Polycrystalline tables, polycrystalline elements, and related methods

Patent metadata

Field	Value
Publication number	US-10099347-B2
Application number	US-201113040921-A
Country	US
Kind code	B2
Filing date	Mar 4, 2011
Priority date	Mar 4, 2011
Publication date	Oct 16, 2018
Grant date	Oct 16, 2018

Abstract

Polycrystalline elements include a substrate and a polycrystalline table attached to an end of the substrate. The polycrystalline table includes a first region of superabrasive material having a first permeability and at least a second region of superabrasive material having a second, lesser permeability, the at least a second region being interposed between the substrate and the first region. Methods of forming a polycrystalline element involve attaching a polycrystalline table including a first region of superabrasive material having a first permeability and at least a second region of superabrasive material having a second, lesser permeability to an end of a substrate, the at least a second region being interposed between the first region and the substrate. Catalyst material is removed from at least the first region of the polycrystalline table.

First claim

What is claimed is:

1. A polycrystalline element, comprising:
a substrate; and
a polycrystalline table attached to an end of the substrate and comprising a first region of superabrasive material having a first permeability and at least a second region of superabrasive material having a second, lesser permeability, the at least a second region being interposed between the substrate and the first region,
wherein the first region comprises a first volume percentage of interstitial volumes among interbonded grains of superabrasive material and the at least a second region comprises a second, smaller volume percentage of interstitial volumes among interbonded grains of superabrasive material.

2. The polycrystalline element of claim 1 , wherein the first region is at least substantially fully leached of catalyst material.

3. The polycrystalline element of claim 1 , wherein an interface between the first and at least a second regions of the polycrystalline table comprises a non-planar interface.

4. The polycrystalline element of claim 1 , wherein the polycrystalline table further comprises a third region disposed adjacent the at least a second region on an end opposing the first region.

5. The polycrystalline element of claim 1 , wherein the first region comprises a first volume percentage of superabrasive material and the at least a second region comprises a second, greater volume percentage of superabrasive material.

6. The polycrystalline element of claim 1 , wherein the first region comprises a first mean grain size of grains of superabrasive material and the at least a second region comprises a second, smaller mean grain size of grains of superabrasive material.

7. The polycrystalline element of claim 6 , wherein the at least a second region comprises at least some nano-sized grains.

8. The polycrystalline element of claim 1 , wherein the first region comprises interstitial volumes having a first interconnectivity and the at least a second region comprises interstitial volumes having a second, lesser interconnectivity.

9. A method of forming a polycrystalline element, comprising:
disposing a first plurality of particles comprising a superabrasive material, a second plurality of particles comprising a superabrasive material, a catalyst material, and a third plurality of particles comprising a mass of hard material in a mold;
sintering the first and second pluralities of particles in the presence of the catalyst material and the third plurality of particles to form a polycrystalline table attached to a substrate, the polycrystalline table having a first region comprising a first volume percentage of interstitial volumes among interbonded grains of superabrasive material and at least a second region comprising a second, smaller volume percentage of interstitial volumes among interbonded grains of superabrasive material, the first region exhibiting a first permeability and the at least a second region exhibiting a second, lesser permeability, the at least a second region being interposed between the first region and the substrate; and
removing catalyst material from at least the first region of the polycrystalline table.

10. The method of claim 9 , further comprising:
pressing the second plurality of particles to form a green part prior to disposing the second plurality of particles in the mold.

11. The method of claim 10 , wherein pressing the second plurality of particles to form a green part prior to disposing the second plurality of particles in the mold comprises imparting a non-planar interface design to the green part.

12. The method of claim 9 , further comprising:
disposing a fourth plurality of particles comprising a non-catalyst material removable by a leaching agent dispersed among the first plurality of particles in the mold.

13. The method of claim 9 , further comprising:
disposing a fourth plurality of particles comprising a non-catalyst material removable by a leaching agent among the first plurality of particles.

14. The method of claim 9 , wherein disposing a first plurality of particles comprising a superabrasive material, a second plurality of particles comprising the superabrasive material, a catalyst material, and a third plurality of particles comprising a mass of hard material in a mold comprises disposing the first plurality of particles having a first packing density and the second plurality of particles having a second, greater packing density in the mold.

15. The method of claim 9 , wherein disposing a first plurality of particles comprising a superabrasive material, a second plurality of particles comprising the superabrasive material, a catalyst material, and a third plurality of particles comprising a mass of hard material in a mold comprises disposing the first plurality of particles having a first mean particle size and the second plurality of particles having a second, smaller mean particle size in the mold.

16. The method of claim 15 , wherein disposing the first plurality of particles having a first mean particle size and the second plurality of particles having a second, smaller mean particle size in the mold comprises disposing the second plurality of particles comprising at least some nanoparticles in the mold.

17. The method of claim 9 , further comprising:
coating at least some of the first plurality of particles with the catalyst material using chemical solution deposition prior to disposing the first plurality of particles in the mold.

18. The method of claim 9 , wherein sintering the first and second pluralities of particles in the presence of the catalyst material and the third plurality of particles to form a polycrystalline table having a first region comprising a first permeability and at least a second region comprising a second, lesser permeability attached to a substrate comprises sintering the first and at least a second pluralities of particles in the presence of the catalyst material and the third plurality of particles to form a polycrystalline table having a first region comprising a first volume percentage of catalyst material disposed in interstitial spaces among interbonded grains of superabrasive material and at least a second region comprising a second, smaller volume percentage of catalyst material disposed in interstitial spaces among interbonded grains of superabrasive material.

19. A method of forming a polycrystalline element, comprising:
attaching a polycrystalline table to an end of a substrate, the polycrystalline table comprising a first region comprising a first volume percentage of interstitial volumes among interbonded grains of superabrasive material and at least a second region comprising a second, smaller volume percentage of interstitial volumes among interbonded grains of superabrasive material, the first region of exhibiting a first permeability and the at least a second region exhibiting a second, lesser permeability, the at least a second region being interposed between the first region and the substrate; and
removing catalyst material from at least the first region of the polycrystalline table.

20. A method of forming a polycrystalline element, comprising:
forming a first polycrystalline table of superabrasive material in the presence of a catalyst material, the first polycrystalline table having a first region having a first volume percentage of interstitial volumes among interbonded grains of superabrasive material, the first region exhibiting a first permeability, and a second region having a second, smaller volume percentage of intersti

Assignees

• Lyons Nicholas J
• Scott Danny E
• Digiovanni Anthony A
• Nelms Derek L
• Baker Hughes Inc

Inventors

• Lyons Nicholas J
• Scott Danny E
• Digiovanni Anthony A
• Nelms Derek L

Classifications

• Y10T428/249981

  Plural void-containing components · CPC title

• B24D99/005

  Segments of abrasive wheels · CPC title

• Y10T428/24996

  With internal element bridging layers, nonplanar interface between layers, or intermediate layer of commingled adjacent foam layers · CPC title

• B24D18/0009 Primary

  using moulds or presses · CPC title

• E21B10/5735

  Interface between the substrate and the cutting element · CPC title