Tri-axial NMR test instrument

Patent metadata

Field	Value
Publication number	US-10048336-B2
Application number	US-201314018557-A
Country	US
Kind code	B2
Filing date	Sep 5, 2013
Priority date	Sep 5, 2013
Publication date	Aug 14, 2018
Grant date	Aug 14, 2018

Abstract

The invention provides a tri-axial nuclear magnetic resonance apparatus for testing of petro-physical properties and gathering of geo-mechanical information and methods of using the same. The tri-axial nuclear magnetic resonance apparatus includes a tri-axial load frame encasing a tri-axial load cell that includes a tri-axial sample holder, at least one electrical sensor, at least one acoustic sensor, and a nuclear magnetic resonance instrument.

First claim

What is claimed is:

1. A tri-axial nuclear magnetic resonance apparatus for testing of petro-physical properties and gathering of geo-mechanical information, the tri-axial nuclear magnetic resonance apparatus comprising:
a tri-axial load frame encasing;
a tri-axial load cell having a tri-axial sample holder and defining at least one pressurizable space surrounding the tri-axial sample holder;
at least one end cap operable to contact the tri-axial load cell;
at least one electrical sensor;
at least one acoustic sensor; and
a nuclear magnetic resonance instrument located external of the tri-axial load cell; wherein
the tri-axial load cell is operable to provide a radial pressure of 30,000 psi, an axial pressure of 500,000 psi, a confining pressure of 31,000 psi, and a pore pressure of 30,000 psi.

2. The tri-axial nuclear magnetic resonance apparatus of claim 1 , wherein the tri-axial load cell comprises TORLON®.

3. The tri-axial nuclear magnetic resonance apparatus of claim 1 , wherein the at least one end cap has pore lines operable to allow for fluid flow.

4. The tri-axial nuclear magnetic resonance apparatus of claim 1 , wherein the at least one end cap further comprises a conductor operable for current flow.

5. The hi-axial nuclear magnetic resonance apparatus of claim 1 , wherein the at least one end cap further defines one or more cavities for the at least one acoustic sensor.

6. The tri-axial nuclear magnetic resonance apparatus of claim 1 , wherein the at least one acoustic sensor is an acoustic transducer operable to analyze variable frequency and mode.

7. The tri-axial nuclear magnetic resonance apparatus of claim 1 , wherein the at least one acoustic sensor is operable to function as a transmitter and a receiver.

8. The tri-axial nuclear magnetic resonance apparatus of claim 1 , wherein the nuclear magnetic resonance instrument further includes a variable probe.

9. A method for testing of petro-physical properties and gathering of geo-mechanical information, said method comprising the steps of:
providing a tri-axial nuclear magnetic resonance apparatus, the tri-axial nuclear magnetic resonance apparatus comprising:
a tri-axial load frame encasing:
a tri-axial load cell having a tri-axial sample holder and defining at least one pressurizable space surrounding the tri-axial sample holder;
at least one end cap operable to contact the tri-axial load cell, an axial end of the at least one end cap being in contact with the tri-axial load frame;
at least one electrical sensor;
at least one acoustic sensor; and
a nuclear magnetic resonance instrument located external of the tri-axial load cell; wherein

the tri-axial load cell is operable to provide an axial pressure that is greater than, and independent of, a confining pressure;

obtaining a sample from a reservoir,
loading the tri-axial sample holder in the tri-axial load cell to create a loaded tri-axial load cell;
placing the loaded tri-axial load cell in contact with the at least one end cap and placing the axial end of the at least one end cap in contact with the tri-axial load frame;
applying the confining pressure by providing fluid flow through the at least one end cap to the at least one space surrounding the tri-axial sample holder;
providing a tri-axial pressure including a radial pressure, the axial pressure, the confining pressure and a pore pressure; wherein the tri-axial load cell is operable to provide the radial pressure of 30,000 psi, the axial pressure of 500,000 psi, the confining pressure of 31,000 psi, and the pore pressure of 30,000 psi;
circulating temperature control fluid around the tri-axial sample holder by providing the temperature control fluid through the at least one end cap to the at least one space surrounding the tri-axial sample holder;
providing a test fluid through pore lines of the at least one end cap to the tri-axial sample holder;
performing a time dependent slice nuclear magnetic resonance scan of the sample using the nuclear magnetic resonance instrument to provide nuclear magnetic resonance measurements;
performing electrical analysis of the sample using the at least one electrical sensor to provide electrical analysis measurements;
performing acoustic analysis of the sample using the at least one acoustic sensor to provide acoustic measurements; and
using the nuclear magnetic resonance measurements, the electrical analysis measurements, and acoustic measurements to determine petro-physical properties and geo-mechanical properties of the sample from the reservoir.

10. The method of claim 9 , wherein the reservoir is a shale gas reservoir.

11. The method of claim 9 , wherein the tri-axial sample holder is maintained at a temperature of between about −20° C. and 350° C.

12. The method of claim 9 , wherein the test fluid is a dead fluid.

13. The method of claim 9 , wherein the test fluid is a live fluid.

14. The method of claim 9 , wherein the nuclear magnetic resonance instrument is operable to function in a frequency range from at least between 0.1 KHz and 20 MHz.

15. The method of claim 9 , wherein the at least one acoustic sensor is operable to measure frequencies from 1 Hz to 100,000 MHz.

16. The method of claim 9 , wherein the sample is a native sample.

17. The method of claim 9 , wherein the sample is a clean sample.

18. The method of claim 9 , further comprising the step of
performing nuclear magnetic resonance analysis of the sample using a variable probe.

Assignees

• Saudi Arabian Oil Co

Inventors

• Hakimuddin Mustafa

Classifications

• G01V3/14

  operating with electron or nuclear magnetic resonance · CPC title

• G01V3/32

  operating with electron or nuclear magnetic resonance · CPC title

• G01N33/28

  Oils {, i.e. hydrocarbon liquids} (edible oils or edible fats G01N33/03) · CPC title

• G01N3/10

  generated by pneumatic or hydraulic pressure (G01N3/18 takes precedence) · CPC title

• G01N24/081 Primary

  Making measurements of geologic samples, e.g. measurements of moisture, pH, porosity, permeability, tortuosity or viscosity · CPC title