Analyzer for fluids containing an inflammable substance and corresponding method

Patent metadata

Field	Value
Publication number	US-10048234-B2
Application number	US-201214405000-A
Country	US
Kind code	B2
Filing date	Jun 4, 2012
Priority date	Jun 4, 2012
Publication date	Aug 14, 2018
Grant date	Aug 14, 2018

Abstract

Analyzer 1 for analyzing a fluid 3 containing at least one substance to be analyzed and at least one inflammable substance containing:
a source of gas 9 to provide a flux of diluent gas, an injecting nozzle 11 for introducing samples of the fluid into the flux of diluent gas and for producing a gaseous flux, and a detector 7 for analyzing the gaseous flux,

wherein:
the source of gas is intended to deliver a flux of diluent gas containing a material capable of supporting the combustion of the inflammable substance, preferably to deliver a flux of air, the injection nozzle is configured so as to introduce into the diluent gas samples of the fluid such that the average volume fraction of the fluid in the gaseous flux is less than 1/2,000 and preferably less than 1/20,000, and the detector contains at least one microsensor for detecting the substance to be analyzed. Corresponding method.

First claim

The invention claimed is:

1. An analyzer for analyzing a fluid containing at least one substance to be analysed and at least one inflammable substance, the analyzer containing:
a source of gas to provide a flux of diluent gas,
an injecting nozzle for introducing samples of the fluid into the flux of diluent gas and producing a gaseous flux,
a detector for analyzing the gaseous flux, the detector being located in a box, and
a modular interface on which the box and the injecting nozzle are fixed, the modular interface being:
intended to receive at an intake the fluid so as to route the fluid toward the injection nozzle, and
connected to the source of gas so as to route a flux of purge gas to the box and/or to route the flux of diluent gas to the injection nozzle,

wherein:
the source of gas is intended to deliver a flux of diluent gas containing a substance supporting combustion of the inflammable substance,
the injecting nozzle is configured so as to introduce into the flux of diluent gas samples of the fluid such that an average volume fraction of the fluid in the gaseous flux is below 1/2,000,
the detector contains at least one microsensor for detecting the substance to be analysed, and
the analyser contains means for injecting the flux of purge gas into the box, the box being provided with an evacuation outlet for evacuating the flux of purge gas, the means of injection of the flux of purge gas and the evacuation outlet being capable of maintaining inside the box an overpressure relative to the outside of the box.

2. The analyzer according to claim 1 , wherein the injecting nozzle is capable of introducing into the flux of diluent gas, samples of the fluid each weighing less than 10 nanograms.

3. The analyzer according to claim 1 , wherein the means of injecting the flux of purge gas are connected fluidically to the source of gas so as to inject the diluent gas as the purge gas.

4. The analyzer according to claim 1 , wherein the means for injecting the flux of purge gas are configured so as to inject the flux of purge gas into the box at a flow rate higher than 5 times an average flow rate of the gaseous flux.

5. The analyzer according to claim 1 , wherein the detector has an outlet to set free, after analysis, at least a fraction of the gaseous flux inside the box.

6. The analyzer according to claim 1 , wherein the detector contains an electronic control card, the microsensor and the electronic card each being provided with a packing to prevent the forming of a spark inside the box.

7. The analyzer according to claim 1 , wherein the source of gas contains a purifier.

8. A method for analyzing a fluid containing at least one substance to be analyzed and at least one inflammable substance, the method comprising providing an analyzer according to claim 1 and at least the following steps:
a) obtaining a flux of diluent gas from a source of gas,
b) introducing into the flux of diluent gas samples of the fluid to produce a gaseous flux, and
c) analyzing the gaseous flux in a detector,
wherein:
in step a) the flux of diluent gas contains a material capable of supporting the combustion of the inflammable substance, said material being a flux of air,
in step b) the samples are such that the average volume fraction of the fluid in the gaseous flux is less than 1/2,000, and
in step c) the detector is at least a microsensor detecting the substance to be analyzed.

9. The method according to claim 8 , in which, in step b), each of the samples of the fluid introduced into the flux of diluent gas weighs less than 10 nanograms.

10. The method according to claim 8 , wherein in step c) the detector is located in a box into which is injected a flux of purge gas, the purge gas leaving the box through at least one evacuation outlet, the injection of the flux of purge gas maintaining an overpressure inside the box relative to the outside of the box.

11. The method according to claim 10 , wherein in step c), the box presenting an internal volume, the injection of the purge gas takes place at a flow rate and temperature such that on no wall delimiting the internal volume of the box there is a point presenting a temperature higher than or equal to 85° C.

12. The analyzer according to claim 1 , wherein the injecting nozzle is configured so as to introduce into the flux of diluent gas samples of the fluid such that the average volume fraction of the fluid in the gaseous flux is below 1/20,000.

13. The analyzer according to claim 2 , wherein the injecting nozzle is capable of introducing into the flux of diluent gas, samples of the fluid each weighing less than 1.5 nanogram.

14. The analyzer according to claim 2 , wherein the injecting nozzle is capable of introducing into the flux of diluent gas in a cyclical manner.

15. The analyzer according to claim 1 , wherein the detector has an outlet to set free, after analysis, the totality of the gaseous flux inside the box.

16. The method according to claim 8 , wherein in step b) the samples are such that the average volume fraction of the fluid in the gaseous flux is less than 1/20,000.

17. The method according to claim 9 , wherein, in step b), each of the samples of the fluid introduced into the flux of diluent gas weighs less than 1.5 nanogram.

Assignees

• Andreucci Phillipe
• Colinet Eric
• Coric Philippe
• De Wit Jean Claude
• Puget Pierre
• Apix Analytics
• Total Sa
• EIF—Astute

Inventors

• Andreucci Phillipe
• Colinet Eric
• Coric Philippe
• De Wit Jean-Claude
• Puget Pierre

Classifications

• G01N30/16 Primary

  Injection (G01N30/24 takes precedence) · CPC title

• G01N33/225 Primary

  Gaseous fuels, e.g. natural gas · CPC title

• G01N33/22

  Fuels; Explosives · CPC title