Production process for TiAl components

Patent metadata

Field	Value
Publication number	US-10029309-B2
Application number	US-201514838802-A
Country	US
Kind code	B2
Filing date	Aug 28, 2015
Priority date	Sep 1, 2014
Publication date	Jul 24, 2018
Grant date	Jul 24, 2018

Abstract

The present invention relates to a process for producing a component, in particular a component for a turbomachine, composed of a TiAl alloy, which comprises the following:
introduction of a powder of the TiAl alloy into the capsule whose shape corresponds to the shape of the component to be produced and closing of the capsule, hot isostatic pressing of the capsule together with the powder, heat treatment of the hot isostatically pressed capsule, removal of the capsule, post-working of the contour of the component by removal of material.

First claim

What is claimed is:

1. A process for producing a component of a TiAl alloy, wherein the process comprises:
introduction of a powder of the TiAl alloy into a capsule whose shape corresponds to a shape of the component to be produced and closing of the capsule,
hot isostatic pressing of the capsule together with the powder,
heat treatment of the hot isostatically pressed capsule,
removal of the capsule,
post-working of a contour of the component by removal of material.

2. The process of claim 1 , wherein the powder has been produced by a process which comprises at least one of the following:
pressing of starting materials or melting of prealloys which consist of or comprise components to be alloyed,
melting of the alloy by one or more of single or multiple plasma arc melting (PAM), vacuum arc remelting (VAR), vacuum induction melting (VIM),
atomization of the alloy to produce the powder from a melt bath or with the aid of a cast ingot,
classification of powder fractions and selection of one or more powder fractions having average or maximum particle diameters or maximum dimensions smaller than or equal to 150 μm, and
purification of the powder in a plasma purification process.

3. The process of claim 1 , wherein the capsule is formed of titanium or a Ti alloy.

4. The process of claim 1 , wherein the capsule is formed by at least two shaped parts.

5. The process of claim 1 , wherein the capsule is overdimensioned relative to the component to be produced.

6. The process of claim 1 , wherein the introduction of the powder is carried out under protective gas or under reduced pressure.

7. The process of claim 1 , wherein the powder before introduction into the capsule or a filled but not yet closed capsule is subjected to a heat treatment under reduced pressure.

8. The process of claim 7 , wherein cooling after the heat treatment is carried out at a cooling rate of from 25° C./min to 35° C./min down to a temperature of 120° C. or less.

9. The process of claim 1 , wherein a packing density of the powder in the capsule is increased by mechanical excitation before or after closing of the capsule.

10. The process of claim 1 , wherein the hot isostatic pressing is carried out in a temperature range of from 1100° C. to 1400° C. at a pressure of from 100 to 250 MPa for from 2 to 6 hours.

11. The process of claim 1 , wherein the heat treatment of the hot isostatically pressed capsule comprises at least two of the following:
a solution heat treatment at a temperature of up to 1400° C. for from 15 to 45 minutes,
a high-temperature heat treatment at a temperature of from 1100° C. to 1300° C. for from 15 to 120 minutes and
an aging heat treatment at a temperature of from 850° C. to 1100° C. for from 6 to 100 hours.

12. The process of claim 11 , wherein the heat treatment of the hot isostatically pressed capsules comprises at least:
a solution heat treatment at a temperature of up to 1400° C. for from 15 to 45 minutes, followed by
a high-temperature heat treatment at a temperature of from 1100° C. to 1300° C. for from 15 to 120 minutes.

13. The process of claim 11 , wherein the heat treatment of the hot isostatically pressed capsule comprises at least:
a high-temperature heat treatment at a temperature of from 1100° C. to 1300° C. for from 15 to 120 minutes, followed by
an aging heat treatment at a temperature of from 850° C. to 1100° C. for from 6 to 100 hours.

14. The process of claim 11 , wherein the heat treatment of the hot isostatically pressed capsule comprises, in the following order:
a solution heat treatment at a temperature of up to 1400° C. for from 15 to 45 minutes,
a high-temperature heat treatment at a temperature of from 1100° C. to 1300° C. for from 15 to 120 minutes and
an aging heat treatment at a temperature of from 850° C. to 1100° C. for from 6 to 100 hours.

15. The process of claim 1 , wherein a net-shape component or near-net-shape component is produced by the hot isostatic pressing.

16. The process of claim 1 , wherein the removal of the capsule is effected by at least one of chemical pickling, electrochemical treatment, mechanical working.

17. The process of claim 1 , wherein the post-working of the contour is carried out by cutting machining and/or by electrochemical treatment.

18. The process of claim 1 , wherein the process further comprises providing the component with one or more functional layers after the post-working of the contour of the component.

19. The process of claim 1 , wherein the alloy comprises Ti and Al as main constituents together with one or more of up to 3 at. % W, from 0.2 to 0.35 at. % Si, up to 0.6 at. % C, up to 6 at. % Zr, up to 0.5 at. % Y, up to 0.3 at. % Hf, up to 0.5 at. % Er, up to 0.5 at. % Gd, up to 0.2 at. % B, from 4 to 25 at. % Nb, from 1 to 10 at. % Mo, from 0.1 to 10 at. % Co, from 0.5 to 3 at. % Cr, from 0.5 to 10 at. % V.

Assignees

• MTU Aero Engines AG

Inventors

• Schloffer Martin
• Smarsly Wilfried

Classifications

• B22F5/04

  of turbine blades · CPC title

• B22F2998/10

  Processes characterised by the sequence of their steps · CPC title

• B22F9/02

  using physical processes · CPC title

• B22D29/00

  Removing castings from moulds, not restricted to casting processes covered by a single main group; Removing cores; Handling ingots {(B22D13/10, B22D11/124, B22D17/00 take precedence)} · CPC title

• B22F9/08

  by casting, e.g. through sieves or in water, by atomising or spraying (using electric discharge B22F9/14) · CPC title