Method for producing water dispersible CuO nanostructures

Patent metadata

Field	Value
Publication number	US-10035712-B2
Application number	US-201514846702-A
Country	US
Kind code	B2
Filing date	Sep 4, 2015
Priority date	Sep 4, 2015
Publication date	Jul 31, 2018
Grant date	Jul 31, 2018

Abstract

A method for producing water dispersible CuO nanostructures includes mixing copper nitrate with an ammonia solution. The copper nitrate and ammonia solution can be treated with ultrasound at room temperature. The water dispersible CuO nanostructures can be produced without any surfactant.

First claim

We claim:

1. A method for producing water dispersible CuO nanostructures, comprising:
dissolving copper nitrate in deionized water to provide an aqueous copper nitrate solution;
placing the aqueous copper nitrate solution in an ultrasonic bath at room temperature for 30 minutes;
mixing ammonia with the copper nitrate solution to form precipitate;
placing the precipitate in an ultrasonic bath to form black precipitate;
washing the black precipitate; and
drying the black precipitate to form CuO nanostructures, wherein the nanostructures are crystalline, spindle-shaped with thickness of about 26.7 nm to about 54.4 nm and a length of about 89.3 nm to about 194.0 nm.

2. The method for producing water dispersible CuO nanostructures according to claim 1 , wherein a pH of the precipitate is adjusted to a level between about 9 and 12.

3. The method for producing water dispersible CuO nanostructures according to claim 1 , wherein the black precipitate is washed with water and ethanol.

4. The method for producing water dispersible CuO nanostructures according to claim 1 , wherein the black precipitate is dried in an oven at about 80° C. for about 24 hours.

5. The method for producing water dispersible CuO nanostructures according to claim 1 , wherein the nanostructures are dispersible in water.

6. A method for producing water dispersible CuO nanostructures, comprising:
dissolving copper nitrate in deionized water to provide an aqueous copper nitrate solution;
placing the aqueous copper nitrate solution in an ultrasonic bath;
mixing ammonia with the copper nitrate solution to form a precipitate;
placing the precipitate in an ultrasonic bath to form a black precipitate;
washing the black precipitate; and
drying the black precipitate to form CuO nanostructures, wherein the nanostructures are crystalline, spindle-shaped with a thickness of about 26.7 nm to about 54.4 nm and a length of about 89.3 nm to about 194.0 nm.

Assignees

• Univ King Abdulaziz

Inventors

• Azam Ameer
• Al-Ghamdi Attieh A

Classifications

• C01P2004/61

  Micrometer sized, i.e. from 1-100 micrometer · CPC title

• C01P2002/85

  by XPS, EDX or EDAX data · CPC title

• C01P2004/62

  Submicrometer sized, i.e. from 0.1-1 micrometer · CPC title

• C01P2004/10

  extending in one dimension, e.g. needle-like · CPC title

• C01P2004/03

  obtained by SEM · CPC title