High temperature sintering furnace systems and methods
US-2024167767-A1 · May 23, 2024 · US
US10071355B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10071355-B2 |
| Application number | US-201314409750-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jun 18, 2013 |
| Priority date | Jun 20, 2012 |
| Publication date | Sep 11, 2018 |
| Grant date | Sep 11, 2018 |
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A method of making a cutter structure ( 1 ) comprises placing a pre-formed body ( 4 ) of hard material having a surface topography in a canister, placing an aggregated mass of grains of superhard material ( 2 ) over said surface topography, placing a punch ( 10 ) in contact with the superhard material ( 2 ), the punch ( 10 ) having a surface with a surface topography inverse to that of the hard material body to imprint a pattern in the superhard material ( 2 ) complementary to the surface topography of the punch ( 10 ). The surface of the punch ( 10 ) contacting the superhard material ( 2 ) being formed of a ceramic material that does not react chemically with the superhard material ( 12 ) and/or a sinter catalyst for the superhard material ( 2 ). A pressure of greater than 3 GPa is then together with a temperature sufficiently high for the catalyst to melt to form the cutter structure ( 1 ) with a layer of polycrystalline superhard material bonded to the hard material and having a surface topography corresponding to the surface topography of the hard material.
Opening claim text (preview).
The invention claimed is: 1. A method of making a cutter structure comprising the steps of: placing a pre-formed body of hard material having a surface topography in a canister; placing an aggregated mass of grains of superhard material into the canister over the surface of the body of hard material having the surface topography, placing a punch in contact with the aggregated mass of grains of superhard material, the punch having a surface with a surface topography inverse to the surface topography of the hard material body, the surface topography of the punch imprinting a pattern in the aggregated mass of grains of superhard material complementary to the surface topography of the punch and corresponding to the surface topography of the body of hard material, the surface of the punch in contact with the aggregated mass of grains of superhard material being formed of a ceramic material that does not react chemically with the superhard material and/or a sinter catalyst material for the grains of superhard material, the method further comprising: subjecting the aggregated mass of grains of superhard material, the punch and the body of hard material to a pressure of greater than around 3 GPa in the presence of the sinter catalyst material for the grains of superhard material at a temperature sufficiently high for the catalyst material to melt, sintering the grains to form the cutter structure comprising a layer of polycrystalline superhard material bonded to the body of hard material and having a surface topography corresponding to the surface topography of the hard material body and complementary to the surface topography of the punch; removing the cutter structure from the canister; and removing the punch from the layer of polycrystalline superhard material. 2. A method according to claim 1 , wherein the step of placing the punch in contact with the aggregated mass of grains is after the step of placing the grains into a canister. 3. A method according to claim 1 , further comprising: placing a second pre-formed body of hard material having a surface topography in the canister spaced from the first pre-formed body by a layer of separating material; placing a second aggregated mass of grains of superhard material into the canister over the surface of the second body of hard material having the surface topography; and placing a second punch in contact with the second aggregated mass of grains of superhard material; wherein the step of sintering comprises sintering to form a first and second cutter structure within the canister. 4. A method according to claim 3 , wherein the punch, superhard grains and pre-formed body of hard material for forming the first cutter structure are placed in the canister prior to the punch, superhard grains and pre-formed body of hard material for forming the second cutter structure are placed in the canister. 5. A method according to claim 1 , wherein the step of subjecting the grains of superhard material to a pressure comprises subjecting the grains to a pressure of greater than: around 4 GPa, or around 5 GPa, or around 5.5 GPa, or around 6.8 GPa, or around 7 GPa. 6. A method according to claim 1 , wherein the step of placing the surface of the punch in contact with the grains comprises placing a punch formed of a ceramic material comprising any one or more of the group of oxide ceramic materials that are not reduced by carbo-thermal reaction in contact with the grains of superhard material. 7. A method according to claim 6 , wherein the ceramic material is formed of any one or more of the group of oxide ceramic materials comprising magnesia, calcia, zirconia, and/or alumina. 8. A method according to claim 1 , wherein the step of placing the surface of the punch in contact with the grains comprises placing a punch having a surface topography coated with a ceramic material comprising any one or more of the group of oxide ceramic materials that are not reduced by carbo-thermal reaction in contact with the grains. 9. A method according to claim 8 , wherein the ceramic material is formed of any one or more of the group of oxide ceramic materials comprising magnesia, calcia, zirconia, and/or alumina. 10. A method according to claim 1 , wherein the step of forming the cutter structure comprises forming a polycrystalline superhard material layer having a free outer surface on removal of the punch therefrom in which the free outer surface is of the same quality as the bulk of the body of polycrystalline superhard material. 11. A method according to claim 1 , wherein the step of placing an aggregated mass of grains of superhard material into a canister comprises placing an aggregated mass of natural or synthetic diamond grains into the canister. 12. A method according to claim 1 , wherein the step of placing an aggregated mass of grains of superhard material into a canister comprises placing an aggregated mass of cubic boron nitride grains into the canister. 13. A method as claimed in claim 1 , further comprising treating the sintered super-hard material to remove catalyst material from interstices between inter-bonded grains in the superhard material after sintering. 14. A method according to claim 1 , wherein the step of placing the grains of superhard material into the canister comprises providing a plurality of sheets comprising the grains and stacking the sheets in the canister to form the aggregation of superhard grains. 15. A method according to claim 1 , wherein the step of placing an aggregated mass of grains of superhard material into a canister comprises placing an aggregated mass of loose grains into the canister. 16. A method according to claim 1 , wherein the step of placing the grains of superhard material into the canister comprises depositing the grains into the canister using sedimentation or electrophoretic deposition techniques. 17. A method according to claim 1 of making a cutter structure comprising an insert for a machine tool, the surface topography on the superhard layer forming a chip-breaker topography. 18. A method according to claim 1 , further comprising placing one or more interlayers between the pre-formed substrate and the aggregated mass of superhard material to form a gradated cutter structure on sintering. 19. A method according to claim 18 , wherein the interlayers comprise a further mass of aggregated grains of superhard material comprising diamond grains and/or PCBN grains. 20. A method according to claim 1 , further comprising forming one or more pinlock holes extending through the aggregated mass of superhard grains and body of hard material prior to sintering; placing a plug into the hole(s); and removing the plug(s) after the step of sintering. 21. A method according to claim 20 , wherein the plug(s) is/are formed of a ceramic that does not react chemically with the superhard material. 22. A method according to claim 21 , wherein the plug(s) is/are formed of alumina or zirconia.
simultaneously · CPC title
Containers or coating used therefor · CPC title
Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents · CPC title
Apparatus, e.g. furnaces (in general F27B) · CPC title
Removing material: carving, cleaning, grinding, hobbing, honing, lapping, polishing, milling, shaving, skiving, turning the surface · CPC title
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