Particulates for additive manufacturing techniques

Patent metadata

Field	Value
Publication number	US-10041171-B2
Application number	US-201514822713-A
Country	US
Kind code	B2
Filing date	Aug 10, 2015
Priority date	Aug 10, 2015
Publication date	Aug 7, 2018
Grant date	Aug 7, 2018

Abstract

A particulate for an additive manufacturing technique includes metallic particulate bodies with exterior surfaces bearing a polymeric coating. The polymeric coating is conformally disposed over the exterior surface that prevents the underlying metallic body from oxidation upon exposure to the ambient environment by isolating the metallic particulate bodies from the ambient environment. Feedstock materials for additive manufacturing techniques, and methods of making such feedstock, are also disclosed.

First claim

What is claimed is:

1. A method of making particulate for an additive manufacturing technique, the method comprising:
receiving a metallic particulate at a fluidized bed apparatus;
flowing a reducing gas through the metallic particulate;
flowing a drying and degassing gas through the metallic particulate; and
flowing a coating gas from vessel containing a polymeric material maintained at a polymeric material vaporization temperature through the metallic particulate, wherein the metallic particulate is maintained at a coating temperature that is less than the polymeric material vaporization temperature to encapsulate the metallic particulate with polymeric material coatings.

2. A method as recited in claim 1 , wherein the metallic particulate is maintained at a drying and degassing temperature while the drying and degassing gas is flowed therethrough at a temperature that is lower than a reducing temperature at which the metallic particulate is held while the reducing gas is flowed therethrough.

3. A method as recited in claim 1 , wherein the metallic particulate is maintained at coating temperature while the coating gas is flowed therethrough that is less than a drying and degassing temperature at which the metallic particulate is held while the drying the degassing temperature is flowed therethrough.

4. A method as recited in claim 1 , wherein the coating gas is flowed from a vessel containing polymeric material that is maintained at a polymeric material vaporization temperature that is greater than a coating temperature at which the metallic particulate is maintained while the coating gas is flowed therethrough.

5. A method as recited in claim 1 , wherein flowing a reducing gas through the metallic particulate includes removing oxygen from oxidized portions of the metallic particulate prior to flowing the coating gas through the particulate material.

6. A method as recited in claim 1 , wherein flowing a degassing and drying gas flow through the metallic particulate includes removing water vapor generated during the reducing process from the metallic particulate.

7. A method as recited in claim 1 , wherein flowing a drying and degassing gas through the metallic particulate and flowing the coating gas through the metallic particulate include flowing an inert gas from an inert gas source.

8. A method as recited in claim 1 , wherein the particulate body includes elemental copper and the coating includes polydimethylsiloxane.

9. A method as recited in claim 1 , wherein the particulate body is oxide-free, wherein an interface between the particulate body and the polymeric coating is metallic oxide-free.

10. A method of making particulate for an additive manufacturing technique, particles of the particulate having a copper particulate body with a surface and a polymeric coating disposed over the surface of the particulate body, the method comprising:
receiving a copper metallic particulate at a fluidized bed apparatus;
flowing a reducing gas through the metallic particulate;
flowing a drying and degassing gas through the metallic particulate; and
flowing a coating gas containing polydimethylsiloxane from vessel containing a polymeric material maintained at a polymeric material vaporization temperature through the metallic particulate,
wherein the metallic particulate is maintained at a coating temperature that is less than the polymeric material vaporization temperature to encapsulate the metallic particulate with polymeric material coatings,
wherein particulate bodies of the metallic particulate include only elemental copper,
wherein polymeric coatings of the particulate bodies include polydimethylsiloxane, and
wherein interfaces between the particulate bodies and the polymeric coating is metallic oxide-free.

11. A method as recited in claim 10 , further comprising aggregating the coated particulate in a pile having an angle repose smaller than an angle of repose for elemental copper.

Assignees

• Delavan Inc
• Delavan Inc

Inventors

• She Ying
• Klecka Michael A
• El-Wardany Tahany I
• Espinal Anais
• Schmidt Wayde R
• Dardona Sameh

Classifications

• B22F10/10

  Formation of a green body · CPC title

• C23C16/442 Primary

  using fluidised bed process · CPC title

• B22F1/102

  Metallic powder coated with organic material · CPC title

• B01J8/1827 Primary

  the fluidising gas being a reactant · CPC title

• B22F10/34

  of powder characteristics, e.g. density, oxidation or flowability · CPC title