Injection well identification using tracer particles

Patent metadata

Field	Value
Publication number	US-10101496-B2
Application number	US-201615379468-A
Country	US
Kind code	B2
Filing date	Dec 14, 2016
Priority date	Jun 23, 2014
Publication date	Oct 16, 2018
Grant date	Oct 16, 2018

Abstract

A system and method of injection well identification using tracer particles is disclosed. A collector-reader for analyzing magnetic particles in a fluid that is moving with respect to the collector-reader includes an array of magnets whose magnetization direction is varied so as to create regions of high magnetic field gradient in the fluid, a stopper configured to concentrate spatially the particles attracted to the array, and a reader including a source configured to excite the particles concentrated by the stopper and a detector configured to capture a particle excitation signature emitted by the magnetic particles. A method for observing a subterranean reservoir penetrated by a production well and two or more injection wells is also disclosed.

First claim

What is claimed is:

1. A collector-reader for analyzing magnetic particles in a fluid that is moving with respect to the collector-reader comprising:
an array of magnets whose magnetization direction is varied so as to create regions of high magnetic field gradient in the fluid, wherein the array of magnets is configured to be suspended in the fluid, and wherein the array of magnets is configured as a disk with an axis and disk fins that spin the disk on the axis when impacted by the fluid;
a stopper configured to concentrate spatially the particles attracted to the array; and
a reader including a source configured to excite the particles concentrated by the stopper and a detector configured to capture a particle excitation signature emitted by the magnetic particles.

2. The collector-reader of claim 1 , wherein adjacent magnets in the array have opposite magnetization polarity or are configured as a Halbach array.

3. The collector-reader of claim 1 , wherein the source excites the particles with X-rays and the detector measures the resulting particle X-ray fluorescence.

4. The collector-reader of claim 1 , further including a window transparent to X-rays adjacent to the stopper.

5. The collector-reader of claim 1 , wherein the source excites the particles optically and the detector measures the resulting optical fluorescence.

6. The collector-reader of claim 1 , wherein the source excites the particles and the detector measures particle excitation using one or more of:
X-ray fluorescence,
optical fluorescence,
atomic absorption,
atomic spectroscopy,
neutron activation,
inductively coupled plasma mass spectrometry, and
X-ray photo-electron spectroscopy.

7. The collector-reader of claim 1 , wherein the stopper is v-shaped.

8. The collector-reader of claim 1 , wherein the reader is at least 10 feet from the array.

9. A method for making observations of a subterranean reservoir penetrated by a production well including a pipe producing a fluid and by at least two injection wells comprising:
delivering a first set of tracer particles to a first subterranean location via a first injection well and delivering a second set of tracer particles to a second subterranean location via a second injection well;
producing fluid out of the reservoir via the production well, wherein producing the fluid includes concentrating tracer particles in the produced fluid using a collector comprising:
an array of magnets positioned within the production well pipe, wherein adjacent magnets in the array have opposite magnetization polarity or the array is a linear array, the fluid moving with respect to the array, and
a removable sheath configured to capture the particles magnetically attracted to the array and transfer them for analysis; and

detecting the presence or absence of the first set of tracer particles in the produced fluid and detecting the presence or absence of the second set of tracer particles in the produced fluid,
wherein the tracer particles each include a magnetic material and an identification element, the identification element in the first set of tracer particles differing from the identification element in the second set of tracer particles and wherein detecting the presence or absence of tracer particles is performed by detecting one or more identification elements using one or more of:
X-ray fluorescence spectroscopy,
atomic absorption,
atomic spectroscopy,
neutron activation,
optical fluorescence,
inductively coupled plasma mass spectrometry, and
X-ray photo-electron spectroscopy.

10. The method according to claim 9 , wherein producing fluid out of the reservoir via the production well further includes concentrating tracer particles in the produced fluid using magnetic extraction.

11. The method according to claim 10 , wherein producing fluid out of the reservoir via the production well further includes concentrating tracer particles in the produced fluid using a collector comprising:
an array of magnets, the fluid moving with respect to the array; and
a stopper configured to concentrate spatially the particles magnetically attracted to the array.

12. The method according to claim 9 , further including determining the proportion of fluid from the first injection well to fluid from the second injection well in the produced fluid by determining the proportion of the first set of tracer particles to the second set of tracer particles in the produced fluid.

13. A collector-reader for analyzing magnetic particles in a fluid that is moving with respect to the collector-reader comprising:
an array of magnets whose magnetization direction is varied so as to create regions of high magnetic field gradient in the fluid, wherein the array of magnets is configured as a collar surrounding a non-magnetic section of a pipe, wherein an axis of the array and an axis of the pipe are coincident, and wherein the array is configured to rotate on its axis;
a stopper configured to concentrate spatially the particles attracted to the array;
a cleaner that removes magnetic particles from the stopper; and
a reader including a source configured to excite the particles concentrated by the stopper and a detector configured to capture a particle excitation signature emitted by the magnetic particles.

14. The collector-reader of claim 13 , wherein the cleaner is a protuberance on an inner surface of the non-magnetic section of the pipe.

15. A method for making observations of a subterranean reservoir penetrated by a production well including a pipe producing a fluid and by at least two injection wells comprising:
delivering a first set of tracer particles to a first subterranean location via a first injection well and delivering a second set of tracer particles to a second subterranean location via a second injection well;
producing fluid out of the reservoir via the production well; and
detecting the presence or absence of the first set of tracer particles in the produced fluid and detecting the presence or absence of the second set of tracer particles in the produced fluid,
wherein the tracer particles each include a ferrite or ferrous alloy magnetic material surrounded by a layer containing an identification element, the identification element in the first set of tracer particles differing from the identification element in the second set of tracer particles, wherein the layer is covered by a protective shell, and wherein detecting the presence or absence of tracer particles is performed by detecting one or more identification elements using one or more of:
X-ray fluorescence spectroscopy,
atomic absorption,
atomic spectroscopy,
neutron activation,
optical fluorescence,
inductively coupled plasma mass spectrometry, and
X-ray photo-electron spectroscopy.

Assignees

• Charles Stark Draper Laboratory Inc

Inventors

• Bernstein Jonathan J
• Guerrero Julio C
• Hansberry Mitchell

Classifications

• G01N33/2882

  Markers · CPC title

• G01N23/223

  by irradiating the sample with X-rays or gamma-rays and by measuring X-ray fluorescence · CPC title

• E21B43/16 Primary

  Enhanced recovery methods for obtaining hydrocarbons · CPC title

• G01V5/125

  and detecting the secondary gamma- or X-rays in different places along the bore hole · CPC title

• G01V15/00 Primary

  Tags attached to, or associated with, an object, in order to enable detection of the object (record carriers for use with machines having a detectable tag or marker G06K19/00) · CPC title