservoir fluid sample

Patent metadata

Field	Value
Publication number	US-10107728-B2
Application number	US-201113984852-A
Country	US
Kind code	B2
Filing date	Feb 11, 2011
Priority date	Feb 11, 2011
Publication date	Oct 23, 2018
Grant date	Oct 23, 2018

Abstract

A system for performing a flash separation of a reservoir fluid includes a sample chamber configured to hold the reservoir fluid and a flash apparatus in fluid communication with the sample chamber. The flash apparatus includes a microfluidic device configured to flash the reservoir fluid in fluid communication with the sample chamber, and a separation chamber configured to separate the flashed reservoir fluid into a liquid phase and a gaseous phase in fluid communication with the microfluidic device. The system further includes a gas receptacle configured to store the gaseous phase, A method for performing a flash separation of a reservoir fluid includes providing a reservoir fluid to a microfluidic device, urging the reservoir fluid through the microfluidic device such that the reservoir fluid is lashed within the microfluidic device, and separating a liquid phase and a gaseous phase from the flashed reservoir fluid.

First claim

What is claimed is:

1. A system for performing a flash separation of a reservoir fluid, comprising:
a sample chamber configured to hold the reservoir fluid;
a flash apparatus, comprising:
a microfluidic device configured to flash the reservoir fluid in fluid communication with the sample chamber by means of an adjustment valve and comprising a serpentine microchannel having a micro-venturi, including a nozzle opening having a width smaller than that of the microchannel, in an inlet thereof, wherein flashing of the reservoir fluid is initiated by one or more constrictions therein; and
a separation chamber configured to separate the flashed reservoir fluid into a liquid phase and a gaseous phase, the separation chamber in fluid communication with the microfluidic device and comprising an inlet in fluid communication with the microfluidic device extending into a liquid phase of reservoir fluid in a liquid trap portion in the separation chamber and an outlet extending from above the liquid phase of reservoir fluid in the separation chamber; and

a gas receptacle configured to store the gaseous phase in fluid communication with the separation chamber outlet.

2. The system of claim 1 , wherein the separation chamber comprises:
an inlet in fluid communication with the microfluidic device extending below an upper reservoir fluid line; and
an outlet in fluid communication with the gas receptacle extending to above the upper reservoir fluid line.

3. The system of claim 1 , further comprising:
a switching valve in fluid communication with the gas receptacle and the separation chamber; and
a chromatograph in fluid communication with the switching valve.

4. The system of claim 1 , wherein the gas receptacle is a gas storage bag.

5. A method for performing a flash separation of a reservoir fluid, comprising:
providing a reservoir fluid to a microfluidic device according to the system of claim 1 ;
urging the reservoir fluid through the microfluidic device, such that the reservoir fluid is flashed within the microfluidic device; and
separating a liquid phase and a gaseous phase from the flashed reservoir fluid.

6. The method of claim 5 , wherein urging the reservoir fluid through the microfluidic device is accomplished by operating a pump.

7. The method of claim 5 , further comprising collecting the gaseous phase in a gas receptacle.

8. The method of claim 5 , further comprising analyzing the gaseous phase using chromatography.

9. The system of claim 1 , wherein the microfluidic device comprises:
a first substrate defining a microchannel, an entrance well, and an exit well, the microchannel extending between and in fluid communication with the entrance well and the exit well; and
a second substrate attached to the first substrate to form a microfluidic device, the second substrate defining an entrance passageway in fluid communication with the entrance well and an exit passageway in fluid communication with the exit well;
wherein the entrance passageway is in fluid communication with the sample chamber and the exit passageway is in fluid communication with the separation chamber.

10. The system of claim 9 , wherein a lower surface of the second substrate is fused to an upper surface of the first substrate using an anodic bonding method.

11. The system of claim 9 , wherein at least one of the first substrate and the second substrate comprises one of glass and silicon.

12. The system of claim 9 , wherein the microchannel, the entrance well, and the exit well are generated in the first substrate by an etching process.

13. The system of claim 9 , wherein the microchannel exhibits a serpentine shape and a length of at least one meter.

14. The system of claim 9 , wherein the microchannel exhibits a width within a range of tens of micrometers to hundreds of micrometers.

15. The system of claim 9 , wherein the microchannel includes a microventuri inlet having a nozzle opening that exhibits a smaller width than a width of the microchannel.

16. The system of claim 9 , wherein the microchannel includes at least one constriction exhibiting a width that is smaller than a width of the microchannel.

17. The system of claim 1 , further comprising a pump for urging the reservoir fluid from the sample chamber.

18. The system of claim 17 , wherein:
the sample chamber comprises a floating piston dividing the sample chamber into a first chamber and a second chamber;
the reservoir fluid is disposed in the second chamber; and
the pump is in fluid communication with the first chamber, such that the pump is configured to urge a fluid into the first chamber to urge the reservoir fluid from the second chamber.

19. The system of claim 17 , further comprising at least one gage or sensor operably associated with the flash apparatus.

20. The system of claim 19 , further comprising a controller operably associated with the pump and the at least one gage or sensor.

21. The system of claim 20 , further comprising a switching valve in fluid communication with the flash apparatus and the gas receptacle and operably associated with the controller.

22. The system of claim 20 , further comprising a chromatograph in fluid communication with the flash apparatus and operably associated with the controller.

23. The system of claim 20 , further comprising at least one temperature control device operably associated with at least one of the sample chamber, the flash apparatus, and a fluid line extending from the flash apparatus.

24. The system of claim 23 , wherein the at least one temperature control device is operably associated with the controller.

25. A system for performing a flash separation of a reservoir fluid, comprising:
a hydraulic pump;
a sample chamber comprising a floating piston separating the chamber into a first chamber and a second chamber, the first chamber being in fluid communication with the hydraulic pump;
a flash apparatus, comprising:
a microfluidic device configured to flash the reservoir fluid, the microfluidic device defining an entrance passageway and an exit passageway, the entrance passageway being in fluid communication with the second chamber of the sample chamber by means of an adjustment valve and comprising a serpentine microchannel having a micro-venturi, including a nozzle opening having a width smaller than that of the microchannel, in an inlet thereof, wherein flashing of the reservoir fluid is initiated by one or more constrictions therein; and
a separation chamber comprising an inlet extending to below an upper reservoir level line and an outlet extending to above the upper reservoir level line, the inlet being in fluid communication with the exit passageway of the microfluidic device in a liquid trap portion in the separation chamber, and an outlet extending from above the upper reservoir level line of reservoir fluid in the separation chamber;

a switching valve in fluid communication with the outlet of the separation chamber;
a gas receptacle in fluid communication with the switching valve;
a chromatograph in fluid communication with the switching valve via a fluid line;
at least one sensor operably associated with the flash apparatus;
at least one temperature control unit operably associated with at least one of the sample chamber, the flash apparatus, and the fluid line; and
a controller operably associated with at least one of the hydraulic pump, the switching valve, the chromatograph, the at

Assignees

• Mostowfi Farshid
• Singh Anil
• Schmidt Kurt
• Fisher Rob
• Schlumberger Technology Corp

Inventors

• Mostowfi Farshid
• Singh Anil
• Schmidt Kurt
• Fisher Rob

Classifications

• G01N1/4022 Primary

  by thermal techniques; Phase changes · CPC title

• G01N30/12

  by evaporation · CPC title

• B01D3/06 Primary

  Flash distillation · CPC title

• B01D1/0082

  Regulation; Control · CPC title

• B01D1/30

  Accessories for evaporators {; Constructional details thereof} · CPC title