Process for producing electrode material, and electrode material

Patent metadata

Field	Value
Publication number	US-10086433-B2
Application number	US-201515318448-A
Country	US
Kind code	B2
Filing date	May 29, 2015
Priority date	Jun 16, 2014
Publication date	Oct 2, 2018
Grant date	Oct 2, 2018

Abstract

A process for producing an electrode material by infiltrating a highly conductive metal such as Cu into a porous object containing heat-resistant elements. Before an infiltration step in which the highly conductive metal is infiltrated, a HIP treatment is given to a powder containing the heat-resistant elements (or to a molded object obtained by molding a powder containing the heat-resistant elements). The composition is controlled so that the HIP treatment yields a porous object which has a degree of filling of 70% or higher, more preferably 75% or higher. The highly conductive metal is infiltrated into the porous object having the controlled composition.

First claim

The invention claimed is:

1. A process for producing an electrode material, comprising the steps of:
subjecting a molded body or a sintered body of the molded body to a hot isostatic pressing treatment to produce a porous body having a degree of filling of 70% or more, the molded body comprising a Cr powder and a heat resistant element powder including at least one heat resistant element selected from the group consisting of Mo, W, Ta, Nb, V and Zr, wherein an amount of the heat resistant element powder is 13 to 94 wt % of the electrode material and an amount of the Cr powder is 0.65 to 76 wt % of the electrode material; and
infiltrating the porous body with Cu and/or Ag in an amount of 5 to 35 wt % relative to the electrode material.

2. The process for producing the electrode material, as claimed in claim 1 , further comprising a step of press molding a mixed powder comprising the heat resistant element powder and the Cr powder to obtain the molded body.

3. The process for producing the electrode material, as claimed in claim 1 , wherein the heat resistant element powder has an average particle diameter of 2 to 20 μm.

4. The process for producing the electrode material, as claimed in claim 1 , wherein the heat resistant element powder has an average particle diameter of 2 to 10 μm.

5. The process for producing the electrode material, as claimed in claim 1 , wherein the amount of the heat resistant element powder is 35 to 92 wt % of the electrode material.

6. The process for producing the electrode material, as claimed in claim 1 , wherein the amount of the Cr powder is 0.7 to 46 wt % of the electrode material.

7. The process for producing the electrode material, as claimed in claim 1 , wherein the Cr powder has a particle diameter of less than 300 μm.

8. The process for producing the electrode material, as claimed in claim 1 , wherein the Cr powder has a particle diameter of less than 150 μm.

9. The process for producing the electrode material, as claimed in claim 1 , wherein the Cr powder has a particle diameter of less than 45 μm.

10. The process for producing the electrode material, as claimed in claim 1 , wherein the infiltrating step comprises infiltrating the porous body with Cu and/or Ag in the amount of 7.5 to 30 wt % relative to the electrode material.

11. The process for producing the electrode material, as claimed in claim 2 , wherein the step of press molding the mixed powder is performed at a molding pressure of 2 to 4.5 t/cm 2 .

12. The process for producing the electrode material, as claimed in claim 1 , wherein the hot isostatic pressing treatment comprises a treatment temperature of 700 to 1100° C., a treatment pressure of 30 to 100 MPa, and a treatment time of 1 to 5 hours.

13. The process for producing the electrode material, as claimed in claim 1 , wherein
the heat resistant element powder includes Mo; and
the infiltrating step comprises infiltrating the porous body with Cu.

Assignees

• Meidensha Electric Mfg Co Ltd

Inventors

• Kitakizaki Kaoru
• Ishikawa Keita
• Hayashi Shota
• Suzuki Nobutaka

Classifications

• B22F1/052

  characterised by a mixture of particles of different sizes or by the particle size distribution · CPC title

• B22F3/15

  Hot isostatic pressing · CPC title

• B22F5/00

  Manufacture of workpieces or articles from metallic powder characterised by the special shape of the product · CPC title

• C22C27/06

  Alloys based on chromium · CPC title

• C22C1/04

  by powder metallurgy (C22C1/08 takes precedence) · CPC title