Arrangement and system for a treatment process

Patent metadata

Field	Value
Publication number	US-10047408-B2
Application number	US-201515321605-A
Country	US
Kind code	B2
Filing date	Jun 24, 2015
Priority date	Jun 26, 2014
Publication date	Aug 14, 2018
Grant date	Aug 14, 2018

Abstract

An arrangement for feeding and dewatering lignocellulosic material in a hydrolysis process between a first reactor unit, where the material is partly hydrolyzed, to a second reactor unit, wherein the first reactor unit operates at a first pressure and the second reactor unit operates at a second pressure being higher than the first pressure. The arrangement includes a first plug screw feeder arranged to receive the partly hydrolyzed material from the first reactor unit and being arranged to compress, dewater and transport the material, wherein the first screw feeder is arranged to operate at a pressure being higher than the first pressure. A dilution vessel is coupled to receive material from the first plug screw feeder and including a liquid inlet for receiving liquid to wash the material, wherein the dilution vessel is arranged to maintain or increase the pressure (PDM). A second plug screw feeder is arranged to receive the diluted material and to compress, dewater and transport the material to the second reactor unit, wherein the second screw feeder is arranged to operate at a pressure being higher than the pressure of the first plug screw feeder. A system including such an arrangement and a first reactor unit and a second reactor unit is also presented.

First claim

The invention claimed is:

1. An arrangement for feeding and washing lignocellulosic material in a hydrolysis process between a first reactor unit where the material is partly hydrolyzed and a second reactor unit where the material is further hydrolyzed, wherein the first reactor unit operates at a first pressure and the second reactor unit operates at a second pressure being higher than the first pressure, said arrangement comprising:
a first plug screw feeder arranged to receive the partly hydrolyzed material from the first reactor unit and being arranged to compress and dewater the partly hydrolyzed material, and transport the material compressed and dewatered in the first plug screw feeder, wherein the first plug screw feeder is arranged to operate at a pressure being higher than the first pressure;
a dilution vessel coupled to receive the material processed from the first plug screw feeder and including a liquid inlet for receiving liquid to wash the material processed from the first plug screw feeder, wherein the dilution vessel is arranged to maintain or increase the pressure; and
a second plug screw feeder arranged to receive the material processed from the dilution vessel and being arranged to compress and dewater the material processed from the dilution vessel, and transport the material compressed and dewatered in the second plug screw feeder to further processing, wherein the second plug screw feeder is arranged to operate at a pressure being higher than the pressure of the first plug screw feeder.

2. The arrangement according to claim 1 , wherein the dilution vessel is arranged to increase the pressure from the pressure of the first plug screw feeder.

3. The arrangement according to claim 1 , wherein the dilution vessel includes an inlet for receiving steam, wherein the material processed from the first plug screw feeder is mixed with steam and liquid.

4. The arrangement according to claim 1 , wherein the second plug screw feeder is arranged to operate at a pressure of at least the pressure of the dilution vessel.

5. The arrangement according to claim 1 , wherein the dilution vessel is arranged to increase the pressure to the second pressure.

6. The arrangement according to claim 1 , wherein a third plug screw feeder is arranged to compress and dewater the material processed from the second plug screw feeder, and transport the material compressed and dewatered in the third plug screw feeder further, wherein the third screw feeder is arranged to operate at a pressure being higher than the pressure of the second plug screw feeder.

7. The arrangement according to claim 1 , wherein a plug breaker is coupled to the second plug screw feeder.

8. The arrangement according to claim 7 , wherein the plug breaker comprises a rotatable plug breaking member.

9. The arrangement according to claim 1 , wherein the lignocellulosic material has a solid content of at least 30%.

10. A system for two-stage hydrolysis comprising:
a first reactor unit where a lignocellulosic material is partly hydrolyzed and a second reactor unit for further hydrolysis of the partly hydrolyzed material, wherein the first reactor unit operates at a first pressure and the second reactor unit operates at a second pressure being higher than the first pressure;
a first plug screw feeder coupled to the first reactor unit arranged to receive the partly hydrolyzed material from the first reactor unit and being arranged to compress and dewater the partly hydrolyzed material, and transport the material compressed and dewatered in the first plug screw feeder, wherein the first plug screw feeder is arranged to operate at a pressure being higher than the first pressure;
a dilution vessel coupled to receive the material processed from the first plug screw feeder and including a liquid inlet for receiving liquid to wash the material processed from the first plug screw feeder, wherein the dilution vessel is arranged to maintain or increase the pressure; and
a second plug screw feeder arranged to receive the material processed from the dilution vessel and being arranged to compress and dewater the material processed from the dilution vessel, and transport the material compressed and dewatered in the second plug screw feeder to the second reactor unit, wherein the second plug screw feeder is arranged to operate at a pressure being higher than the pressure of the first plug screw feeder.

11. The system according to claim 10 , wherein the dilution vessel is arranged to increase the pressure from the pressure of the first screw feeder.

12. The system according to claim 10 , wherein the dilution vessel includes an inlet for receiving steam, wherein the material processed from the first plug screw feeder is mixed with steam and liquid.

13. The system according to claim 10 , wherein the second plug screw feeder is arranged to operate at a pressure of at least the pressure of the dilution vessel.

14. The system according to claim 10 , wherein the dilution vessel is arranged to increase the pressure to the second pressure.

15. The system according to claim 10 , wherein the first plug screw feeder is directly coupled to the first reactor unit to receive the partly hydrolyzed material and is arranged to compress the partly hydrolyzed material, and transport the material compressed in the first plug screw feeder to the dilution vessel; and the second plug screw feeder is directly coupled to the dilution vessel and is arranged to compress and transport the material processed from the dilution vessel to the second reactor unit.

16. The system according to claim 10 , wherein the first reactor unit is arranged to operate at a temperature above 180° C. degrees.

17. The system according to claim 10 , wherein the second reactor unit is arranged to operate at a temperature above 235° C. degrees.

18. The system according to claim 10 , wherein the first reactor unit is arranged to operate with a treatment time below 5 minutes.

19. The system according to claim 10 , wherein the second reactor unit is arranged to operate with a treatment time below 1 minute.

20. The system according to claim 10 , wherein the first reactor unit includes a horizontal, or vertical, or inclined reactor.

21. The system according to claim 10 , wherein the second reactor unit includes a horizontal, or vertical, or inclined reactor.

22. The system according to claim 10 , wherein the first and second reactors each comprise a conveyor screw with an adjustable rotational speed for transporting the material processed from the first and second reactors towards a discharge outlet at a desired rate.

23. The system according to claim 10 , wherein a plug breaker is coupled between the second plug screw feeder and the second reactor unit.

24. The system according to claim 23 , wherein the plug breaker comprises a rotatable plug breaking member.

25. The system according to claim 10 , wherein the lignocellulosic material has a solid content of at least 30%.

26. A method for feeding and washing lignocellulosic material in a hydrolysis process between a first reactor unit where the material is partly hydrolyzed and a second reactor unit where the material is further hydrolyzed, wherein the first reactor unit operates at a first pressure and the second reactor unit operates at a second pressure being higher than the first pressure, the method comprising the steps of:
a) compressing and dewatering the partly hydro

Assignees

• Valmet Oy

Inventors

• Thyr Anders
• Ahlgren Örjan
• Sjöblom Krister

Classifications

• C08H8/00

  Macromolecular compounds derived from lignocellulosic materials {(pretreatment thereof B27N)} · CPC title

• D21B1/22

  with screw feed · CPC title

• C13K1/02 Primary

  obtained by saccharification of cellulosic materials (manufacture of fodder A23K10/32) · CPC title

• C12P2203/00

  Fermentation products obtained from optionally pretreated or hydrolyzed cellulosic or lignocellulosic material as the carbon source · CPC title

• D21C9/02

  Washing {; Displacing cooking or pulp-treating liquors contained in the pulp by fluids, e.g. wash water or other pulp-treating agents} · CPC title